IP Library Granted Patent US 12678840
Granted Patent B2
US 12678840 · App. 18/924,563 · Granted Jul 14, 2026

Waste plastic density separation

Inventors: Bruce Roger DeBruin (Gray, TN); Kyle Lyn Collings (Jonesborough, TN); James Stewart Nelson (Kingsport, TN)
Assignee: Eastman Chemical Company
B09B3/32B09B3/35B09B3/70B29B17/02B29B2017/0203B29B2017/0231B29B2017/0244
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Quick Facts
Patent No.
US 12678840
App. No.
18/924,563
Filed
Oct 23, 2024
Granted
Jul 14, 2026
Kind
B2
Art Unit
3655
USPC
209/1
Abstract

Methods and systems for separating mixed plastic waste are provided herein. The methods generally comprise separating the mixed plastic waste into a PET-enriched stream and one or more PET-depleted streams. The separating may be accomplished using the combinations of two or more density separation stages. Exemplary density separation stages include sink-float separators and centrifugal force separators. The PET-enriched and PET-depleted streams may be recovered and/or directed to downstream chemical recycling processes.

Claims (28)

1 . A waste plastic separation method comprising separating a mixed plastic waste (MPW) into a polyethylene terephthalate (PET)-enriched stream and a PET-depleted stream, wherein said PET-enriched stream comprises at least 70 weight percent PET on a dry basis and at least 0 . 1 weight percent and not more than 10 weight percent halogens on a dry basis, wherein the PET-enriched stream has a microorganism content of less than 10 5 CFU/g.

2 . The method of claim 1 , wherein said PET-enriched stream is also enriched in PVC and said PET-depleted stream is also depleted in PVC.

3 . The method of claim 1 , wherein said PET-enriched stream comprises not more than 2 weight percent of adhesives on a dry basis, and/or wherein said PET-enriched stream comprises not more than 4 weight percent plastic fillers and additives on a dry basis.

4 . The method of claim 1 , wherein PVC is not separated from said MPW or said PET-enriched stream as a PVC-enriched stream relative to said MPW or said PET-enriched stream.

5 . The method of claim 1 , wherein at least 50 weight percent of the PVC content in said MPW is separated from said MPW together with the PET into said PET-enriched stream.

6 . The method of claim 1 , wherein the PVC content in said PET-enriched stream is not separated from said PET-enriched stream prior to processing the PET in said PET-enriched stream in a chemical recycling process.

7 . A waste plastic separation method comprising:

(a) introducing mixed waste plastic (MPW) particulates into a first density separation stage; and

(b) feeding an output stream from said first density separation stage into a second density separation stage,

wherein one of said first and second density separation stages is a low-density separation stage and the other of said first and second density separation stages is a high-density separation stage,

wherein said low-density separation stage has a target separation density that is less than 1.35 g/cc and at least 1.25 g/cc,

wherein said high-density separation stage has a target separation density that is at least 0.01 g/cc greater than the target separation density of said low-density separation stage and that is at least 1.31 g/cc.

8 . The method of claim 7 , wherein the target separation density of said high-density separation stage is at least 1.33 g/cc and not more than 1.45 g/cc.

9 . The method of claim 7 , wherein said MPW particulates comprise PET and polyolefins in combination in an amount of at least 50 weight percent.

10 . The method of claim 7 , wherein said first density separation stage has a separation efficiency with respect to PET of at least 90 percent, and/or wherein said second density separation stage has a separation efficiency with respect to PET of at least 90 percent.

11 . The method of claim 7 , wherein said first density separation stage is a high-density sink-float density separation stage, and wherein said second density separation stages is a low-density centrifugal density separation stage.

12 . The method of claim 7 , wherein said first density separation stage is said high-density separation stage and said second density separation stage is said low-density separation stage.

13 . A waste plastic separation method comprising:

(a) feeding a stream of a caustic solution into at least one of a first or second density separation stages;

(b) introducing mixed waste plastic (MPW) particulates into said first density separation stage; and

(c) feeding an output stream from said first density separation stage into the second density separation stage,

wherein one of said first and second density separation stages is a low-density separation stage and the other of said first and second density separation stages is a high-density separation stage,

wherein no separate caustic component is introduced into said first density separation stage and/or said second density separation stage as a unit operation separate from said stream of caustic solution in step (a), and wherein said MPW particulates are not subjected to a separate antimicrobial processing stage, comprising addition of a caustic component, before being introduced into said first density separation stage.

14 . The method of claim 13 , wherein said caustic solution has a pH of greater than 8.

15 . The method of claim 13 , wherein said first density separation stage is a high-density sink-float separation stage, and wherein said second density separation stage is a low-density centrifugal density separation stage.

16 . The method of claim 13 , wherein said caustic solution is fed into said first density separation stage.

17 . The method of claim 13 , wherein said caustic solution comprises sodium hydroxide and/or potassium hydroxide.

18 . The method of claim 13 , wherein said caustic solution comprises potassium hydroxide.