IP Library Granted Patent US 12674173
Granted Patent B2
US 12674173 · App. 17/288,764 · Granted Jul 7, 2026

Organelle-selective gene delivery and expression in the chloroplast in planta using chitosan-complexed single-walled carbon nanotube carriers

Inventors: Michael Strano (Lexington, MA); Seonyeong Kwak (Cambridge, MA); Tedrick Salim Lew (Cambridge, MA)
Assignee: MASSACHUSETTS INSTITUTE OF TECHNOLOGY
C12N15/8206
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Quick Facts
Patent No.
US 12674173
App. No.
17/288,764
Filed
Apr 26, 2021
Granted
Jul 7, 2026
Kind
B2
Art Unit
1663
USPC
800/293
Abstract

In one aspect, a composition can include an organelle, and a nanoparticle having a zeta potential of less than −10 mV or greater than 10 mV contained within the organelle. In a preferred embodiment, the organelle can be a chloroplast and the nanoparticle can be a single-walled carbon nanotube associated with a strongly anionic or strongly cationic polymer.

Claims (110)

1 . A composition, comprising:

a chitosan-complexed single-walled carbon nanotube complexed with a gene cassette for delivery to a chloroplast, wherein the chitosan-complexed single-walled carbon nanotube comprises chitosan is covalently bonded to the single-walled carbon nanotube;

wherein the gene cassette comprises plasmid DNA;

wherein the gene cassette and the chitosan-complexed single-walled carbon nanotube are present in a ratio of 1:3 to 1:10 w/w of gene cassette to chitosan-complexed single-walled carbon nanotube; and

wherein the chitosan-complexed single-walled carbon nanotube complexed with the gene cassette has a zeta potential in the range of −35 to −30 mV or in the range of 30 to 35 mV.

2 . The composition of claim 1 , wherein the chitosan is deacetylated.

3 . The composition of claim 1 , wherein the polysaccharide chitosan is pegylated.

4 . The composition of claim 1 , wherein the gene cassette includes a zinc finger nuclease, a TALEN vector or a CRISPR/Cas vector.

5 . A method of delivering genetic material to a plant chloroplast comprising:

contacting a plant with the composition of claim 1 .

6 . The method of claim 5 , wherein the plant is a watercress plant, a tobacco plant, a spinach plant or isolated Arabidopsis thaliana mesophyll protoplast.

7 . The method of claim 5 , further comprising releasing the genetic material in the interior of a chloroplast.

8 . The composition of claim 1 , wherein a threshold zeta potential is determined by Equation 1 :

ξ

*

=

±

(

ε

M

+

ε

W

ε

W

)

(

d

a

)

e

κ

(

d

-

a

)

(

Γ

-

a

γ

0

+

4

a

Δ

Δ

H

ρ

n

)

L

2

a

ε

0

ε

M

(

1

-

ε

M

ε

W

)

(

Equation

1

)

wherein:

ε M , a relative permittivity of a double lipid bilayers of the chloroplast, is about 2.2;

ε W , a relative permittivity of a medium of the chloroplast, is about 80;

ε 0 , a dielectric permittivity of vacuum, is about 8.854×10 −12 F/m;

“d” is an effective charge radius of the composition;

“a” is a radius of the composition;

κ −1 is a Debye-Huckle screening length of the composition;

Γ, a pore line tension of the chloroplast, is about 10 −12 N;

γ 0 , a resting membrane tension of the chloroplast, is about 0.6 mN/m;

ΔΔH, a change in free energy due to the lipid of the chloroplast binding on the composition, is about 0.05 k b T;

ρ n , a lipid density on the composition, is about 10 18 ; and

L, a thickness of the double lipid bilayers of the chloroplast, is about 1.1×10 −10 m,

wherein the radius of the composition is in the range of 104-190 nm.

9 . The composition of claim 1 , wherein the zeta potential is about −30 m V or about 30 m V.

10 . The composition of claim 1 , wherein the gene cassette and the chitosan-complexed single-walled carbon nanotube are present in a ratio of 1:3 to 1:6 w/w of gene cassette to chitosan-complexed single-walled carbon nanotube.

11 . A composition, comprising:

a chitosan-complexed single-walled carbon nanotube complexed with a gene cassette for delivery to a chloroplast in a plant,

wherein the chitosan-complexed single-walled carbon nanotube comprises chitosan is covalently bonded to the single-walled carbon nanotube;

wherein the gene cassette comprises plasmid DNA;

wherein the gene cassette and the chitosan-complexed single-walled carbon nanotube are present in a ratio of 1:3 to 1:10 w/w of gene cassette to chitosan-complexed single-walled carbon nanotube; and

wherein the chitosan-complexed single-walled carbon nanotube complexed with the gene cassette has a zeta potential in the range of −35 to −30 mV or in the range of 30 to 35 mV; and

wherein the plant is a watercress plant, a tobacco plant, a spinach plant or isolated Arabidopsis thaliana mesophyll protoplast.

12 . The composition of claim 1 , wherein the chloroplast is in a plant, and the composition is in contact with the plant.

13 . The composition of claim 11 , wherein the composition is in contact with the plant.