Structured filter material for nicotine delivery products
A filter material is described for manufacturing a nicotine delivery product, wherein the filter material is hydroentangled and contains at least 50% and at most 100% cellulose fibers, each with respect to the mass of the filter material, wherein the filter material has a basis weight of at least 25 g/m 2 and at most 60 g/m 2 , and wherein the filter material has a structure that is characterized in that it provides the filter material with a transparency that, measured in accordance with DIN 53147:1993-01, is at least 45% and at most 70%. Furthermore, a segment comprising a filter material for a nicotine delivery product, a smoking article which comprises such a segment, an oral nicotine delivery product, and a process for the manufacture of the filter material are described.
1 . A filter material for manufacturing a nicotine delivery product, wherein the filter material is hydroentangled and contains at least 50% and at most 100% cellulose fibers, each with respect to the mass of the filter material, wherein the filter material has a basis weight of at least 25 g/m 2 and at most 60 g/m 2 , and wherein the filter material has a structure that is characterized in that it provides the filter material with a transparency which, measured in accordance with DIN 53147:1993-01, is at least 45% and at most 70%.
2 . The filter material according to claim 1 , in which the proportion of cellulose fibers in the filter material is at least 70% and at most 95%, each with respect to the mass of the filter material.
3 . The filter material according to claim 1 , in which the cellulose fibers are formed by pulp fibers, fibers from regenerated cellulose or mixtures thereof.
4 . The filter material according to claim 3 , in which the proportion of fibers produced from regenerated cellulose is at least 15% and at most 40% with respect to the mass of the filter material.
5 . The filter material according to claim 1 , the basis weight of which, in accordance with ISO 536:2012 is at least 28 g/m 2 and at most 55 g/m 2 .
6 . The filter material according to claim 1 , the transparency of which, measured in accordance with DIN 53147:1993-01 is at least 50% and at most 66%.
7 . The filter material according to claim 1 , in which said structure comprises a plurality of holes in the filter material, wherein at least 90% of the holes have an area of less than 10 mm 2 .
8 . The filter material according to claim 1 , which further contains one or more additional components selected from the group consisting of alkyl ketene dimers (AKD), alkenyl succinic acid anhydrides (ASA), fatty acids, starch, starch derivatives, carboxy methyl cellulose, alginates, wet strength agents, organic or inorganic acids or bases, or burn additives selected from the group consisting of citrates, malates, tartrates, acetates, nitrates, succinates, fumarates, gluconates, glycolates, lactates, oxalates, salicylates, α-hydroxy caprylates, phosphates, polyphosphates, chlorides and hydrogen carbonates, and mixtures thereof.
9 . The filter material according to claim 1 , which further contains one or more substances selected from the group consisting of triacetin, propylene glycol, sorbitol, glycerol, polyethylene glycol, polypropylene glycol, polyvinyl alcohol and triethyl citrate.
10 . The filter material according to claim 1 , the thickness of which, measured in accordance with ISO 534:2011 is at least 70 μm and at most 1000 μm.
11 . The filter material according to claim 1 , the tensile strength with respect to width of which, measured in accordance with ISO 1924-2:2008 in at least one direction, is at least 0.05 kN/m and at most 5 kN/m.
12 . The filter material according to claim 1 , the elongation at break of which, measured in accordance with ISO 1924-2:2008 in at least one direction, is at least 3% and at most 40%.
13 . A segment for a nicotine delivery product, wherein the nicotine delivery product is a smoking article, comprising a filter material according to claim 1 and a wrapping material, which wraps the filter material.
14 . The segment according to claim 13 , wherein the segment is in the shape of a cylinder with a circular base area, wherein the circular base area has a diameter of at least 5 mm and at most 8 mm.
15 . The segment according to claim 13 , which has a length of at least 4 mm and at most 40 mm.
16 . The segment according to claim 13 , the draw resistance per length of the segment of which, measured in accordance with ISO 6565:2015, is at least 1 mmWG/mm and at most 12 mmWG/mm.
17 . The segment according to claim 13 , in which the wrapping material is a paper or a film.
18 . The segment according to claim 13 , in which the wrapping material has a basis weight of at least 20 g/m 2 and at most 150 g/m 2 .
19 . A smoking article, comprising a segment, which contains an aerosol-forming material, and a segment according to claim 13 .
20 . The smoking article according to claim 19 , in which the segment according to claim 13 is a segment located next to the mouth end of the smoking article.
21 . The smoking article according to claim 19 , in which the smoking article is a filter cigarette and the aerosol-forming material is tobacco.
22 . The smoking article according to claim 19 , during the intended use of which the aerosol-forming material is only heated but not burned, and the aerosol-forming material comprises tobacco, reconstituted tobacco, nicotine, glycerol, propylene glycol or mixtures of two or more of these components.
23 . The smoking article according to claim 19 , in which the wrapping material of said segment according to claim 13 is at least partially transparent or has holes and the filter material has a transparency, measured in accordance with DIN 53147:1993-01, of at least 50%.
24 . An oral nicotine delivery product comprising a pouch which is formed by a filter material according to claim 1 and contains a nicotine-containing material, wherein the filter material has said transparency, measured in accordance with DIN 53147:1993-01, of at least 50% and at most 70%.
25 . A process for the manufacture of a filter material, which comprises the steps A to D:
A—providing a fiber web comprising cellulose fibers,
B—hydroentangling the fiber web by at least one water jet directed onto the fiber web in order to manufacture a hydroentangled fiber web,
C—generating a structure in the hydroentangled fiber web,
D—drying the hydroentangled fiber web,
wherein the amount of cellulose fibers in step A is selected such that after drying in step D, the filter material contains at least 50% and at most 100% cellulose fibers with respect to the mass of the filter material, and
after drying in step D, the filter material has a basis weight of at least 25 g/m 2 and at most 60 g/m 2 , and
wherein after drying in step D, said structure is characterized in that it provides the filter material with a transparency, measured in accordance with DIN 53147:1993-01, of at least 45% and at most 70%, and
the generation of a structure in step C is carried out by directing at least one water jet onto the fiber web while the fiber web is supported by a surface that has a plurality of prominences.
26 . The process according to claim 25 , wherein step A comprises the steps A1 to A4:
A1—manufacturing an aqueous suspension comprising cellulose fibers,
A2—applying the suspension from step A to a running wire,
A3—de-watering the suspension through the running wire in order to form a fiber web, and
A4—transferring the fiber web from step A3 to a support wire.
27 . The process according to claim 26 , in which the aqueous suspension in step A1 has a solid content of at most 0.2%.
28 . The process according to claim 25 , in which a plurality of water jets is used in order to carry out the hydroentangling in step B, wherein the water jets are arranged in at least one row transverse to the running direction of the fiber web.
29 . The process according to claim 25 , in which the hydroentangling in step B is carried out by at least two water jets directed onto the fiber web, wherein the at least two water jets act from different sides of the fiber web.
30 . The process according to claim 25 , in which the fiber web in step C is supported by a cylinder, on the surface of which a plurality of prominences is located.
31 . The process according to claim 25 , in which the area of each prominence, projected onto the surface that supports the fiber web in step C, is at least 0.1 mm 2 and at most 15 mm 2 .
32 . The process according to claim 25 , in which the drying in step D is at least partially carried out by contact with hot air, by infra-red radiation or by microwave radiation.
33 . The process according to claim 25 , in which after drying in step D, the filter material is a filter material used for manufacturing a nicotine delivery product according to claim 1 .