IP Library Granted Patent US 12703798
Granted Patent B2
US 12703798 · App. 18/145,142 · Granted Aug 11, 2026

Compositions for manufacturing thin film and methods for manufacturing semiconductor device using the same

Inventors: Jae Woon Kim (Seoul, KR); Seung-Min Ryu (Hwaseong-si, KR); Haruyoshi Sato (Tokyo, JP); Kazuya Saito (Tokyo, JP); Masayuki Kimura (Tokyo, JP); Takahiro Yoshii (Tokyo, JP); Tsubasa Shiratori (Tokyo, JP); Min Jae Sung (Seoul, KR); Gyu-Hee Park (Hwaseong-si, KR); Youn Joung Cho (Hwaseong-si, KR)
Assignees: Samsung Electronics Co., Ltd.; Adeka Corporation
C09D1/00C07F3/003H10B12/033
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Quick Facts
Patent No.
US 12703798
App. No.
18/145,142
Granted
Aug 11, 2026
Kind
B2
Abstract

Compositions for manufacturing a thin film are provided. The compositions may include a compound having a structure of Chemical Formula 1: M may be strontium (Sr) or barium (Ba), X 1 and X 2 may each independently be oxygen (O) or a substituted or unsubstituted alkylamino group having 1 to 5 carbon atoms, R 1 and R 2 may each independently be a substituted or unsubstituted alkyl group having 1 to 5 carbon atoms or a substituted or unsubstituted perfluoro alkyl group having 1 to 5 carbon atoms, R 3 may be hydrogen or a substituted or unsubstituted alkyl group having 1 to 5 carbon atoms, L may be a substituted or unsubstituted polyether having 1 to 6 oxygen atoms, or a substituted or unsubstituted polyamine having 1 to 6 nitrogen atoms, or a substituted or unsubstituted polyetheramine having 1 to 6 oxygen atoms or nitrogen atoms, and n may be an integer of 1 to 6.

Claims (37)

1 . A composition for manufacturing a thin film, the composition comprising a compound having a structure of Chemical Formula 1:

wherein M is strontium (Sr) or barium (Ba),

X 1 and X 2 are each independently oxygen (O) or a substituted or unsubstituted alkylamino group having 1 to 5 carbon atoms,

R 1 and R 2 are each independently a perfluoro alkyl group having 1 to 5 carbon atoms,

wherein R 1 and R 2 are different from each other,

R 3 is hydrogen or a substituted or unsubstituted alkyl group having 1 to 5 carbon atoms,

L is a substituted or unsubstituted polyether having 1 to 6 oxygen atoms, a substituted or unsubstituted polyamine having 1 to 6 nitrogen atoms, or a substituted or unsubstituted polyetheramine having 1 to 6 oxygen atoms and 1 to 6 nitrogen atoms, and

n is an integer of 1 to 6.

2 . The composition according to claim 1 , wherein L has a structure of Chemical Formula 2:

wherein R 6 and R 7 are each independently a methyl group, an ethyl group, an n-propyl group, an isopropyl group, an n-butyl group, a tert-butyl group, a sec-butyl group, or a substituted or unsubstituted perfluoroalkyl group having 1 to 4 carbon atoms, and

wherein X is an integer of 1 to 5.

3 . The composition according to claim 2 , wherein L includes at least one of diglyme and tetraethylene glycol dimethyl ether (tetraglyme).

4 . The composition according to claim 1 , wherein L includes at least one of TMEDA (tetramethlyethlyenediamine) and HMTETA (hexamethyltriethylenetriamine).

5 . The composition according to claim 1 , wherein X 1 and X 2 are the same.

6 . The composition according to claim 1 , wherein X 1 and X 2 are different from each other.

7 . The composition according to claim 1 , wherein the compound having the structure of Chemical Formula 1 is in a liquid state at room temperature.

8 . The composition according to claim 1 , wherein a melting point of the compound having the structure of Chemical Formula 1 is 60° C. or lower.

9 . A method for manufacturing a semiconductor device, the method comprising:

providing a substrate including an active region;

forming a lower electrode on the substrate so as to be connected to the active region; and

forming a capacitor dielectric film disposed along a profile of the lower electrode,

wherein forming the capacitor dielectric film includes sequentially providing a composition for manufacturing a thin film, and a metal,

wherein the composition for manufacturing the thin film includes a compound having a structure of Chemical Formula 1:

wherein M is strontium (Sr) or barium (Ba),

X 1 and X 2 are each independently oxygen (O) or a substituted or unsubstituted alkylamino group having 1 to 5 carbon atoms,

R 1 and R 2 are each independently a perfluoro alkyl group having 1 to 5 carbon atoms, wherein R 1 and R 2 are different from each other,

R 3 is hydrogen or a substituted or unsubstituted alkyl group having 1 to 5 carbon atoms,

L is a substituted or unsubstituted polyether having 1 to 6 oxygen atoms, a substituted or unsubstituted polyamine having 1 to 6 nitrogen atoms, or a substituted or unsubstituted polyetheramine having 1 to 6 oxygen atoms and 1 to 6 nitrogen atoms, and

n is an integer of 1 to 6.

10 . The method according to claim 9 , wherein the capacitor dielectric film includes at least one of SrTiO 3 , BaTiO 3 , or SrBaTi 2 O 6 .

11 . The method according to claim 9 , wherein the compound having the structure of Chemical Formula 1 is in a liquid state at room temperature.

12 . The method according to claim 9 , wherein L has a structure of Chemical Formula 2:

wherein R 6 and R 7 are each independently a methyl group, an ethyl group, an n-propyl group, an isopropyl group, an n-butyl group, a tert-butyl group, a sec-butyl group, or a substituted or unsubstituted perfluoroalkyl group having 1 to 4 carbon atoms, and

wherein X is an integer of 1 to 5.

13 . The method according to claim 9 , wherein L includes at least one of diglyme and tetraethylene glycol dimethyl ether (tetraglyme).

14 . The method according to claim 9 , wherein L includes at least one of TMEDA (tetramethlyethlyenediamine) and HMTETA (hexamethyltriethylenetriamine).

15 . The method according to claim 9 , wherein X 1 and X 2 are the same.