IP Library Granted Patent US 12674034
Granted Patent B2
US 12674034 · App. 17/584,569 · Granted Jul 7, 2026

Biodegradable biopolymer films

Inventors: Orlin D. Velev (Raleigh, NC); Yosra Kotb (Raleigh, NC)
Assignee: North Carolina State University
C08J5/18B65D65/466C08L5/08C08L5/12C08J2305/08C08J2305/12C08J2405/08C08J2405/12C08L2201/06C08L2203/16
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Quick Facts
Patent No.
US 12674034
App. No.
17/584,569
Granted
Jul 7, 2026
Kind
B2
Abstract

Provided is a biopolymer composite film that includes a polysaccharide matrix reinforced with soft dendritic colloids and methods for making. The method can include dissolving agarose in water to form a first mixture, mixing nanofibrillated chitosan in the agarose, sonicating or stirring the mixture to form a homogeneous second mixture, casting the second mixture, and gelling the second mixture to form a film. Also provided is a food or consumer product packaging film that includes the biopolymer composite film.

Claims (17)

1 . A biopolymer composite film comprising a polysaccharide and soft dendritic colloids, wherein the soft dendritic colloids are about 5% w/w to 20% of the polysaccharide, and wherein the soft dendritic colloids are synthesized from chitosan to form nanofibrillated chitosan.

2 . The biopolymer composite film according to claim 1 , wherein the polysaccharide is agarose.

3 . The biopolymer composite film according to claim 1 , further comprising a plasticizer.

4 . A biopolymer composite film comprising a polysaccharide and soft dendritic colloids;

wherein the soft dendritic colloids are synthesized from chitosan to form nanofibrillated chitosan;

wherein the polysaccharide is agarose;

wherein the nanofibrillated chitosan is about 15% w/w of the agarose; and

wherein the biopolymer composite film has a tensile strength of about 50 MPa.

5 . A consumer product packaging film comprising:

a biopolymer composite film comprising a polysaccharide and soft dendritic colloids, wherein the soft dendritic colloids are about 5% w/w to 20% of the polysaccharide, and wherein the soft dendritic colloids are synthesized from chitosan to form nanofibrillated chitosan.

6 . The consumer product packaging film of claim 5 , wherein the polysaccharide is agarose.

7 . The consumer product packaging film according to claim 5 , wherein the consumer product packaging film is optically transparent.

8 . The consumer product packaging film according to claim 5 , wherein the consumer product packaging film has a water contact angle of about 85° to 95°, and wherein the polysaccharide is agarose.

9 . The consumer product packaging film according to claim 5 , wherein the consumer product packaging film is a food packaging film.

10 . The consumer product packaging film according to claim 5 , wherein the consumer product packaging film is selected from a cosmetics packaging film and a household products packaging film.

11 . The consumer product packaging film according to claim 5 , wherein the consumer product packaging film is environmentally benign.

12 . The consumer product packaging film according to claim 6 , wherein the nanofibrillated chitosan is about 15% w/w of the agarose, and wherein the film has a tensile strength of about 50 MPa.