IP Library Granted Patent US 6,841,603
Granted Patent B1
US 6,841,603 · App. 09/714,469 · Granted Jan 11, 2005

Polymer blends containing polyhydroxyalkanoates and compositions with good retention of elongation

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Quick Facts
Patent No.
US 6,841,603
App. No.
09/714,469
Granted
Jan 11, 2005
Kind
B1
Abstract

Biodegradable polymer blend compositions are provided which contain oligomeric esters. The oligoester compound can compatibilize blends of two or more biodegradable polymers resulting in excellent ductility and reduced tendency to embrittlement of products produced from therefrom. In a preferred embodiment of the invention, the blend composition comprises a PHA, polycaprolactone (PCL) and one or more oligomeric esters. In another preferred embodiment of the invention, the blend composition comprises a PHA, polybutylenesuccinate-adipate (PBSUA), and one or more oligomeric esters.

Claims (27)

1. A polymer composition comprising poly-3-hydroxybutyrate-co-4hydroxybutyrate (P3HB4HB) blend and a nucleant with no plasticizer, wherein the percentage of 4hydroxybutyrate (4HB) in the P3HB41B is between 16% and 99%.

2. The composition of claim 1 wherein the nucleant is boron nitride.

3. The composition of claim 1 wherein the nucleant is present at levels between 0.1 and 20 wt % of the blend.

4. The composition of claim 1 wherein the nucleant is present at levels between 1 and 10 wt % of the blend.

5. A method of producing a shaped polymeric object comprising melting a composition comprising a poly-3hydroxybutyrate-co-4hydroxybutyrate (P3HB4HB) blend wherein the percentage of 4-hydroxybutyrate (4HB) in the P3HB4HB is between 16% and 99% and a nucleant with no plasticizer, and producing a shaped object therefrom by extrusion, molding, coating, spinning, blowing, thermoforming or calendaring processes or combinations of the processes.

6. The method of claim 5 , wherein the nucleant is boron nitride.

7. A shaped object made according to claim 5 .

8. A shaped object made according to claim 6 .

9. A polymer composition comprising a poly-3-hydroxybutyrate-co-hydroxybutyrate (P3HB 4HB) blend and a nucleant with no plasticizer, wherein the nucleant is present at a level of 0.1 wt % of the composition.

10. The composition of claim 9 wherein the nucleant is boron nitride.

11. A method of producing a shaped polymeric object comprising melting a composition comprising a poly-3-hydroxybutyrate-co-4-hydroxybutyrate (P3HB4HB) blend and a nucleant with no plasticizer, and producing a shad object therefrom by extrusion, molding, coating, spinning, blowing, thermoforming or calendaring processes or combinations of the processes, wherein the nucleant is present at a level of 0.1 wt % of the composition.

12. The method of claim 11 wherein the nucleant is boron nitride.

13. A shaped object made comprising the composition of claim 10 .

14. A shaped object made according to claim 11 .

15. A polymer composition comprising poly-3-hydroxybutyrate-co-4-hydroxybutyrate (P3HB4HB) blend and a nucleant with no plasticizer wherein the composition is capable of forming a film having elongation.

16. The composition of claim 15 wherein the elongation at break is in the range between 560% and 1100% as measured by tensile testing on molded bars (4 mm wide and 20 mm gauge length.

17. The composition of claim 15 , wherein the nucleant is present at a level between 0.1 and 20 wt % of the composition.

18. The composition of claim 15 wherein the nucleant is present at a level between 1 and 10% of the composition.

19. A method of producing a shaped polymeric object comprising melting a composition comprising a poly-3-hydroxybutyrate-co-4-hydroxybutyrate (P3HB4HB) blend and a nucleant with no plasticizer, and producing a shaped object therefrom by extrusion, molding, coating, spinning, blowing, thermoforming or calendaring processes or combinations of the processes, wherein the composition is capable of forming a film having elongation.

20. The method of claim 19 wherein the elongation at break is in the range between 560% and 1100 as measured by tensile testing on molded bars (4 mm wide and 20 mm gauge length).

21. The method of claim 19 , wherein the nucleant is present at a level between 0.1 and 20 wt % of the composition.

22. The method of claim 19 wherein the nucleant is present at a level of 1 to 10% of the composition.

23. The method of claim 20 wherein the nucleant is present at a level between 0.1 and 20 wt % of the composition.

24. The method of claim 20 , wherein the nucleant is present at a level of 1 to 10% of the composition.

25. The method of claim 19 wherein the nucleant is boron nitride.

26. A shaped article made according to the method of claim 19 .

27. A shaped article made according to the method of claim 20 .

Assignments (7)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded May 19, 2017
From: CJ RESEARCH CENTER LLC
To: CJ CHEILJEDANG CORPORATION
Reel/Frame 042522/0729 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 3, 2017
From: METABOLIX, INC.
To: CJ RESEARCH CENTER LLC
Reel/Frame 041234/0890 →
ADDRESS CHANGE Recorded May 2, 2016
From: METABOLIX, INC.
To: METABOLIX, INC.
Reel/Frame 038665/0359 →
RELEASE OF SECURITY INTEREST Recorded Nov 9, 2006
From: MONSANTO COMPANY
To: METABOLIX, INC.
Reel/Frame 018498/0719 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 7, 2006
From: ASRAR, JAWED; PIERRE, JEAN R.
To: MONSANTO COMPANY
Reel/Frame 017730/0568 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 30, 2004
From: MONSANTO COMPANY
To: METABOLIX, INC.
Reel/Frame 015051/0818 →
SECURITY INTEREST Recorded Jun 4, 2001
From: METABOLIX, INC.
To: MONSANTO COMPANY
Reel/Frame 012066/0562 →