IP Library Granted Patent US 6,875,759
Granted Patent B1
US 6,875,759 · App. 09/625,196 · Granted Apr 5, 2005

Substituted guanidines and the use thereof

Assignee: Kadmus Pharmaceuticals
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Quick Facts
Patent No.
US 6,875,759
App. No.
09/625,196
Granted
Apr 5, 2005
Kind
B1
Abstract

A method for the treatment of cancer and pain in an animal subject is disclosed, comprising administering to said animal in need of such treatment an effective amount of a compound of formula I: wherein R 1 -R 6 are defined herein. Pharmaceutical compositions comprising one or more compounds of formula I and a pharmaceutically acceptable carrier are also disclosed.

Claims (17)

1. A compound of formula I:

wherein,

R 1 and R 2 are each independently selected from the group consisting of (a) hydrogen, halogen, hydroxy, cyano, amino, nitro, acylamido, thiol, azido, formyl, carboxy, carbonylamido and (b) aryl, fused aryl, carbocyclic, heterocyclic, heteroatyl, alkyl, alkenyl, alkynyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroarylalkynyl, carbocycloalkyl, heterocycloalkyl, acyloxy, alkoxy, alkylthiol, alkoxyalkyl and alkylthioalkyl, each of which is optionally substituted by one or more substituents independently selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido;

R 3 is

R 4 is selected from the group consisting of (a) hydrogen said (b) aryl, fused aryl, carbocyclic, heterocyclic, heteroaryl, alkyl, alkenyl, alkynyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroarylalkynyl, carbocycloalkyl, heterocycloalkyl, alkoxyalkyl and akylthioalkyl, COR, CO 2 R and CONR x R y , each of which is optionally substituted by one or more substituents selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido, wherein R, R x and R y , are independently selected from the group consisting of hydrogen, aryl, fused aryl, carbocyclic, heterocyclic, heteroaryl, alkyl alkenyl, alkynyl, alkoxyalkyl, alkylthioalkyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroalkynyl, carbocycloalkyl and heterocycloalkyl; or R x and R y are taken together to form a heterocycle, which is optionally substituted by one or more substituents independently selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido;

R 5 and R 6 are each zero to four substituents and are independently selected from the group consisting of (a) halogen, hydroxy, cyano, amino, nitro, acylamido, thiol, azido, formyl, carboxy, carbonylamido and (b) aryl, fused aryl, carbocyclic, heterocyclic, heteroaryl, alkyl, alkenyl, alkynyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroarylalkynyl, carbocycloalkyl, heterocycloalkyl, acyloxy, alkoxy, alkylthiol, alkoxyalkyl and alkylthioalkyl, each of which is optionally substituted by one or more substituents independently selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido;

R 7 is selected from the group consisting of (a) hydrogen and (b) aryl fused aryl, carbocyclic, heterocyclic, heteroaryl, alkyl, alkenyl, alkynyl, alkoxyalkyl, alkylthioalkyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroarylalkynyl, carbocycloalkyl, heterocycloalkyl, COR, CO 2 R and CONR X R Y , each of which is optionally substituted by one or more substituents independently selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido, wherein R, R x and R y , are independently selected from the group consisting of hydrogen, aryl, fused aryl, carbocyclic, heterocyclic, heteroaryl, alkyl, alkenyl, alkynyl, alkoxyalkyl, alkylthioalkyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroalkynyl, carbocycloalkyl and heterocycloalkyl; or R, and R Y are taken together to form a heterocycle, which is optionally substituted by one or more substituents independently selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido;

where R 1 , R 2 , R 4 , R 5 , R 6 and R 7 are defined above; and

R 10 is selected from the group consisting of (a) hydrogen and (b) aryl, fused aryl, carbocyclic, heterocyclic, heteroaryl, alkyl, alkenyl, alkynyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroarylalkynyl, carbocycloalkyl, heterocycloalkyl, alkoxyalkyl, alkylthioalkyl, COR, CO 2 R and CONR x R y , each of which is optionally substituted by one or more substituents independently selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido, wherein R, R X and R y are independently selected from the group consisting of hydrogen, aryl, fused aryl, carbocyclic, heterocyclic, heteroaryl, alkyl, alkenyl, alkynyl, alkoxyalkyl, alkylthioalkyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroalkynyl, carbocycloalkyl and heterocycloalkyl; or R x and R y are taken together to form a heterocycle, which is optionally substituted by one or more substituents independently selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido; or R 10 is

where R 1 , R 2 , R 4 , R 5 , R 6 and R 7 are defined above; k is 0 or 1 and X is a (C 1-6 )alkylene group, which is optionally substituted by one or more substituents independently selected from the group consisting of (a) halogen, hydroxy, cyano, amino, nitro, acylamido, thiol, azido, formyl, carboxy, carbonylamido and (b) aryl, fused aryl, carbocyclic, heterocyclic, heteroaryl, alkyl, alkenyl, alkynyl, arylalkyl, arylalkenyl, arylalkynyl, heteroarylalkyl, heteroarylalkenyl, heteroarylalkynyl, carbocycloalkyl heterocycloalkyl, acyloxy, alkoxy, alklythiol, alkoxyalkyl and alkylthioalkyl, each of which is optionally substituted by one or more substituents independently selected from the group consisting of halogen, hydroxy, cyano, methoxy, amino, nitro, acylamido, thiol, azido, formyl, carboxy and carbonylamido;

with the proviso that (a) when R 1 and R 2 are both methyl, R 3 is not cyclohexylamino, (b) when R 1 , R 2 , R 5 and R 6 comprise not more than three substitutents other than hydrogen, R 3 is not (C 1-6 )alkylamino, di(C 1-6 )alkylamino, unsubstituted piperazinyl or N—(C 1-6 )alkylpiperazinyl and (c) when Y is ethylene, at least one of the group consisting of R 1 , R 2 , R 4 , R 5 , R 6 and R 7 is other than hydrogen; or

the pharmaceutically acceptable salts or esters thereof.

2. The compound of claim 1 , wherein R 10 is hydrogen or optionally substituted alkyl.

3. The compound of claim 1 , wherein R 10 is optionally substituted alkenyl.

4. The compound of claim 1 , wherein R 10 is

5. A pharmaceutical composition comprising the compound of claim 1 and a pharmaceutically acceptable carrier.

6. The pharmaceutical composition of claim 5 , wherein the compound is 1-[(N,N′-di-p-tolyl)amidino]-4-(trans-1′-cinnamyl)piperizine.

Assignments (2)
SECURITY AGREEMENT Recorded Feb 12, 2007
From: KADMUS PHARMACEUTICALS, INC.
To: SANDERLING VENTURE PARTNERS IV, L.P.
Reel/Frame 018883/0018 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 21, 2000
From: LIPKOWSKI, ANDRZEJ; GEE, KELVIN
To: KADMUS PHARMACEUTICALS, INC.
Reel/Frame 010962/0101 →
Continuity (1)
Provisional Application 6014481000 · Jul 21, 1999