IP Library Granted Patent US 12668524
Granted Patent B2
US 12668524 · App. 18/049,853 · Granted Jun 30, 2026

Glass and method for manufacturing glass

Inventors: Mikio Nagano (Chiyoda-ku, JP); Seiji Inaba (Chiyoda-ku, JP); Rikiya Kado (Chiyoda-ku, JP); Kiyoshi Tamai (Chiyoda-ku, JP); Yuha Kobayashi (Chiyoda-ku, JP)
Assignee: AGC Inc.
C03C3/085C03C3/062H10W74/019
View Patent ↗
Loading inventors, assignments & file history…
Monitor This Case
Get email alerts when status or documents change.
Order Certified Copies
Most orders are placed with the USPTO same day — all within 24 business hours.
Order via The Patent Place →
Pre-filled with this patent's details
Quick Facts
Patent No.
US 12668524
App. No.
18/049,853
Granted
Jun 30, 2026
Kind
B2
Abstract

Glass contains, in mol percentage on an oxide basis, SiO 2 : 35% to 60%, B 2 O 3 : 0.8% to 8%, Al 2 O 3 : 6% to 21%, and MgO: 17% to 44%. Additionally, (MgO/Al 2 O 3 )≥1 is satisfied, a measured Madelung constant m calculated by an expression (1A) is equal to or larger than 1.05, and a thermal expansion factor as a ratio of a measured value α of a linear thermal expansion coefficient to a calculated value α cal of a linear thermal expansion coefficient calculated from composition is equal to or smaller than 0.7. Herein, E is a measured value of a Young's modulus of the glass, V p is an average atomic packing factor of the glass, and G t is average bond dissociation energy of the glass.

Claims (234)

1 . Glass A glass containing:

SiO 2 : 35% to 60%;

B 2 O 3 : 0.8% to 8%;

Al 2 O 3 : 6% to 21%; and

MgO: 17% to 44% and

TiO 2 : 0.3% to 8%,

in mol percentage on an oxide basis, wherein

(MgO/Al 2 O 3 )≥1 is satisfied,

a measured Madelung constant m calculated by an expression (1A) is equal to or larger than 1.05,

m

=

E

/

(

2

·

V

p

·

G

t

)

(

1

A

)

where E is a measured value of a Young's modulus (GPa) of the glass, V p is an average atomic packing factor of the glass, and G, is average bond dissociation energy of the glass, and

a thermal expansion factor as a ratio of a measured value α (ppm/K) of a linear thermal expansion coefficient to a calculated value α cal (ppm/K) of the linear thermal expansion coefficient calculated from composition is equal to or smaller than 0.7.

2 . The glass according to claim 1 , wherein

assuming that a thermal expansion parameter α pi of an oxide is a value calculated by the following expression (2A), a calculated value α cal of a linear thermal expansion coefficient of glass containing only a modified oxide component of a monovalent element contained in the glass is a value calculated by the following expression (2B), a calculated value α cal 2 of a linear thermal expansion coefficient of glass containing only a modified oxide component of a divalent element contained in the glass is a value calculated by the following expression (2C), and a calculated value α cal 3 of a linear thermal expansion coefficient of glass containing only a modified oxide component of a trivalent element contained in the glass is a value calculated by the following expression (2D),

the calculated value deal is calculated by the following expression (2E),

α

p

i

=

{

ni

/

(

ni

-

1

)

}

·

(

Z

+

i

·

Z

-

i

/

r

e

q

i

)

-

1

(

2

A

)

α

ca

l

1

=

(

290

·

α

p

-

8

9

.6

)

/

10

(

2

B

)

α

ca

l

2

=

(

300

·

α

p

-

4

9

.1

)

/

10

(

2

C

)

α

ca

l

3

=

(

848

·

α

p

-

2

34

)

/

10

(

2

D

)

α

ca

l

=

(

M

1

·

α

ca

l

1

+

M

2

·

α

ca

l

2

+

M

3

·

α

ca

l

3

)

/

{

10

·

(

M

1

+

M

2

+

M

3

)

(

2

E

)

where ni is a Born exponent, Z +i is a cationic charge of the oxide, Z −i is an anionic charge of the oxide, r eqi is an equilibrium value of an average distance between a pair of ions of the oxide at a temperature 0 (K), α p in the expressions (2B), (2C), and (2D) is a numerical value obtained by adding up values that are obtained by multiplying the expression (2A) by a cation ratio of each oxide, M1 is a cation ratio (%) of a content of a modified oxide of the monovalent element, M2 is a cation ratio (%) of a content of a modified oxide of the divalent element, and M3 is a cation ratio (%) of a content of a modified oxide of the trivalent element.

3 . The glass according to claim 1 , wherein the measured Madelung constant m is equal to or smaller than 1.35.

4 . The glass according to claim 1 , wherein the thermal expansion factor is equal to or larger than 0.45.

5 . The glass according to claim 1 , containing:

CaO: 0% to 8%,

TiO 2 : 0.3% to 8%,

ZrO 2 : 0% to 8%,

Na 2 O 3 : 0% to 7%, and

K 2 O: 0% to 6%,

in mol percentage on an oxide basis.

6 . The glass according to claim 1 , containing:

SiO 2 : 35% to 52%,

Al 2 O 3 : 9.6% to 20%,

MgO: 24% to 44%,

B 2 O 3 : 0.8% to 4.5%, and

TiO 2 : 0.3% to 5%,

in mol percentage on an oxide basis.

7 . The glass according to claim 1 , wherein the glass is amorphous glass.

8 . The glass according to claim 1 , wherein the glass is a support glass substrate for manufacturing at least one of a Fan Out Wafer Level Package and a Fan Out Panel Level Package.

9 . A method for manufacturing the glass of claim 1 , the method comprising:

shaping glass, the glass containing:

SiO 2 : 35% to 60%,

B 2 O 3 : 0.8% to 8%,

Al 2 O 3 : 6% to 21%, and

MgO: 17% to 44%, and

TiO 2 : 0.3% to 8%,

in mol percentage on an oxide basis;

holding the shaped glass at a temperature higher than a glass transition point Tg by a temperature equal to or higher than 0° C. and equal to or lower than 100° C. for a time longer than 0 hours and equal to or shorter than 10 hours; and

cooling the glass so that a temperature lowering speed is equal to or higher than 0.5° C./min and equal to or lower than 100° C./min.