IP Library Granted Patent US 12662380
Granted Patent B1
US 12662380 · App. 17/931,393 · Granted Jun 23, 2026

Printability and profile control of screen-printed gridlines by rheological manipulation

Inventors: Sang M. Han (Albuquerque, NM); Brian Rummel (Albuquerque, NM); Andre Chavez (Albuquerque, NM)
C01B32/158B82Y40/00C01B2202/02
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Quick Facts
Patent No.
US 12662380
App. No.
17/931,393
Granted
Jun 23, 2026
Kind
B1
Abstract

A conductive composition is disclosed. The conductive composition includes a plurality of silver particles and one or more cellulose-based binders. The composition also includes an amount of glass frit, an organic solvent and a plurality of carbon nanotubes, where the conductive composition is formed into a cross-sectional triangular shape, which may include a top cross-sectional dimension and a bottom cross-sectional dimension, where a ratio of the top cross-sectional dimension to the bottom cross-sectional dimension is 0.8 or less. A screen-printed gridline and a method of printing gridlines is also disclosed where the gridlines may be incorporated into a solar cell device.

Claims (56)

1 . A conductive composition, comprising:

a plurality of silver particles;

one or more cellulose-based binders;

an amount of glass frit;

an organic solvent; and

a plurality of carbon nanotubes; and wherein:

a viscosity of the conductive composition is from about 300,000 cP to about 50,000 cP at a shear rate of from about 10/sec to about 40/sec.

2 . The conductive composition of claim 1 , wherein the cross-sectional triangular shape comprises a cross-sectional height of from about 15 μm to about 40 μm.

3 . The conductive composition of claim 1 , wherein the silver particles are present in an amount of from about 10% to about 99% by a total weight of the conductive composition.

4 . The conductive composition of claim 1 , wherein the amount of glass frit has a particle size of 5 μm or less.

5 . The conductive composition of claim 1 , wherein the carbon nanotubes are present in an amount of from about 0.01% to about 20% by a total weight of the conductive composition.

6 . The conductive composition of claim 1 , wherein the carbon nanotubes comprise multi-walled carbon nanotubes having a length of 2 μm or less.

7 . The conductive composition of claim 1 , wherein the carbon nanotubes comprise multi-walled carbon nanotubes having a length of from about 2 μm to about 30 μm.

8 . The conductive composition of claim 1 , wherein the carbon nanotubes comprise single-walled carbon nanotubes having a length of from about 1 μm to about 30 μm.

9 . The conductive composition of claim 1 , wherein the carbon nanotubes comprise a mixture of multi-walled carbon nanotubes and single-walled carbon nanotubes wherein:

the multi-walled carbon nanotubes have a length of 2 μm or less; and

the single-walled carbon nanotubes have a length of from about 1 μm to about 30 μm.

10 . The conductive composition of claim 9 , wherein a ratio of multi-walled carbon nanotubes to single-walled carbon nanotubes is from 1:1 to approximately 9:1.

11 . The conductive composition of claim 1 , having an increased fracture toughness by as much as approximately 600%, as compared to a conductive composition without carbon nanotubes.

12 . A screen-printed gridline, comprising:

a cross-sectional triangular shape, comprising:

a top cross-sectional dimension;

a bottom cross-sectional dimension; and wherein:

a ratio of the top cross-sectional dimension to the bottom cross-sectional dimension is 0.8 or less; and

the conductive composition of claim 1 .

13 . A solar cell device, comprising one or more gridlines having the conductive composition of claim 1 .

14 . A screen-printed gridline, comprising:

a cross-sectional triangular shape, comprising:

a top cross-sectional dimension; and

a bottom cross-sectional dimension; and

a conductive composition; and wherein:

a ratio of the top cross-sectional dimension to the bottom cross-sectional dimension is 0.8 or less; and

the conductive composition comprises:

silver particles;

one or more cellulose-based binders;

glass frit;

an organic solvent; and

carbon nanotubes.

15 . The screen-printed gridline of claim 14 , further comprising a cross-sectional height of the screen-printed gridline of from about 15 μm to about 40 μm.

16 . A method of printing gridlines, comprising:

screen-printing one or more gridlines onto a substrate with a conductive composition comprising silver particles, one or more cellulose-based binders, glass frit, organic solvent, carbon nanotubes; and

sintering the gridlines at an elevated temperature.

17 . The method of claim 16 , wherein the substrate is incorporated into a solar cell device.

18 . The method of claim 16 , wherein a viscosity of the conductive composition prior to sintering is from about 300,000 cP to about 50,000 cP at a shear rate of from about 10/sec to about 40/sec.

19 . The method of claim 16 , wherein the carbon nanotubes are present in an amount of from about 0.01% to about 20% by a total weight of the conductive composition.

20 . The method of claim 16 , wherein the carbon nanotubes comprise multi-walled carbon nanotubes having a length of from about 2 μm to about 30 μm.

21 . The method of claim 16 , wherein the carbon nanotubes comprise a mixture of multi-walled carbon nanotubes and single-walled carbon nanotubes wherein:

the multi-walled carbon nanotubes have a length of 2 micron or less; and

the single-walled carbon nanotubes have a length of from about 1 μm to about 30 μm.

22 . The method of claim 21 , wherein a ratio of multi-walled carbon nanotubes to single-walled carbon nanotubes is from 1:1 to approximately 9:1.

23 . The method of claim 21 , wherein a height of the one or more gridlines is from about 15 to about 40 μm.

24 . The method of claim 16 , wherein the one or more gridlines comprises:

a cross-sectional triangular shape, comprising:

a top cross-sectional dimension; and

a bottom cross-sectional dimension; and

a ratio of the top cross-sectional dimension to the bottom cross-sectional dimension is 0.8 or less.