IP Library Granted Patent US 12,679,737
Granted Patent B1
US 12,679,737 · App. 19/543,792 · Granted Jul 14, 2026

System and method for generating metal oxide borate from a boron solution

Inventors: Kirk M. Pumphrey (Silverton, OR); James L. Guidry (Campti, LA)
Assignee: Westwind Farms Inc.
C01B35/127C02F1/463C02F11/121C01P2004/16C01P2004/64C02F2101/108
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Quick Facts
Patent No.
US 12,679,737
App. No.
19/543,792
Granted
Jul 14, 2026
Kind
B1
Abstract

In a method for extracting boron from a boron solution, a boron solution is processed at an electrocoagulation system utilizing metal electrodes to generate a sludge comprising water, metal oxide and boric oxide, wherein the boric oxide is encapsulated within the metal oxide. The sludge is filtered at a dewatering system to remove at least a portion of the water from the sludge to generate a cake. The cake is processed at a furnace to generate metal oxide borate.

Claims (28)

1 . A method for generating metal oxide borate from a boron solution, the method comprising:

processing a boron solution at an electrocoagulation system utilizing metal electrodes to generate a sludge comprising water, metal oxide and boric oxide, wherein the boric oxide is encapsulated within the metal oxide;

filtering the sludge at a dewatering system to remove at least a portion of the water from the sludge to generate a cake; and

processing the cake at a furnace to generate metal oxide borate.

2 . The method of claim 1 , further comprising:

concentrating the boron solution at a condenser system prior to processing the boron solution at the electrocoagulation system.

3 . The method of claim 2 , wherein the condenser system comprises an evaporation tank operating at ambient temperature.

4 . The method of claim 1 , wherein the dewatering system comprises a filter.

5 . The method of claim 1 , wherein the processing the boron solution at the electrocoagulation system comprises:

generating metal hydroxide and boric acid from the boron solution; and

generating the water, the metal oxide and the boric oxide from the metal hydroxide and the boric acid.

6 . The method of claim 1 , wherein the water is returned to the boron solution for further processing.

7 . The method of claim 1 , wherein the water is conveyed to an irrigation system.

8 . The method of claim 1 , wherein the furnace is a sintering furnace.

9 . The method of claim 1 , wherein the processing the cake at a furnace to generate the metal oxide borate comprises:

heating the cake to at least 100 degrees Centigrade to remove additional water from the cake.

10 . The method of claim 1 , wherein the processing the cake at a furnace to generate the metal oxide borate comprises:

heating the cake to 600 to 1400 degrees Centigrade to morphologically transform the cake into metal oxide borate nanorods.

11 . The method of claim 10 , wherein the metal oxide borate nanorods have a width of 10 to 20 nanometers and a length of 70 to 120 nanometers.

12 . The method of claim 1 , wherein the metal electrodes are selected from a group of metals consisting of: aluminum, iron, magnesium, and manganese.

13 . A method for generating metal oxide borate nanorods from a boron solution, the method comprising:

processing a boron solution at an electrocoagulation system utilizing sacrificial metal electrodes to generate a sludge comprising water, metal oxide and boric oxide, wherein the boric oxide is encapsulated within the metal oxide; wherein the processing the boron solution at the electrocoagulation system comprises:

generating metal hydroxide and boric acid from the boron solution; and

generating the water, the metal oxide and the boric oxide from the metal hydroxide and the boric acid;

filtering the sludge at a dewatering system to remove at least a portion of the water from the sludge to generate a cake; and

processing the cake at a furnace to generate metal oxide borate, wherein the processing the cake at a furnace to generate the metal oxide borate comprises:

heating the cake to at least 100 degrees Centigrade to remove additional water from the cake; and

heating the cake to 600 to 1400 degrees Centigrade to morphologically transform the cake into metal oxide borate nanorods.