IP Library Granted Patent US 12692474
Granted Patent B2
US 12692474 · App. 16/492,293 · Granted Jul 28, 2026

Microgel particles for use in 3D printing and 3D cell growth medium and related compositions, systems, and methods

Inventors: Wallace Gregory Sawyer (Gainesville, FL); Sangwoo Park (Gainesville, FL); Christopher S. O'Bryan (Philadelphia, PA); Christopher P. Kabb (Gainesville, FL); Brent S. Sumerlin (Gainesville, FL); Thomas Ettor Angelini (Gainesville, FL)
Assignee: University of Florida Research Foundation, Inc.
C12N5/0062B01J13/00B33Y70/00C08F2/38C08F220/26C08L33/26C12P21/00C08J9/16C12N5/0676
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Quick Facts
Patent No.
US 12692474
App. No.
16/492,293
Granted
Jul 28, 2026
Kind
B2
Abstract

Microgel particles for use in a three-dimensional cell growth medium are described. The microgel particles may be swellable and may have properties conducive to improved function and health of cells distributed within the three-dimensional cell growth medium. Related compositions, systems, and methods are also described. Also provided is a plurality of microgel particles and a liquid cell culture medium, wherein the microgel particles are swelled with the liquid cell culture medium to form a granular gel. Also provided is a method of preparing a three-dimensional cell growth medium is disclosed. The method may comprise: mixing a plurality of microgel particles, such as those described above, in a liquid cell culture medium. Also provided is a method of placing cells in a three-dimensional cell growth medium is disclosed. Also provided is a method of synthesizing a protein is disclosed.

Claims (13)

1 . A three-dimensional cell growth medium, the three-dimensional cell growth medium consisting of:

a plurality of microgel particles, wherein each of the plurality of microgel particles consists of a crosslinked polymeric network, and wherein the crosslinked polymeric network consists of:

low charge density polymer molecules, wherein each of the low charge density polymer molecules consists of a first set of neutral monomer units derived from acrylamide and a second set of charged monomer units derived from methacrylic acid, wherein an average spacing between the charged monomer units is greater than the Bjerrum length; and

a crosslinker;

wherein a molar ratio of the first monomer to the crosslinker present in the solution is between 20:1 and 200:1; and

a liquid cell culture medium, wherein the plurality of microgel particles swell with the liquid cell culture medium to form a three-dimensional granular gel; and

wherein the three-dimensional cell growth medium is a yield stress material.

2 . The three-dimensional cell growth medium of claim 1 , wherein the charged groups are negatively charged groups.

3 . The three-dimensional cell growth medium of claim 1 , wherein less than 60% of the sum of the first and second sets of monomer units are second monomer units.

4 . The three-dimensional cell growth medium of claim 1 , wherein less than 20% of the sum of the first and second sets of monomer units are second monomer units.

5 . The three-dimensional cell growth medium of claim 1 , wherein the crosslinker has an average molecular weight of between 250 g/mol and 10,000 g/mol.

6 . The three-dimensional cell growth medium of claim 1 , wherein the crosslinker is selected from poly(ethylene glycol) diacrylate (PEGDA) or N,N′-methylenebisacrylamide (MBA).

7 . The three-dimensional cell growth medium of claim 1 , wherein the crosslinker is hydrophilic.