IP Library Granted Patent US 12696676
Granted Patent B2
US 12696676 · App. 18/199,513 · Granted Jul 28, 2026

Electrical planarization of carbon nanotube thin films for electronic device applications

Inventors: Andrew Gabriel Rinzler (Gainesville, FL); Rajib Kumar Das (Gainesville, FL); Bo Liu (Gainesville, FL); Max G. Lemaitre (Gainesville, FL)
Assignees: UNIVERSITY OF FLORIDA RESEARCH FOUNDATION, INC.; MATTRIX TECHNOLOGIES, INC.
H10K71/18B82Y40/00H10K71/60
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Quick Facts
Patent No.
US 12696676
App. No.
18/199,513
Granted
Jul 28, 2026
Kind
B2
Abstract

Various examples are provided related to electrical planarization of carbon nanotube thin films or networks. In one example, a method includes depositing one or more thin protective organic and/or inorganic layer across a nanotube film; disrupting electrical conductance of portions of the nanotube film by exposure of out-of-plane nanotubes to a planarization process that disrupts the electrical conductance through the one or more thin protective organic and/or inorganic layer; and removing the one or more thin protective organic and/or inorganic layer from the nanotube film.

Claims (31)

1 . A method for electrical planarization of nanotube films or networks, comprising:

depositing one or more thin protective organic and/or inorganic layer across a nanotube film;

disrupting electrical conductance of portions of the nanotube film by exposure of out-of-plane nanotubes to a planarization process that disrupts the electrical conductance through the one or more thin protective organic and/or inorganic layer; and

removing the one or more thin protective organic and/or inorganic layer from the nanotube film.

2 . The method of claim 1 , wherein the nanotube film is disposed on a substrate surface, the nanotube film having an average nanotube film thickness, and the electrical conductance of out-of-plane nanotubes that protrude more than 10 times the average nanotube film thickness above the substrate surface is disrupted.

3 . The method of claim 1 , wherein the nanotube film comprises single wall carbon nanotubes.

4 . The method of claim 1 , wherein the nanotube film is disposed on a substrate in electrical contact with one or more contact pad or contact electrode.

5 . The method of claim 4 , wherein the substate is a glass substrate.

6 . The method of claim 4 , wherein at least one of the one or more contact pad or contact electrode is connected to a current supply line.

7 . The method of claim 1 , wherein at least a portion of the out-of-plane nanotubes is formed over a particle.

8 . The method of claim 1 , wherein the one or more thin protective organic and/or inorganic layer is deposited over the nanotube film.

9 . The method of claim 8 , wherein the one or more thin protective organic and/or inorganic layer comprises PMMA (polymethyl methacrylate).

10 . The method of claim 8 , wherein the one or more thin protective organic and/or inorganic layer has a thickness in a range from about 50 nm to about 300 nm.

11 . The method of claim 10 , wherein the one or more thin protective organic and/or inorganic layer has a thickness in a range from about 70 nm to about 200 nm.

12 . The method of claim 1 , wherein the planarization process comprises exposure of the out-of-plane nanotubes to oxidation through the one or more thin protective organic and/or inorganic layer.

13 . The method of claim 12 , where the out-of-plane nanotubes are exposed to an electrolyte for electrochemical oxidation.

14 . The method of claim 13 , wherein the electrolyte comprises a KOH electrolyte.

15 . The method of claim 12 , where the out-of-plane nanotubes are exposed to an oxygen plasma asher for oxidation.

16 . The method of claim 12 , where the out-of-plane nanotubes are exposed to ultraviolet (UV)/ozone for oxidation.

17 . The method of claim 12 where the out-of-plane nanotubes are exposed to chemicals that disrupt the nanotube conductance by esterification/amidation, halogenation, cycloaddition, radical, nucleophilic or electrophilic addition.

18 . The method of claim 1 , further comprising:

forming a layer of semiconducting channel material on top of the nanotube film; and

forming one or more electrodes on top of the layer of semiconducting channel material.

19 . The method of claim 18 , wherein the layer of semiconducting channel material comprises an organic semiconductor.

20 . The method of claim 18 , wherein the one or more electrodes comprises a drain electrode.

21 . The method of claim 18 , wherein OLED layers are deposited on top of the level of semiconducting channel material followed by deposition of an electron injecting drain electrode.

22 . The method of claim 1 , further comprising:

forming a layer of dielectric material on top of the nanotube film; and

forming one or more electrodes on top of the layer of dielectric material to provide a top gate electrode.

23 . The method of claim 1 , further comprising:

forming a layer of dielectric material on top of the nanotube film to isolate the nanotube film from subsequently deposited layers.