IP Library Granted Patent US 12686054
Granted Patent B2
US 12686054 · App. 18/246,784 · Granted Jul 21, 2026

Device and method for producing metal powders

Inventors: Sébastien Doublet (Jouy-en-Josas, FR); Eric Verna (Jouy-en-Josas, FR); Olivier Debellemaniere (Jouy-en-Josas, FR)
Assignee: L'Air Liquide Socíété Anonyme pour l'Etude et l'Exploitation des Procédés George Claude
B22F9/082B05B7/224B22F1/065B22F1/145B22F2009/0844B22F2009/0848B22F2009/0876B22F2009/0896B22F2998/10
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Quick Facts
Patent No.
US 12686054
App. No.
18/246,784
Granted
Jul 21, 2026
Kind
B2
Abstract

A method of manufacturing powder from a first and a second materials for use in additive manufacturing, the manufacturing process including melting the first and second materials by an electric arc; spraying the melted materials so as to form droplets; cooling the droplets by a carrier gas so as to form solid particles; separating the solid particles from the carrier gas and collecting the solid particles so as to form the powder; and enriching the droplets and/or the particles by means of an active substance.

Claims (26)

1 . A method for manufacturing powder from a first material and a second material, the manufacturing method comprising:

a step of melting the first and second materials, by an electric arc, to form first and second molten materials;

a step of spraying the first and second molten materials with a carrier gas so as to form droplets;

a step of cooling the droplets by the carrier gas and a cooling gas so as to form solid particles with a particle size distribution between 5 μm and 150 μm;

a step of enriching the droplets and/or the particles by an active substance, implemented during the cooling step, the enrichment step being preceded by a step of ionising the active substance; and

a step of separating the solid particles from the carrier gas and collecting the solid particles so as to form the powder,

wherein the carrier gas and the cooling gas present a volume flow ratio of 2 to 1.

2 . The manufacturing method according to claim 1 , wherein the active substance comprises:

at least one neutral gas; and

at least one active compound comprising at least one of the following atoms:

oxygen, nitrogen, carbon or hydrogen;

each active compound being in the gas, liquid or solid phase, the content of each active compound being between 5 ppm and 20,000 ppm.

3 . The manufacturing method according to claim 1 , wherein the enrichment step is implemented during the spraying and cooling steps.

4 . The manufacturing method according to claim 1 , wherein the cooling gas is injected at a temperature below 50° C.

5 . The manufacturing method according to claim 1 , wherein, in addition to the carrier gas, the cooling step is performed by a gas buffer.

6 . The manufacturing method according to claim 5 , wherein the temperature of the gas buffer is kept below 400° C.

7 . The manufacturing method according to claim 5 , wherein the gas buffer comprises a gas, the gas being argon.

8 . The manufacturing method according to claim 7 , wherein the speed of the gas within the gas buffer is less than 1 m/s.

9 . The manufacturing method according to claim 5 , wherein the manufacturing method is performed in sequences and wherein the sequences are spaced apart by times of cooling the gas buffer.

10 . The manufacturing method according to claim 1 , wherein the steps of the method are implemented by a manufacturing device, said method comprising a step of inerting the manufacturing device by a neutral gas, for purging the manufacturing device, the melting step being triggered subsequently to the inerting step.

11 . The manufacturing method according to claim 1 , wherein the collection step is followed by a step of passivating the particles.

12 . The manufacturing method according to claim 11 , wherein the passivation step is triggered when the maximum temperature of the powder is below a threshold temperature.

13 . The manufacturing method according to claim 11 , wherein the passivation step is triggered after a set waiting time.

14 . The manufacturing method according to claim 11 , wherein the duration of the passivation step is controlled as a function of the temperature of the powder.

15 . The manufacturing method according to claim 11 , wherein the duration of the passivation step is set.

16 . The manufacturing method according to claim 1 , wherein the particle size distribution of the solid particles is between 10 μm and 63 μm.