IP Library Granted Patent US 12668049
Granted Patent B2
US 12668049 · App. 18/076,226 · Granted Jun 30, 2026

Methods and formulations for bonding dissimilar materials

Inventors: Zehra Sevinc (Franklin Lakes, NJ); Tea Datashvili (Franklin Lakes, NJ); Fanqing Meng (Franklin Lakes, NJ); Shang-Ren Wu (Franklin Lakes, NJ); Chinnu Brahatheeswaran (Franklin Lakes, NJ)
Assignee: CAREFUSION 303, INC.
B32B37/12C09J5/00C09J11/06C09J11/08C09J151/06B32B2323/00B32B2369/00C09J2423/04C09J2427/006C09J2431/00C09J2451/00C09J2455/006C09J2469/006
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Quick Facts
Patent No.
US 12668049
App. No.
18/076,226
Granted
Jun 30, 2026
Kind
B2
Abstract

The present disclosure is directed to a formulations of cements and methods for bonding dissimilar materials. The formulations and methods can bond a Non-polyvinyl chloride (PVC) containing first polyolefin that is amorphous or has low crystallinity to a second material that is a rigid material or a hard PVC. The methods and formulations can work by co-dissolution at an interface, or activation of a one of the materials prior to bonding.

Claims (21)

1 . A method of bonding a first material to a second material, the first and second materials being dissimilar, wherein

the first material comprises a non-polyvinyl chloride (Non-PVC) polyolefin polymer, wherein the Non-PVC polyolefin polymer is amorphous or has a degree of crystallinity in the range of about 0.1% to about 50% crystallinity;

the second material comprises a rigid amorphous material having a tensile modulus in the range of about 1800 to about 3000 MPa, a PVC having a Shore A hardness in the range of about 70 to about 85, or a combination thereof;

the method comprising:

i.) modifying the first material with a polar functional group, the polar functional group increasing an affinity of the first material to the second material, wherein modifying the first material comprises:

grafting the polar functional group to the first material via a reactive extrusion, wherein the reactive extrusion comprises activating the first material with an initiator to provide an activated material;

ii.) bonding the first material to the second material, wherein bonding the first material to the second material comprises integrating the modified first material to the second material by applying a solvent at an interface between the modified first material and the second material.

2 . The method of claim 1 , wherein the initiator is selected from the group consisting of benzyl peroxide, dicumyl peroxide, and 2,2′-Azobisisobutyronitrile.

3 . The method of claim 1 , wherein the polar functional group is formed from reacting with a monomeric compound comprising at least one ester group.

4 . The method of claim 3 , wherein the monomeric compound comprises a carbon-carbon double bond capable of reacting with the activated material.

5 . The method of claim 3 , wherein the monomeric compound is selected from the group consisting of methyl methacrylate, glycidyl methacrylate, and vinyl acetate.

6 . The method of claim 1 , wherein modifying the first material comprises grafting the polar functional group to the first material using one or more tackifiers selected from the group consisting of a terpene phenol, a styrenated terpene, a rosin ester, a terpene resin, and a hydrocarbon resin.

7 . The method of claim 1 , wherein the solvent is selected from the group consisting of cyclohexanone, methyl ethyl ketone, cyclohexane, ethyl acetate, isobutyl acetate, n-butyl acetate, methyl isobutyl ketone, tetrahydrofuran, heptane, and any combination thereof.

8 . The method of claim 1 , wherein modifying the first material further comprises combining the first material with up to about 10 wt % of a secondary compatibilizer selected from polyether amine, ethylene-vinyl acetate (EVA), or both, wherein the secondary compatibilizer increases the polarity of the first material.

9 . The method of claim 1 , wherein modifying the first material further comprises combining the first material with up to about 1 wt % of an antioxidant, up to about 1 wt % of a processing aid, or both.

10 . The method of claim 9 , wherein the antioxidant is selected from the group consisting of penterythritol tetrakis (3-(3,5-di-t-butyl-4-hydroxyphenyl)propionate), or 1, 3, 5-trimethyl-2,4,6-tris (3,5-di-tert-butyl-4-hydroxybenzyl) benzene.

11 . The method of claim 1 , wherein modifying the first material further comprises combining the first material with up to about 10 wt % of an isoprene-based tackifier.

12 . The method of claim 11 , wherein the isoprene-based tackifier is a terpene.

13 . The method of claim 1 , wherein the non-PVC polyolefin polymer is a styrenic based thermoplastic elastomer (TPE) or a styrenic based thermoplastic olefin (TPO).

14 . The method of claim 1 , wherein the rigid amorphous material comprises a polycarbonate or copolymer thereof, a polyacrylate or copolymer thereof, or an acrylonitrile butadiene styrene (ABS) or copolymer thereof.

15 . The method of claim 1 , wherein an adhesive is not utilized in bonding the first material to the second material.