IP Library Granted Patent US 12668739
Granted Patent B2
US 12668739 · App. 17/632,913 · Granted Jun 30, 2026

Organic electroluminescent element and electronic device using same

Inventors: Hiroaki Itoi (Sodegaura, JP); Yuki Nakano (Sodegaura, JP); Satomi Tasaki (Sodegaura, JP); Taro Yamaki (Sodegaura, JP)
Assignee: IDEMITSU KOSAN CO., LTD.
C09K11/06C07C13/62C07C15/62C07C49/76C07C211/54C07C255/50C07C321/26C07D209/86C07D213/16C07D215/06C07D223/24C07D235/08C07D277/66C07D279/22C07D311/82C07D333/54C07D335/12C07D405/10C07D405/14C07D407/10C07D409/04C07D409/10C07D487/22C07D493/04C07F5/027C07F7/081C07F7/0812C07F9/28H10K50/11H10K85/40H10K85/60H10K85/615H10K85/621H10K85/622H10K85/623H10K85/624H10K85/625H10K85/631H10K85/649H10K85/652H10K85/653H10K85/654H10K85/655H10K85/656H10K85/6572H10K85/6574H10K85/6576H10K85/658C07B2200/05
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Quick Facts
Patent No.
US 12668739
App. No.
17/632,913
Granted
Jun 30, 2026
Kind
B2
Abstract

An organic electroluminescence device comprising: a cathode, an anode, and an organic layer disposed between the cathode and the anode, wherein the organic layer comprises a compound represented by the following formula (1), and a compound A having a Stokes shift of 20 nm or smaller and an emission peak wavelength of 440 nm to 465 nm (at least one of Ar 1 and Ar 2 is a monovalent group having a structure represented by the following formula (2)).

Claims (232)

1 . An organic electroluminescence device comprising:

a cathode;

an anode; and

an organic layer disposed between the cathode and the anode, wherein

the organic layer comprises a compound represented by the following formula (1-1) or the following formula (1-2), and

a compound A having a Stokes shift of 20 nm or smaller and an emission peak wavelength of 440 nm to 465 nm

wherein in the formula (1-1) or (1-2),

one or more sets of adjacent two or more of R 1 to R 8 form a substituted or unsubstituted, saturated or unsaturated ring by bonding with each other, or do not form a substituted or unsubstituted, saturated or unsaturated ring;

R 1 to R 8 that do not form the substituted or unsubstituted, saturated or unsaturated ring are independently a hydrogen atom or a substituent R;

the substituent R is

a halogen atom,

a cyano group,

a nitro group,

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted alkenyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted alkynyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms,

—Si(R 901 )(R 902 )(R 903 ),

—O—(R 904 ),

—S—(R 905 ),

—N(R 906 )(R 907 ),

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms;

R 901 to R 907 are independently

a hydrogen atom,

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms,

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms;

when two or more of each of R 901 to R 907 are present, the two or more of each of R 901 to R 907 are the same as or different from each other;

L 1 and L 2 are independently

a single bond,

a substituted or unsubstituted arylene group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted divalent heterocyclic group including 5 to 50 ring atoms;

X 1 is O;

one or more sets of adjacent two or more of R 11 to R 14 and adjacent two or more of R 15 to R 20 form a substituted or unsubstituted, saturated or unsaturated ring by bonding with each other, or do not form a substituted or unsaturated, saturated or unsaturated ring;

R 11 to R 20 that do not form the substituted or unsubstituted, saturated or unsaturated ring are independently a hydrogen atom or a substituent R;

the substituent R is as defined in the formula (1-1) or (1-2);

Ar 2 is

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms.

2 . The organic electroluminescence device according to claim 1 , wherein L 1 and L 2 are independently

a single bond, or

a substituted or unsubstituted arylene group including 6 to 14 ring carbon atoms.

3 . The organic electroluminescence device according to according to claim 1 , wherein L 1 and L 2 are independently

a single bond,

a substituted or unsubstituted phenylene group,

a substituted or unsubstituted naphthylene group,

a substituted or unsubstituted fluorenylene group,

a substituted or unsubstituted phenanthrylene group, or

a substituted or unsubstituted biphenyldiyl group.

4 . The organic electroluminescence device according to claim 1 , wherein either or both of L 1 and L 2 are single bonds.

5 . The organic electroluminescence device according to claim 1 , wherein the compound represented by the formula (1-1) or (1-2) is a compound represented by the following formula (1-1-1):

wherein in the formula (1-1-1), R 1 to R 8 , L 2 , Ar 2 , X 1 , R 11 to R 17 , R 19 , and R 20 are as defined in the formula (1-1) or (1-2).

6 . The organic electroluminescence device according to claim 1 , wherein L 2 is a single bond.

7 . The organic electroluminescence device according to claim 1 , wherein Ar 2 is

a substituted or unsubstituted phenyl group,

a substituted or unsubstituted naphthyl group,

a substituted or unsubstituted fluorenyl group,

a substituted or unsubstituted phenanthryl group,

a substituted or unsubstituted biphenyl group,

a substituted or unsubstituted chrysenyl group,

a substituted or unsubstituted benzophenanthrenyl group,

a substituted or unsubstituted benzotriphenylenyl group,

a substituted or unsubstituted dibenzofuranyl group,

a substituted or unsubstituted naphthobenzofuranyl group,

a substituted or unsubstituted carbazolyl group, or

a substituted or unsubstituted benzo[def]carbazolyl group.

8 . The organic electroluminescence device according to claim 1 , wherein Ar 2 is a group represented by any of the following formulas (Ar 2 -11) to (Ar 2 -14):

wherein in the formulas (Ar 2 -11) to (Ar 2 -14),

* is bonded with L 2 ;

R a is a substituent;

the substituent R a is

a halogen atom,

a cyano group,

a nitro group,

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted alkenyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted alkynyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms,

—Si(R 901 )(R 902 )(R 903 ),

—O—(R 904 ),

—S—(R 905 ),

—N(R 906 )(R 907 ),

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms;

R 901 to R 907 are as defined in the formula (1-1) or (1-2);

m1 is an integer of 0 to 4;

m2 is an integer of 0 to 5;

m3 is an integer of 0 to 7;

when each of m1 to m3 is 2 or more, a plurality of R a 's may be the same as or different from each other;

when m1 to m3 are each 2 or more, a plurality of adjacent R a 's form a substituted or unsubstituted, saturated or unsaturated ring by bonding with each other, or do not form a substituted or unsubstituted, saturated or unsaturated ring.

9 . The organic electroluminescence device according to claim 1 , wherein Ar 2 -L 2 -,

a substituted or unsubstituted phenyl group,

a substituted or unsubstituted naphthyl group,

a substituted or unsubstituted phenylnaphthyl group,

a substituted or unsubstituted biphenyl group,

a substituted or unsubstituted naphthylphenyl group,

a substituted or unsubstituted fluorenyl group,

a substituted or unsubstituted phenanthryl group,

a substituted or unsubstituted phenylphenanthryl group,

Substituted or unsubstituted benzophenanthryl groups

a substituted or unsubstituted benzotriphenylenyl group,

a substituted or unsubstituted chrysenyl group,

a substituted or unsubstituted dibenzofuranyl group,

a substituted or unsubstituted phenyldibenzofuranyl group,

a substituted or unsubstituted naphthobenzofuranyl group,

a substituted or unsubstituted carbazolyl group,

a substituted or unsubstituted carbazolyl-phenyl group, or

a substituted or unsubstituted benzo[def]carbazolyl-phenyl group.

10 . The organic electroluminescence device according to claim 1 , wherein one or more of

R 1 to R 8 that are hydrogen atoms,

R 11 to R 20 that are hydrogen atoms,

hydrogen atoms possessed by the substituted or unsubstituted, saturated or unsaturated ring formed by bonding one or more sets of adjacent two or more of R 1 to R 8 with each other,

hydrogen atoms possessed by R 1 to R 8 that are the substituents R,

hydrogen atoms possessed by the substituted or unsubstituted, saturated or unsaturated ring formed by bonding one or more sets of adjacent two or more of R 11 to R 20 with each other,

hydrogen atoms possessed by R 11 to R 20 that are the substituents R,

hydrogen atoms possessed by L 1 ,

hydrogen atoms possessed by L 2 , and

hydrogen atoms possessed by Ar 2 are deuterium atoms.

11 . The organic electroluminescence device according to claim 1 , wherein the compound A is one or more selected from the group consisting of a compound represented by the following formula (11), a compound represented by the following formula (21), a compound represented by the following formula (31), and a compound represented by the following formula (41):

wherein in the formula (11),

one or more sets of adjacent two or more of R 101 to R 107 and R 111 to R 117 form a substituted or unsubstituted, saturated or unsaturated ring by bonding with each other, or do not form a substituted or unsubstituted, saturated or unsaturated ring;

R 121 and R 122 , and R 101 to R 107 and R 111 to R 117 that do not form the substituted or unsubstituted, saturated or unsaturated ring are independently a hydrogen atom or a substituent R; and

the substituent R is as defined in the formula (1-1) or (1-2);

wherein in the formula (21),

a ring a, a ring b, and a ring c are independently

a substituted or unsubstituted aromatic hydrocarbon ring including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted heterocycle including 5 to 50 ring atoms;

R 201 forms a substituted or unsubstituted heterocycle by bonding with either or both of the ring a and the ring b, or do not form a substituted or unsubstituted heterocycle;

R 202 forms a substituted or unsubstituted heterocycle by bonding with either or both of the ring a and the ring c, or do not form a substituted or unsubstituted heterocycle;

R 201 and R 202 that do not form the substituted or unsubstituted heterocycle are independently

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted alkenyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted alkynyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms,

—Si(R 901 )(R 902 )(R 903 ),

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms; and

R 901 to R 903 are as defined in the formula (1-1) or (1-2);

wherein in the formula (31),

any one or more sets among one or more sets of adjacent two or more of R 311 to R 320 , one or more sets of adjacent two or more of R 301 to R 305 , and one or more sets of adjacent two or more of R 306 to R 310 form a substituted or unsubstituted, saturated or unsaturated ring including 3 to 30 ring atoms by bonding with each other;

R 311 to R 320 , R 301 to R 305 , and R 306 to R 310 that do not form the substituted or unsubstituted, saturated or unsaturated ring are independently a hydrogen atom or a substituent R b ;

the substituent R b is

a halogen atom, a cyano group, a nitro group, a carboxy group,

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted alkenyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted alkynyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms,

—Si(R 901 )(R 902 )(R 903 ),

—O—(R 904 ),

—S—(R 905 ),

—N(R 906 )(R 907 ),

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms,

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms,

a substituted or unsubstituted phosphanyl group,

a substituted or unsubstituted phosphoryl group, or

a substituted or unsubstituted arylcarbonyl group including 6 to 50 ring carbon atoms; and

R 901 to R 907 are as defined in the formula (1-1) or (1-2); and

wherein in the formula (41),

a ring d is a substituted or unsubstituted aromatic hydrocarbon ring including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted heterocycle including 5 to 50 ring atoms;

L 401 to L 404 are independently

a single bond,

a substituted or unsubstituted arylene group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted divalent heterocyclic group including 5 to 50 ring atoms;

Ar 401 to Ar 404 are independently

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms,

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms; and

provided that, when the ring d is a substituted or unsubstituted aromatic hydrocarbon ring including 10 to 50 ring carbon atoms, two or more of Ar 401 to Ar 404 are independently

an aryl group including 6 to 50 carbon atoms substituted by an alkyl group including 1 to 50 carbon atoms, or

a monovalent heterocyclic group including 5 to 50 ring atoms substituted by an alkyl group including 1 to 50 carbon atoms.

12 . The organic electroluminescence device according to claim 11 , wherein the compound represented by the formula (11) is a compound represented by the following formula (12):

wherein in the formula (12), R 101 to R 104 , R 111 to R 114 , R 121 , and R 122 are as defined in the formula (11); and

R 131 to R 134 are independently

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms.

13 . The organic electroluminescence device according to claim 11 , wherein the compound represented by the formula (11) is a compound represented by the following formula (13):

wherein in the formula (13), R 121 and R 122 are as defined in the formula (1-1) or (1-2), and R 131 to R 134 are as defined in the formula (12).

14 . The organic electroluminescence device according to claim 11 , wherein

the ring a, the ring b, or the ring c in the formula (21) is the substituted aromatic hydrocarbon ring including 6 to 50 ring carbon atoms, or the substituted heterocycle including 5 to 50 ring atoms, and

the substituent is one or more selected from the group consisting of:

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

—Si(R 901 )(R 902 )(R 903 ),

—N(R 906 )(R 907 ) (where R 901 to R 903 , R 906 , and R 907 are as defined in the formula (1-1) or (1-2),

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, and

a substituted or unsubstituted monovalent heterocyclic group including 5 to 60 ring atoms.

15 . The organic electroluminescence device according to claim 11 , wherein the compound represented by the formula (21) is a compound represented by the following formula (22):

wherein in the formula (22),

R 201A forms a substituted or unsubstituted heterocycle by bonding with one or more selected from the group consisting of R 211 and R 221 , or do not form a substituted or unsubstituted heterocycle;

R 202A forms a substituted or unsubstituted heterocycle by bonding with one or more selected from the group consisting of R 213 and R 214 , or do not form a substituted or unsubstituted heterocycle;

R 201A and R 202A that do not form the substituted or unsubstituted heterocycle are independently

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted alkenyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted alkynyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms,

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms;

one or more sets of adjacent two or more of R 211 to R 221 form a substituted or unsubstituted, saturated or unsaturated ring by bonding with each other, or do not form a substituted or unsubstituted, saturated or unsaturated ring;

R 211 to R 221 that do not form the substituted or unsubstituted heterocycle, or the substituted or unsubstituted, saturated or unsaturated ring are independently

a hydrogen atom,

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted alkenyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted alkynyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms,

—Si(R 901 )(R 902 )(R 903 ),

—O—(R 904 ),

—S—(R 905 ),

—N(R 906 )(R 907 ),

a halogen atom, a cyano group, a nitro group,

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms, or

a substituted or unsubstituted monovalent heterocyclic group including 5 to 50 ring atoms; and

R 901 to R 907 are as defined in the formula (1-1) or (1-2).

16 . The organic electroluminescence device according to claim 11 , wherein the compound represented by the formula (21) is a compound represented by the following formula (23A):

wherein in the formula (23A),

R 261 to R 265 are

a hydrogen atom,

a substituted or unsubstituted alkyl group including 1 to 50 carbon atoms,

a substituted or unsubstituted alkenyl group including 2 to 50 carbon atoms,

a substituted or unsubstituted alkynyl group including 2 to 50 carbon atoms,

—N(R 906 )(R 907 ),

a substituted or unsubstituted cycloalkyl group including 3 to 50 ring carbon atoms, or

a substituted or unsubstituted aryl group including 6 to 50 ring carbon atoms;

R 906 and R 907 are as defined in the formula (1-1) or (1-2); and when two or more of each of R 906 and R 907 are present, the two or more of each of R 906 and R 907 are the same as or different from each other.

17 . The organic electroluminescence device according to claim 11 , wherein the ring d in the formula (41) is a substituted or unsubstituted divalent group having a structure selected from the group consisting of structures represented by the following formulas.

18 . The organic electroluminescence device according to claim 11 , wherein the ring d in the formula (41) is a substituted or unsubstituted pyrene ring.

19 . The organic electroluminescence device according to claim 1 , wherein

the organic layer comprises an emitting layer, and

the emitting layer comprises the compound represented by the formula (1-1) or (1-2) and the compound A.

20 . An electronic apparatus equipped with the organic electroluminescence device according to claim 1 .