IP Library Granted Patent US 12679821
Granted Patent B2
US 12679821 · App. 17/630,859 · Granted Jul 14, 2026

Cyclic azine compound, material for organic light emitting diode, electron transport material for organic light emitting diode, and organic light emitting diode

Inventors: Naoki Uchida (Ayase, JP); Hidenori Aihara (Ayase, JP); Takuya Yamagata (Ayase, JP); Naoki Hayakawa (Ayase, JP); Natsumi Nakajima (Ayase, JP); Kazuki Hattori (Ayase, JP); Fuminari Uehara (Ayase, JP); Yohei Ono (Ayase, JP); Masaya Hirano (Ayase, JP); Yuta Morinaka (Ayase, JP); Keisuke Nomura (Ayase, JP); Eriko Ohta (Ayase, JP); Tomohiro Shono (Shunan, JP); Kana Oike (Ayase, JP); Kazushi Hayashi (Ayase, JP); Keiya Aoyagi (Ayase, JP); Kosuke Sato (Ayase, JP); Toshiki Nishiura (Ayase, JP)
Assignees: TOSOH CORPORATION; SAGAMI CHEMICAL RESEARCH INSTITUTE
C07D401/10C07C255/46C07D209/86C07D251/24C07D307/91C07D401/14C07D487/14C07F5/027C07F7/081H10K50/166H10K85/611H10K85/652H10K85/654H10K85/6572H10K85/6574
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Quick Facts
Patent No.
US 12679821
App. No.
17/630,859
Granted
Jul 14, 2026
Kind
B2
Abstract

An object of the present invention is to provide a cyclic azine compound exhibiting both excellent driving voltage characteristics and excellent current efficiency characteristics. The desired cyclic azine compound has a specific structure represented by formula (1).

Claims (35)

1 . A cyclic azine compound of formula (1):

wherein

Ar 1 is a phenyl group or a 4-biphenylyl group;

Ar 2 has one of formulas (2-1) to (2-3):

Ar 3 has one of formulas (3-2), (3-3), (3-5), (3-6), (3-7) and (3-9);

2 . The cyclic azine compound according to claim 1 , wherein

Ar 2 has one of formulas (2-1), (2-2a), (2-2b), (2-3a), and (2-3b)

3 . The cyclic azine compound according to claim 1 , wherein Ar 2 has formula (2-2b)

4 . The cyclic azine compound according to claim 1 , which has one of formulas (1-6), (1-15), (1-48), (1-51), (1-52), (1-54), (1-65), and (1-66):

5 . An organic light emitting diode, comprising:

an electron transport material comprising the cyclic azine compound of claim 1 .

6 . An organic light emitting diode, comprising:

an electron transport material comprising the cyclic azine compound of claim 2 .

7 . An organic light emitting diode, comprising:

an electron transport material comprising the cyclic azine compound of claim 3 .

8 . A method for producing a cyclic azine compound of formula (1), comprising:

reacting a compound of formula (4) with a compound of formula (3),

wherein

Ar 1 is a phenyl group or a 4-biphenylyl group;

Ar 2 has one of formulas (2-1) to (2-3):

 and

Ar 3 has one of formulas (3-2), (3-3), (3-5), (3-6), (3-7), and (3-9):

X 4 is a leaving group; and

Y 4 is a halogen atom, a metal-containing group, or a boron-containing group.

9 . A pyridine compound of formula (5):

wherein

Art has one of formulas (2-1) to (2-3):

Ar 3 has one of formulas (3-2), (3-3), (3-5), (3-6), (3-7) and (3-9):

Y 4 is a halogen atom, a metal-containing group, or a boron-containing group.

10 . The pyridine compound according to claim 9 , which has one of formulas (5-1), (5-2) or (5-3)

wherein

in formula (5-1), Ar 31 is selected from the group consisting of unsubstituted phenyl, unsubstituted 2-biphenylyl, and unsubstituted 4-biphenylyl,

in formula (5-2), Ar 31 is unsubstituted phenyl,

in formula (5-3), Ar 31 is unsubstituted phenyl, and

Y 4 and Ar 2 are as defined in claim 9 .