IP Library Granted Patent US 12662415
Granted Patent B2
US 12662415 · App. 17/642,099 · Granted Jun 23, 2026

Glass filler and method for producing the same, and resin-containing composition including glass filler

Inventors: Hidetoshi Fukuchi (Mie, JP); Tomohiro Yagyu (Mie, JP)
Assignee: NIPPON SHEET GLASS COMPANY, LIMITED
C03C3/093C03C3/087C08K3/40
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Quick Facts
Patent No.
US 12662415
App. No.
17/642,099
Granted
Jun 23, 2026
Kind
B2
Abstract

Provided is a novel glass filler having a low permittivity. The glass filler provided includes a glass composition, wherein the glass composition includes, in wt %: 95≤SiO 2 ≤99.5; 0≤B 2 O 3 ≤2; 0.01≤Al 2 O 3 ≤4; 0≤R 2 O≤4; 0.01≤RO≤4; and 0≤TiO 2 ≤4, where RO is at least one selected from MgO, CaO, SrO, and ZnO, and R 2 O is at least one selected from Li 2 O, Na 2 O, and K 2 O. This glass filler can have a permittivity of less than 4 at 1 GHz.

Claims (58)

1 . A glass filler comprising a glass composition, wherein

the glass composition comprises, in wt %:

95≤SiO 2 ≤99.5;

0≤B 2 O 3 ≤2;

0.01≤Al 2 O 3 ≤4;

0≤R 2 O≤4;

0.2≤RO≤1.5; and

0.1≤TiO 2 ≤2,

where RO is at least one compound selected from the group consisting of MgO, CaO, SrO, and ZnO, and R 2 O is at least one compound selected from the group consisting of Li 2 O, Na 2 O, and K 2 O.

2 . The glass filler according to claim 1 , wherein

the glass composition comprises, in wt %:

95≤SiO 2 ≤99;

0≤B 2 O 3 ≤2;

0.01≤Al 2 O 3 ≤2;

0≤R 2 O≤2;

0.2≤RO≤1.5; and

0.1≤TiO 2 ≤2.

3 . The glass filler according to claim 1 , wherein

the glass composition is substantially free of T-Fe 2 O 3 , where the T-Fe 2 O 3 represents total iron oxide calculated as Fe 2 O 3 .

4 . The glass filler according to claim 1 , wherein

the glass composition is substantially free of R 2 O.

5 . The glass filler according to claim 1 , wherein

the glass composition comprises, in wt %,

95≤SiO 2 ≤99;

0≤B 2 O 3 ≤2;

0.01≤Al 2 O 3 ≤4;

0.4≤R 2 O≤2;

0.2≤RO≤1.5; and

0.1≤TiO 2 ≤2.

6 . The glass filler according to claim 1 , wherein

the glass composition comprises, in wt %,

0.25≤TiO 2 ≤2.

7 . The glass filler according to claim 1 , wherein

the glass composition comprises, in wt %,

97.5≤SiO 2 ≤99.

8 . The glass filler according to claim 1 , wherein

the glass composition comprises, in wt %,

0.2≤Al 2 O 3 ≤0.6.

9 . The glass filler according to claim 1 , wherein

the glass composition comprises, in wt %:

0.05≤MgO≤0.5; and

0.1≤CaO≤1.

10 . The glass filler according to claim 1 , having a permittivity of less than 4 at a frequency of 1 GHz.

11 . The glass filler according to claim 1 , having a surface roughness Ra of 0 to 100 nm.

12 . The glass filler according to claim 1 , having a specific surface area of 0.03 to 10 m 2 /g.

13 . The glass filler according to claim 1 , having a pore volume of 0 to 0.1 cm 3 /g.

14 . The glass filler according to claim 1 , wherein the form of the glass filler is at least one selected from the group consisting of a glass flake, a chopped strand, a milled fiber, a glass powder, a glass bead, and a flat fiber.

15 . A resin-containing composition comprising:

the glass filler according to claim 1 ; and

a resin.

16 . A method for producing the glass filler according to claim 1 , the method comprising:

producing a glass filler precursor including a base glass composition; and

eluting at least partially the base glass composition from the glass filler precursor a so as to obtain the glass filler, which has a glass composition differing in composition from a glass composition of the base glass composition.

17 . The method according to claim 16 , further comprising

heat treating after the eluting, wherein

in the heat treating, a heat treatment at 1000° C. or higher is performed.

18 . The method according to claim 16 , wherein

a SiO 2 content on a weight basis in the glass composition included in the glass filler is higher than a SiO 2 content on a weight basis in the base glass composition.