IP Library Granted Patent US 12662389
Granted Patent B2
US 12662389 · App. 17/923,111 · Granted Jun 23, 2026

Method for producing lithium-containing solution

Inventors: Osamu Ikeda (Niihama, JP); Masatoshi Takano (Niihama, JP); Satoshi Asano (Niihama, JP); Shin-ichi Heguri (Niihama, JP); Shin-ya Matsumoto (Niihama, JP); Yohei Kudo (Niihama, JP); Yusuke Senba (Niihama, JP); Kyohei Maeda (Niihama, JP)
Assignee: SUMITOMO METAL MINING CO., LTD.
C01D15/04B01J39/02B01J39/10B01J49/53
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Quick Facts
Patent No.
US 12662389
App. No.
17/923,111
Granted
Jun 23, 2026
Kind
B2
Abstract

Provided is a method for producing a lithium-containing solution that allows increasing a content rate of lithium in a solution after an eluting step, and suppressing an amount of an eluted solution used in a process after the eluting step, thus suppressing production cost of lithium. A method for producing a lithium-containing solution includes an adsorption step of bringing a lithium adsorbent obtained from lithium manganese oxide in contact with a low lithium-containing solution to obtain post-adsorption lithium manganese oxide, an eluting step of bringing the post-adsorption lithium manganese oxide in contact with an acid-containing solution to obtain an eluted solution, and a manganese oxidation step of oxidating manganese to obtain a lithium-containing solution with a suppressed manganese concentration. The adsorption step, the eluting step, and the manganese oxidation step are performed in this order, and the acid-containing solution includes the eluted solution with acid added. The method allows the usage amount of the acid in the eluting step to be suppressed, the content rate of lithium in the eluted solution after the eluting step to be increased, and thus the production cost of the lithium-containing solution to be suppressed.

Claims (14)

1 . A method for producing a lithium-containing solution, comprising:

an adsorption step of bringing a lithium adsorbent obtained from lithium manganese oxide in contact with a lithium-containing solution to obtain post-adsorption lithium manganese oxide;

an eluting step of bringing the post-adsorption lithium manganese oxide in contact with an acid-containing solution to obtain an eluted solution; and

a manganese oxidation step of oxidating manganese by adding an oxidant and a pH adjuster to the eluted solution to obtain a lithium-containing solution with a suppressed manganese concentration, wherein

the adsorption step, the eluting step, and the manganese oxidation step are performed in this order, and

the acid-containing solution includes the eluted solution with acid added, and wherein:

in the manganese oxidation step, the oxidant is selected from the group consisting of sodium hypochlorite, sodium chlorite, ozone, and permanganate.

2 . A method for producing a lithium-containing solution, comprising:

an adsorption step of bringing a lithium adsorbent obtained from lithium manganese oxide in contact with a lithium-containing solution to obtain post-adsorption lithium manganese oxide;

an eluting step of bringing the post-adsorption lithium manganese oxide in contact with an acid-containing solution to obtain an eluted solution; and

a manganese oxidation step of oxidating manganese by adding an oxidant and a pH adjuster to the eluted solution to obtain a lithium-containing solution with a suppressed manganese concentration, wherein

the adsorption step, the eluting step, and the manganese oxidation step are performed in this order, and

the acid-containing solution includes the eluted solution with acid added, and wherein:

in the manganese oxidation step, the pH adjuster is selected from the group consisting of sodium hydroxide and calcium hydrate.