IP Library Granted Patent US 12709571
Granted Patent B2
US 12709571 · App. 18/283,871 · Granted Aug 18, 2026

Production of activated-belite-CSA clinkers at extremely low firing temperature

Inventors: Tristana Duvallet (Lexington, KY); Thomas Lee Robl (Sadieville, KY); Robert B. Jewell (Lexington, KY); Anne Elizabeth Oberlink (Lexington, KY)
Assignee: University of Kentucky Research Foundation
C04B7/3453C04B7/424C04B28/025
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Quick Facts
Patent No.
US 12709571
App. No.
18/283,871
Granted
Aug 18, 2026
Kind
B2
Abstract

A raw meal for a cement clinker, a cement clinker made from that raw meal and a process for producing a cement clinker are provided. The clinker contains mainly the hydraulically activate alpha′H-belite polymorph and calcium sulfoaluminate (ye'elimite or C 4 A 3 Ś), at the low firing temperature of 1050° C., using a combination of fluoride and boron oxide.

Claims (30)

1 . A raw meal of a cement clinker, comprising:

about 45-57 weight percent calcium oxide;

about 15-25 weight percent silicon dioxide;

about 9-18 weight percent aluminum oxide;

about 0.5-5 weight percent iron oxide;

about 2-8 weight percent sulfur trioxide;

about 0.2-3 weight percent calcium fluoride;

about 0.2-4 weight percent sodium oxide; and

about 0.5-5 weight percent boron oxide wherein the raw meal is adapted to produce a cement clinker with no more than 2.4 weight percent tetracalcium aluminoferrite.

2 . The raw meal of claim 1 , further including at least one of limestone, hydrated lime, river sand, calcium sulfate, flue gas desulfurization gypsum, fly ash, bauxite, red mud, calcium fluoride, borax, boric acid, and sodium oxide.

3 . The raw meal of claim 1 incorporating fluoride and boron oxide.

4 . The raw meal of claim 3 wherein the fluoride is calcium fluoride and the boron oxide is borax.

5 . The raw meal of claim 4 , including about 48-54 weight percent calcium oxide.

6 . The raw meal of claim 5 , including about 18-22 weight percent silicon oxide.

7 . The raw meal of claim 6 , including about 12-15 weight percent aluminum oxide.

8 . The raw meal of claim 7 , including about 1.5-4 weight percent iron oxide.

9 . The raw meal of claim 8 , including about 4.5-5 weight percent sulfur trioxide.

10 . The raw meal of claim 9 , including about 1-1.5 weight percent calcium fluoride.

11 . The raw meal of claim 10 , including about 1-2 weight percent sodium oxide.

12 . The raw meal of claim 11 , including about 2-4 weight percent boron oxide.

13 . The raw meal of claim 1 including:

about 51-52 weight percent calcium oxide;

about 19.5-21 weight percent silicon dioxide;

about 13-14.5 weight percent aluminum oxide;

about 2-3 weight percent iron oxide;

about 4.5-5 weight percent sulfur trioxide;

about 1.1-1.4 weight percent calcium fluoride;

about 1.2-1.6 weight percent sodium oxide; and

about 2.5-3.5 weight percent boron oxide.

14 . A cement clinker made from the raw meal of claim 1 .