IP Library Granted Patent US 12673899
Granted Patent B2
US 12673899 · App. 18/004,080 · Granted Jul 7, 2026

Moisture regulating material and production method thereof

Inventors: Nevin Gül Karagüler (Istanbul, TR); Hande Mumcu (Istanbul, TR); Yildiz Yildirim (Çan, TR); Elif Solak (Çan, TR); Kagan Kayaci (Çan, TR); Erdem Günsür (Besiktas, TR)
C04B33/20C04B2235/3409C04B2235/349C04B2235/448C04B2235/6567C04B2235/6588
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Quick Facts
Patent No.
US 12673899
App. No.
18/004,080
Granted
Jul 7, 2026
Kind
B2
Abstract

Disclosed is a moisture regulating ceramic material production method which includes the following process steps: mixing starting powders containing sepiolite and reactive alumina sulfate; grinding the starting powders; obtaining granules by dry granulation using alkaline solution with the starting powders; carrying out a pressing process of the granules; and obtaining the materials.

Claims (33)

1 . A method for producing a moisture-regulating ceramic material, the method comprising:

mixing a sepiolite and a reactive alumina silicate to form a starting powder;

grinding the starting powder;

adding an alkaline solution to the starting powder;

obtaining granules by dry granulation of the alkaline-added starting powder;

pressing the obtained granules, wherein a weight ratio of the sepiolite and the reactive alumina silicate and the alkaline solution are between 4.5% to 7.5% and 26% to 29% and 54.5% to 64%, respectively;

adding 3% to 10% by weight of the boron-containing material to the starting powder or alkaline solution; and

geopolymerizing a structure obtained by the pressing of the granules at a temperature of between 25° C. and 250° C. in an environment of at least 50% humidity for a period of time of between two hours and twenty-four hours.

2 . The method of claim 1 , wherein the boron-containing material is boric acid.

3 . The method of claim 2 , wherein the boric acid has a weight ratio of between 3% and 8%.

4 . The method of claim 2 , wherein the weight ratio of the reactive alumina silicate is between 27% and 29%.

5 . The method of claim 2 , wherein the weight ratio of the sepiolite is between 6% and 7.5%.

6 . The method of claim 1 , wherein the boron-containing material is borax.

7 . The method of claim 6 , wherein the ratio of the borax is between 5% and 8%.

8 . The method of claim 6 , wherein the weight ratio of the reactive alumina silicate is between 26% and 27.25%.

9 . The method of claim 6 , wherein the weight ratio of the sepiolite is between 4.5% and 6.75%.

10 . The method of claim 1 , wherein the boron-containing material is a mixture of boric acid and borax.

11 . The method of claim 10 , wherein the mixture is mixed with waterglass at an ambient temperature of between 25° C. and 35° C. for between ten minutes and fifteen minutes.

12 . The method of claim 1 , wherein the reactive alumina silicate is metakaolin.

13 . The method of claim 1 , wherein the alkaline solution contains a caustic and a waterglass.

14 . The method of claim 13 , wherein the alkaline solution contains water.

15 . The method of claim 1 , wherein the step of geopolymerization is carried out in the environment of at least 80% humidity.

16 . The method of claim 1 , wherein the step of geopolymerization is carried out at a temperature of between 125° C. and 175° C.

17 . The method of claim 1 , further comprising:

embossing the moisture regulating ceramic material.

18 . The method of claim 1 , further comprising:

coloring the moisture regulating ceramic material.

19 . The method of claim 1 , further comprising:

partially glazing the moisture regulating ceramic material.

20 . The method of claim 1 , wherein the boron-containing material is added to the starting powder is solid form.

21 . The method of claim 1 , wherein the boron-containing material is added to the alkaline solution in liquid form.

22 . The method of claim 21 , wherein the boron-containing material is added to the alkaline solution by being dissolved in the alkaline solution.

23 . The method of claim 1 , wherein the boron-containing solution is added to the starting powder or to the alkaline solution in a fluid form.