IP Library Granted Patent US 12698224
Granted Patent B2
US 12698224 · App. 18/983,121 · Granted Aug 4, 2026

Synthesis of nanophotocatalyst for sewage water treatment

Inventors: Manal Ahmed Awad (Riyadh, SA); Hanan Fahad AlHarbi (Riyadh, SA); Khalid Mustafa Ortashi (Riyadh, SA); Latifah Abdullrahman AlHumaid (Riyadh, SA); Abdullah Anwar Ibrahim (Riyadh, SA)
Assignee: KING SAUD UNIVERSITY
C02F1/725B01J23/06B01J35/39B01J37/009B01J37/038B01J37/082C02F1/32B01J2235/15B01J2235/30B82Y30/00B82Y40/00C02F2101/308C02F2305/10
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Quick Facts
Patent No.
US 12698224
App. No.
18/983,121
Granted
Aug 4, 2026
Kind
B2
Abstract

A method of synthesizing a ZnO nano-photocatalyst is provided, including providing an aqueous extract comprising pigeon droppings, filtering the aqueous extract to produce a filtrate, precipitating a solution of zinc nitrate with the filtrate to obtain a paste, and calcining the paste to obtain ZnO nanoparticles, wherein the ZnO nanoparticles are suitable for use as a nano-photocatalyst in sewage water treatment applications.

Claims (28)

1 . A method of producing a ZnO nano-photocatalyst comprising:

providing an aqueous extract comprising pigeon droppings;

filtering the aqueous extract to produce a filtrate;

mixing zinc nitrate with the filtrate to obtain a paste; and

calcining the paste to produce the ZnO nano-photocatalyst.

2 . The method of claim 1 , wherein the filtering comprises:

filtering the aqueous extract through gauze to produce a first filtrate; and

filtering the first filtrate through filter paper to produce a second filtrate.

3 . The method of claim 1 , comprising:

suspending about 20 g of pigeon droppings in about 100 mL of water to provide the pigeon droppings aqueous extract.

4 . The method of claim 1 , comprising mixing about 2 g of the zinc nitrate with about 100 mL of the filtrate to obtain the paste; wherein the zinc nitrate comprises zinc nitrate hexahydrate.

5 . The method of claim 4 , comprising mixing the zinc nitrate hexahydrate and the filtrate under constant stirring at about 60° C.

6 . The method of claim 1 , comprising calcining the paste in a muffle furnace at about 400° C. for about 4 hours to produce the ZnO nano-photocatalyst.

7 . A method of treating sewage, comprising:

providing an aqueous extract comprising pigeon droppings;

filtering the aqueous extract to produce a filtrate;

mixing zinc nitrate with the filtrate to obtain a paste;

calcining the paste to obtain a ZnO nano-photocatalyst; and

applying the ZnO nano-photocatalyst to the sewage;

wherein the ZnO nano-photocatalyst catalyzes degradation of at least one organic compound in the sewage.

8 . The method of treating sewage of claim 7 , wherein the filtering comprises:

filtering the aqueous extract through gauze to produce a first filtrate; and

filtering the first filtrate through filter paper to produce a second filtrate.

9 . The method of treating sewage of claim 7 , comprising:

suspending about 20 g of pigeon droppings in about 100 mL of water to provide the pigeon droppings aqueous extract.

10 . The method of treating sewage of claim 7 , comprising mixing about 2 g of the zinc nitrate with about 100 mL of the filtrate to obtain the paste; wherein the zinc nitrate comprises zinc nitrate hexahydrate.

11 . The method of treating sewage of claim 10 , comprising mixing the zinc nitrate hexahydrate and the filtrate under constant stirring at about 60° C.

12 . The method of treating sewage of claim 7 , comprising calcining the paste in a muffle furnace at about 400° C. for about 4 hours to obtain the ZnO nano-photocatalyst.