IP Library Granted Patent US 2,233
Granted Patent H1
US 2,233 · App. 09/633,664 · Granted Nov 3, 2009

Catalysts which stabilize hydrofluorocarbon blowing agents in polyurethane foam compositions

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Quick Facts
Patent No.
US 2,233
App. No.
09/633,664
Granted
Nov 3, 2009
Kind
H1
Abstract

A composition comprising a polyisocyanate, a polyol, a hydrofluorocarbon blowing agent, optionally water, a surfactant, and at least one catalyst for the reaction of the polyisocyanate with the polyol and/or the reaction of the polyisocyanate with water, the catalyst being selected from the group consisting of triethylenediamine; N-2-hydroxy-propyltriethylenediamine ammonium salt; N-cetyl-N,N-dimethylamine; N,N-diethylethanamine; N,N-dimethylaminoethylmorpholine; bis(3-dimethylaminopropyl)-N,N-dimethylpropanediamine; N-cyclohexyl-N-methylcyclohexylamine; 1,3,5-tris(3-(dimethylamino)propyl)hexahydro-s-triazine; bis(dimethylaminopropyl)methylamine; dibutyltin dilaurylmercaptide; dibutyltin diisooctylmaleate; dibutyltin bis(2-ethylhexylmercaptoacetate); stannous octoate, 1,2-dimethylimidizole, bis-(dimethylaminoethyl)ether; bis(3-dimethylaminopropyl)-N,N-dimethylpropanediamine and bis(N,N-dimethylaminoethyl)-ether and resulting in a decreased amount of decomposition of the hydrofluorocarbon blowing agent to fluoroalkene.

Claims (2)

1. A composition comprising a polyisocyanate, a polyol, a hydrofluorocarbon blowing agent, optionally water as an additional blowing agent, a surfactant, and at least one catalyst for the reaction of the polyisocyanate with the polyol and/or the reaction of the polyisocyanate with water, the catalyst being selected from the group consisting of triethylenediamine; N-2-hydroxypropyltriethylenediamine ammonium salt; N-cetyl-N,N-dimethylamine; N,N-diethyl-ethanamine; N,N-dimethylaminoethylmorpholine; bis(3-dimethylamino-propyl)-N,N-dimethylpropanediamine; N-cyclohexyl-N-methylcyclohexylamine; 1,3,5-tris(3-(dimethylamino)propyl)hexahydro-s-triazine; bis(dimethylaminopropyl)methylamine; dibutyltin dilaurylmercaptide; dibutyltin diisooctylmaleate; dibutyltin bis(2-ethylhexylmercaptoacetate); stannous octoate, 1,2-dimethylimidizole; bis-(dimethylaminoethyl)ether; bis(3-dimethylaminopropyl)-N,N-dimethylpropanediamine and bis(N,N-dimethylaminoethyl)ether and resulting in a decreased amount of decomposition of the hydrofluorocarbon blowing agent to fluoroalkene.

2. A process for preparing polyurethane foam which comprises reacting a polyol with a polyisocyanate in the presence of a hydrofluorocabon blowing agent, optionally water as an additional blowing agent, a surfactant, and at least one catalyst selected from the group consisting of trithylenediamine; N-2-hydroxypropyltriethylenediamine ammonium salt; N-cetyl-N,N-dimethylamine; N,N-diethyl-ethanamine; N,N-dimethylaminoethylmorpholine; bis(3-dimethylaminopropyl)-N,N-dimethylpropanediamine; N-cyclohexyl-N-methylcyclohexylamine; 1,3,5-tris(3-dimethylamino)popyl)-hexahydro-s-triazine; bis(dimethylamino-propyl)methylamine; dibutyltin dilauryl-mercaptide; dibutyltin diisooctylmaleate; dibutyltin bis(2-ethylhexylmercaptoacetate); stannous octoate, 1,2-dimethylimidizole, bis-(dimethylaminoethyl)ether; bis(3-dimethylaminorpopyl)-N,N-dimethylpropanediamine and bis(N,N-dimethylaminoethyl)ether, in which the catalyst results in a decreased amount of decomposition of the hydrofluorocarbon blowing agent to fluoroalkene.

Assignments (2)
CHANGE OF NAME Recorded Dec 16, 2019
From: EVONIK DEGUSSA GMBH
To: EVONIK OPERATIONS GMBH
Reel/Frame 051301/0646 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 14, 2017
From: AIR PRODUCTS AND CHEMICALS, INC.
To: EVONIK DEGUSSA GMBH
Reel/Frame 044432/0676 →