IP Library Granted Patent US 12678770
Granted Patent B2
US 12678770 · App. 18/985,220 · Granted Jul 14, 2026

Super absorbent polymer

Inventors: Soo Young Kwak (Daejeon, KR); Kwang In Shin (Daejeon, KR); Kyung Su Kim (Daejeon, KR)
Assignee: LG Chem, Ltd.
B01J20/267B01J20/28016B01J2220/68
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Quick Facts
Patent No.
US 12678770
App. No.
18/985,220
Granted
Jul 14, 2026
Kind
B2
Abstract

A polyacrylic acid (salt)-based super absorbent polymer may be analyzed by a time-domain nuclear magnetic resonance spectroscopy (TD-NMR) analysis. The results of the TD-NMR analysis may satisfy Equation 1. In Equation 1, N t=0.1 is a normalized intensity measured at a signal acquisition time of 0.1 ms. 2.5 ( % ) ≤ N t = 0.1 ( % ) ≤ 3.5 ( % ) [ Equation ⁢ 1 ]

Claims (104)

1 . A polyacrylic acid (salt)-based super absorbent polymer,

wherein a TD-NMR analysis result satisfies Equation 1, and

wherein the polyacrylic acid (salt)-based super absorbent polymer has an average convexity value of 0.93 or less and 0.87 or more for all particles, calculated using Equation 2:

2.5

(

%

)

N

t

=

0.1

(

%

)

3

.

5

(

%

)

[

Equation

1

]

M

c

=

L

s

/

L

[

Equation

2

]

wherein in Equation 1 and Equation 2,

N t=0.1 is a normalized intensity measured at a signal acquisition time of 0.1 ms,

M c is convexity,

L s is a length of a perimeter of a polygon of minimal perimeter that surrounds a two-dimensional (2D) image of a three-dimensional (3D) particle to be measured, and

L is an actual perimeter length of the 2D image of the 3D particle to be measured.

2 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein the polyacrylic acid (salt)-based super absorbent polymer has an extractable component content of 10 wt % or less based on a total weight of the polyacrylic acid (salt)-based super absorbent polymer, measured after free swelling in water having an electrical conductivity of 100 to 130 μS/cm for 30 minutes.

3 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein the polyacrylic acid (salt)-based super absorbent polymer has an extractable component content of 17 wt % or less based on a total weight of the polyacrylic acid (salt)-based super absorbent polymer, measured after free swelling in water having an electrical conductivity of 100 to 130 μS/cm for 3 hours.

4 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein the polyacrylic acid (salt)-based super absorbent polymer has an absorbency under pressure (AUP) of 28 g/g or more, measured under 0.3 psi according to EDANA method WSP 242.3.

5 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein the polyacrylic acid (salt)-based super absorbent polymer has a centrifuge retention capacity (CRC) of 33 g/g or more, measured according to EDANA method WSP 241.3.

6 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein the polyacrylic acid (salt)-based super absorbent polymer has an effective absorption capacity (EFFC) of 30 g/g or more, calculated by the Equation 3:

EFFC

=

(

C

R

C

+

A

UP

)

/

2

[

Equation

3

]

wherein in Equation 3,

CRC is a centrifuge retention capacity (units: g/g) measured according to EDANA method WSP 241.3, and

AUP is an absorbency under pressure (units: g/g) measured under 0.3 psi according to EDANA method WSP 242.3.

7 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein the polyacrylic acid (salt)-based super absorbent polymer has an absorption rate (vortex time) of 40 seconds or less measured by a vortex measurement method at 24.0° C.

8 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein when the polyacrylic acid (salt)-based super absorbent polymer is swelled in water having an electrical conductivity of 100 to 130 μS/cm for 1 minute, a maximum capacity of water that the polyacrylic acid (salt)-based super absorbent polymer is able to hold (free swelling capacity) is 170 g/g or more.

9 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein the polyacrylic acid (salt)-based super absorbent polymer has a liquid permeability of 65 ml or more, calculated by Equation 4:

Perm

=

[

20

mL

/

T

1

(

sec

)

]

×

60

sec

[

Equation

4

]

wherein in Equation 4,

Perm is liquid permeability, and

T1 is a time (seconds) taken for 20 mL of saline to pass through the polyacrylic acid (salt)-based super absorbent polymer under a pressure of 0.3 psi after placing 0.2 g of the polyacrylic acid (salt)-based super absorbent polymer in a cylinder, pouring saline (0.9 wt % sodium chloride aqueous solution) so that the polyacrylic acid (salt)-based super absorbent polymer is completely submerged, and allowing the polyacrylic acid (salt)-based super absorbent polymer to swell for 30 minutes.

10 . The polyacrylic acid (salt)-based super absorbent polymer of claim 1 , wherein the polyacrylic acid (salt)-based super absorbent polymer comprises pores of 100 μm or less.