Single crystal pulling apparatus and method for pulling single crystal
The present invention is a single crystal pulling apparatus which includes a pulling furnace having a central axis and a magnetic field generating apparatus having coils, and applies a horizontal magnetic field to a molten semiconductor raw material, wherein the coils are saddle-shaped, two pairs of the coils are provided with the coils of each pair arranged facing each other, two coil axes in the two pairs of coils are included in the same horizontal plane, when a magnetic force line direction on the central axis of the pulling furnace in the horizontal plane is defined as a X-axis, and a direction perpendicular to the X-axis in the horizontal plane is defined as a Y-axis, a center angle α between the two coil axes sandwiching the X-axis is 90 degrees or less and an inter-coil angle β between adjacent superconducting coils sandwiching the Y-axis is 20 degrees or less. As a result, the coil height can be reduced by increasing the magnetic field generation efficiency, the magnetic field center can be raised to near the melt surface of the semiconductor raw material, and it is possible to provide a single crystal pulling apparatus and a single crystal pulling method capable of pulling a single crystal with an even lower oxygen concentration than before and a defect-free crystal at a higher speed can be obtained.
1 . A single crystal pulling apparatus comprising: a pulling furnace in which a heating heater and a crucible containing a molten semiconductor raw material are arranged and has a central axis; and a magnetic field generating apparatus provided around the pulling furnace and having superconducting coils, for applying a horizontal magnetic field to the molten semiconductor raw material by energizing the superconducting coils to suppress convection of the molten semiconductor raw material in the crucible,
wherein the superconducting coils of the magnetic field generating apparatus are saddle-shaped and are curved along an outer shape of the pulling furnace, the saddle-shaped superconducting coils having a vertical width shorter than a horizontal width, and two pairs of the saddle-shaped superconducting coils are arranged around the pulling furnace with the saddle-shaped superconducting coils of each pair arranged facing each other,
when an axis passing through the centers of a pair of superconducting coils arranged facing each other is defined as a coil axis,
two coil axes of the two pairs of superconducting coils are included in the same horizontal plane, and
when a magnetic force line direction on the central axis of the pulling furnace in the horizontal plane is defined as a X-axis, and a direction perpendicular to the X-axis in the horizontal plane is defined as a Y-axis, a center angle α between the two coil axes sandwiching the X-axis is 90 degrees or less and an inter-coil angle β between adjacent superconducting coils sandwiching the Y-axis is 20 degrees or less.
2 . The single crystal pulling apparatus according to claim 1 , wherein the magnetic field generating apparatus comprises an elevating device capable of moving up and down in a vertical direction.
3 . The single crystal pulling apparatus according to claim 2 , wherein the saddle-shaped superconducting coils have a vertical width shorter than a horizontal width.
4 . A method for pulling a single crystal, comprising pulling a semiconductor single crystal using the single crystal pulling apparatus according to claim 1 .
5 . A method for pulling a single crystal, comprising pulling a semiconductor single crystal using the single crystal pulling apparatus according to claim 2 .
6 . A method for pulling a single crystal, comprising pulling a semiconductor single crystal using the single crystal pulling apparatus according to claim 3 .
7 . The method for pulling a single crystal according to claim 4 , wherein when the semiconductor single crystal is pulled, a height position of the magnetic field generating apparatus is adjusted according to a target value of oxygen concentration contained in the semiconductor single crystal.
8 . The method for pulling a single crystal according to claim 5 , wherein when the semiconductor single crystal is pulled, a height position of the magnetic field generating apparatus is adjusted according to a target value of oxygen concentration contained in the semiconductor single crystal.
9 . The method for pulling a single crystal according to claim 6 , wherein when the semiconductor single crystal is pulled, a height position of the magnetic field generating apparatus is adjusted according to a target value of oxygen concentration contained in the semiconductor single crystal.
10 . The method of pulling a single crystal according to claim 4 , wherein, when the semiconductor single crystal is pulled, a magnetic field strength is adjusted according to a target defect region of the semiconductor single crystal.
11 . The method of pulling a single crystal according to claim 5 , wherein, when the semiconductor single crystal is pulled, a magnetic field strength is adjusted according to a target defect region of the semiconductor single crystal.
12 . The method of pulling a single crystal according to claim 6 , wherein, when the semiconductor single crystal is pulled, a magnetic field strength is adjusted according to a target defect region of the semiconductor single crystal.
13 . The method of pulling a single crystal according to claim 7 , wherein, when the semiconductor single crystal is pulled, a magnetic field strength is adjusted according to a target defect region of the semiconductor single crystal.
14 . The method of pulling a single crystal according to claim 8 , wherein, when the semiconductor single crystal is pulled, a magnetic field strength is adjusted according to a target defect region of the semiconductor single crystal.
15 . The method of pulling a single crystal according to claim 9 , wherein, when the semiconductor single crystal is pulled, a magnetic field strength is adjusted according to a target defect region of the semiconductor single crystal.