IP Library Granted Patent US 12687529
Granted Patent B2
US 12687529 · App. 18/259,211 · Granted Jul 21, 2026

Method and system for mass spectrometry signal quality assessment

Inventors: Gordana Ivosev (Condord, CA); Chang Liu (Richmond Hill, CA)
Assignee: DH Technologies Development Pte. Ltd.
G01N30/8624B01D15/08G01N30/72
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Quick Facts
Patent No.
US 12687529
App. No.
18/259,211
Granted
Jul 21, 2026
Kind
B2
Abstract

Methods and systems for a signal quality assessment for mass spectrometry are provided. The system includes a processor that utilizes a wavelet-based feature extraction for the signal quality assessment of a chromatogram signal. The signal quality assessment is used to control operational parameters such as a flowrate of a pump that moves liquid droplets toward an ionization device of a mass spectrometer.

Claims (41)

1 . A system, wherein the system comprises:

a mass analyzer operable to generate a multidimensional signal, wherein the multidimensional signal comprises a plurality of outputs; and

a processor, wherein the processor is operable to:

generate a multidimensional wavelet scale-space response of the multidimensional signal,

generate an ideal wavelet scale-space response of an ideal signal,

generate a signal quality metric according to the multidimensional wavelet scale-space response,

compare the signal quality metric to an expected value generated from the ideal wavelet scale-space response, and

according to the comparison of the signal quality metric to the expected value, iteratively:

adjust an operational parameter of the mass analyzer,

regenerate a multidimensional wavelet scale-space response of the multidimensional signal,

regenerate the ideal wavelet scale-space response of an ideal signal,

regenerate the signal quality metric according to the regenerated multidimensional wavelet scale-space response, and

compare the signal quality metric to an expected value generated from the regenerated ideal wavelet scale-space response.

2 . The system of claim 1 , wherein the wavelet scale-space response comprises a wavelet response over time for each of two or more scales.

3 . The system of claim 1 , wherein the signal quality metric is generated according to a region of interest.

4 . The system of claim 3 , wherein the region of interest comprises a local maxima of the multidimensional signal.

5 . The system of claim 1 , wherein the multidimensional signal is a chromatogram signal.

6 . The system of claim 1 , wherein the processor is operable to generate the signal quality metric according to a quality feature extraction from a wavelet scale-space response over a region of interest, and wherein the wavelet scale-space response comprises at least one scale.

7 . The system of claim 1 , wherein the processor is operable to generate the signal quality metric by combining two or more features of the multidimensional signal.

8 . The system of claim 1 , wherein the processor is operable to generate the signal quality metric according to a number of local maxima in a region of interest.

9 . The system of claim 1 , wherein the processor is operable to generate the signal quality metric by determining a wavelet scale-space response of the multidimensional signal, and wherein the wavelet scale-space response comprises a first number of local maxima at a first scale and a second number of local maxima at a second scale.

10 . A method, wherein the method comprises:

generating a multidimensional signal via a mass analyzer, wherein the multidimensional signal comprises a plurality of outputs;

generating a multidimensional wavelet scale-space response of the multidimensional signal;

generating an ideal wavelet scale-space response of an ideal signal;

generating a signal quality metric according to the multidimensional wavelet scale-space response;

comparing the signal quality metric to an expected value generated from the ideal wavelet scale-space response; and

according to the comparison of the signal quality metric to the expected value, iteratively:

adjusting an operational parameter of the mass analyzer,

regenerating a multidimensional wavelet scale-space response of the multidimensional signal,

regenerating the ideal wavelet scale-space response of an ideal signal,

regenerating the signal quality metric according to the regenerated multidimensional wavelet scale-space response, and

comparing the signal quality metric to an expected value generated from the regenerated ideal wavelet-scale space response.

11 . The method of claim 10 , wherein the wavelet scale-space response comprises a wavelet response over time for each of two or more scales.

12 . The method of claim 10 , wherein the signal quality metric is generated according to a region of interest.

13 . The method of claim 12 , wherein the region of interest comprises a local maxima of the multidimensional signal.

14 . The method of claim 10 , wherein the multidimensional signal is a chromatogram signal.

15 . The method of claim 10 , wherein generating the signal quality metric comprises extracting a quality feature from a wavelet scale-space response over a region of interest, and wherein the wavelet scale-space response comprises at least one scale.

16 . The method of claim 10 , wherein generating the signal quality metric comprises combining two or more features of the multidimensional signal.

17 . The method of claim 10 , wherein generating the signal quality metric is according to a number of local maxima in a region of interest.

18 . The method of claim 10 , wherein generating the signal quality metric comprises determining a wavelet scale-space response of the multidimensional signal, and wherein the wavelet scale-space response comprises a first number of local maxima at a first scale and a second number of local maxima at a second scale.