Transparent wood surface imprinting optical device and application thereof
A transparent wood surface imprinting optical device is provided. A preparation method for the device includes cleaning and drying surfaces of transparent wood, spin-coating polymethyl methacrylate (PMMA) on a substrate of the transparent wood to obtain a PMMA layer, and spin-coating an ultraviolet (UV) glue on the PMMA layer to obtain a UV glue layer; placing the transparent wood on a silicon wafer, attaching a transparent grating array imprinting template on the UV glue layer, exposing the UV glue layer, and removing the transparent grating array imprinting after the exposing, thereby to obtain a grating-structure-based transparent wood; and replacing the grating structure imprinting template by a lattice structure imprinting template to prepare lattice-structure-based transparent wood. The diffraction efficiency of the grating structure and the lattice structure on the transparent wood are greater and more stable than those of PMMA substrates.
1 . A preparation method for a transparent wood surface imprinting optical device, comprising: preparation of transparent wood and preparation of target structure transparent wood;
wherein the preparation of transparent wood comprises:
taking balsa wood as a raw material, and cutting the balsa wood into a wood veneer;
using sodium chlorite to prepare a bleaching solution with a mass fraction in a range of 0.5% to 1.5%;
adjusting, by using one of glacial acetic acid/acetic acid buffer solution, a potential of hydrogen (pH) value of the bleaching solution to be in a range of 4.5 to 4.7;
immersing the balsa wood veneer in the bleaching solution and cooking the balsa wood veneer at a temperature in a range of 75 Celsius degrees (° C.) to 85° C. to obtain delignified porous wood;
prepolymerizing methyl methacrylate (MMA) by using 2,2′-azobisisobutyronitrile as an initiator at a temperature in a range of 70° C. to 80° C. for 15 minutes, to obtain prepolymerized MMA;
placing the prepolymerized MMA in ice water to cool the prepolymerized MMA to an ambient temperature, and then adding the prepolymerized MMA into the delignified porous wood;
impregnating the delignified porous wood filled by the prepolymerized MMA with a solution under a vacuum pressure in a range of −0.09 megapascals (MPa) to −0.08 MPa;
wrapping the delignified porous wood between two layers of glass slides with aluminum foil, and drying and curing the delignified porous wood; and
taking out the delignified porous wood from the two layers of glass slides to obtain the transparent wood;
wherein the preparation of target structure transparent wood comprises:
cleaning and drying a surface of the transparent wood;
spin-coating polymethyl methacrylate (PMMA) on a substrate of the transparent wood to obtain a PMMA layer;
spin-coating an ultraviolet (UV) glue on the PMMA layer to obtain a UV glue layer and thereby obtaining PMMA and UV glue coated transparent wood; and
placing the PMMA and UV glue coated transparent wood on a P-doped (100) n-type silicon wafer with a resistivity in a range of 1 ohm per centimeter (Ω/cm) to 10 Ω/cm, attaching a target template on the UV glue layer, exposing the UV glue layer, and removing the target template after the exposing to obtain target structure transparent wood;
wherein the P-doped (100) n-type silicon wafer is configured to ensure that the PMMA and UV glue coated transparent wood is evenly imprinted by the target template;
wherein the target template is one of a transparent grating array imprinting template and a lattice structure imprinting template; and
wherein in a situation that the target template is the transparent grating array imprinting template, the target structure transparent wood is grating-structure-based transparent wood, and in a situation that the target template is the lattice structure imprinting template, the target structure transparent wood is lattice-structure-based transparent wood.
2 . A preparation method for a transparent wood surface imprinting optical device comprises:
cleaning and drying a surface of transparent wood;
spin-coating PMMA on a substrate of the transparent wood to obtain a PMMA layer;
spin-coating a UV glue on the PMMA layer to obtain a UV glue layer and thereby obtaining PMMA and UV glue coated transparent wood; and
placing the PMMA and UV glue coated transparent wood on a P-doped (100) n-type silicon wafer with a resistivity in a range of 1 Ω/cm to 10 Ω/cm, attaching a target template on the UV glue layer, exposing the UV glue layer, and removing the target template after the exposing to obtain target structure transparent wood;
wherein the P-doped (100) n-type silicon wafer is configured to ensure that the PMMA and UV glue coated transparent wood is evenly imprinted by the target template;
wherein the target template is one of a transparent grating array imprinting template and a lattice structure imprinting template; and
wherein in a situation that the target template is the transparent grating array imprinting template, the target structure transparent wood is grating-structure-based transparent wood, and in a situation that the target template is the lattice structure imprinting template, the target structure transparent wood is lattice-structure-based transparent wood.
3 . The preparation method for the transparent wood surface imprinting optical device as claimed in claim 2 , further comprising:
step 1, taking balsa wood as a raw material, and performing delignification on the balsa wood to prepare delignified porous wood; and
step 2, performing vacuum-repeated impregnation on the delignified porous wood to obtain the transparent wood.
4 . The preparation method for the transparent wood surface imprinting optical device as claimed in claim 3 , wherein in the step 1, the performing delignification comprises:
cutting the balsa wood into a balsa wood veneer;
using sodium chlorite to prepare a bleaching solution with a mass fraction in a range of 0.5% to 1.5%;
adjusting, by using one of glacial acetic acid or acetic acid buffer solution, a pH value of the bleaching solution to be in a range of 4.5 to 4.7; and
immersing the balsa wood veneer in the bleaching solution and boiling cooking the balsa wood veneer at a temperature in a range of 75° C. to 85° C. to obtain the delignified porous wood.
5 . The preparation method for the transparent wood surface imprinting optical device as claimed in claim 4 , wherein in the step 2, the vacuum-repeated impregnation comprises:
prepolymerizing MMA by using 2,2′-azobisisobutyronitrile as an initiator at a temperature in a range of 70° C. to 80° C. for 15 minutes, to obtain prepolymerized MMA;
placing the prepolymerized MMA in ice water to cool the prepolymerized MMA to an ambient temperature, and then adding the prepolymerized MMA into the delignified porous wood;
impregnating the delignified porous wood filled by the prepolymerized MMA with a solution under a vacuum pressure in a range of −0.09 MPa to −0.08 MPa;
wrapping the delignified porous wood between two layers of glass slides with aluminum foil, and drying and curing the delignified porous wood; and
taking out the delignified porous wood from the two layers of glass slides to obtain the transparent wood.