IP Library Granted Patent US 12680192
Granted Patent B2
US 12680192 · App. 18/457,324 · Granted Jul 14, 2026

Nanocomposite-seeded epitaxial growth of single-domain lithium niobate thin films for surface acoustic wave devices

Inventors: Haiyan Wang (West Lafayette, IN); Robynn-Lynne Paldi (Albuquerque, NM); Aleem Siddiqui (Albuquerque, NM)
Assignee: Purdue Research Foundation
C30B29/30C30B25/06C30B25/18
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Quick Facts
Patent No.
US 12680192
App. No.
18/457,324
Granted
Jul 14, 2026
Kind
B2
Abstract

A method for making LNO film, including the steps of identifying a substrate, identifying a deposition target, placing the substrate and deposition target in a deposition environment, evolving target material into the deposition environment, and depositing evolved target material onto the substrate to yield an LNO film. The deposition environment defines a temperature of between 500 degrees Celsius and 750 degrees Celsius and a pressure of about 10 −6 Torr. A seed or buffer layer may be first deposited onto the substrate, wherein the seed layer is about 30 mole percent gold and about 70 LiNbO 3 .

Claims (32)

1 . A LNO film, comprising:

a single crystal-like LNO film;

a substrate; and

a seed layer between the substrate and the single crystal-like LNO film;

wherein the single crystal-like LNO film has a single domain;

wherein the single crystal-like LNO film is between 100 nm and 5 μm thick; and

wherein the single crystal-like LNO film is at least 80 cm 2 in area;

wherein the seed layer is 70 mole percent LiNbO 3 and 30 mole percent metal;

wherein the metal is selected from the group consisting of Au, Ag, Ni, Co, Cu, and combinations thereof.

2 . The LNO film of claim 1 wherein the substrate is a c-cut Al 2 O 3 substrate.

3 . The LNO film of claim 2 wherein the seed layer is between 10 nm and 50 nm thick.

4 . The LNO film of claim 2 wherein the seed layer is between 10 nm and 30 nm thick.

5 . The LNO film of claim 1 wherein the single crystal-like LNO film is free of twinning.

6 . The LNO film of claim 1 wherein the single crystal-like LNO film is between 100 nm and 150 nm thick.

7 . A LNO film, comprising:

a single domain LNO film;

a substrate; and

a seed layer between the substrate and the single domain LNO film;

wherein the seed layer is 70 mole percent LiNbO 3 and 30 mole percent Au;

wherein the seed layer is between 10 nm and 50 nm thick.

8 . The LNO film of claim 7 , wherein the single domain LNO film is untwinned.

9 . The LNO film of claim 7 , wherein the substrate is one of c-plane Al 2 O 3 , LiTaO 3 , LTO, LNO, and SiO.

10 . The LNO film of claim 7 , wherein the seed layer is between 10 nm and 30 nm thick.

11 . The LNO film of claim 7 , wherein the single domain LNO film is at least 80 cm 2 in area.

12 . The LNO film of claim 7 , wherein the LNO film has three-fold symmetry.

13 . A LNO film, comprising:

a single crystal-like LNO film;

a substrate; and

a seed layer between the substrate and the single crystal-like LNO film;

wherein the single crystal-like LNO film has a single domain;

wherein the single crystal-like LNO film is between 100 nm and 5 μm thick;

wherein the seed layer comprises LiNbO 3 and a metal selected from the group consisting of Au, Ag, Ni, Co, Cu, and combinations thereof.