IP Library Granted Patent US 6,923,631
Granted Patent B2
US 6,923,631 · App. 09/906,281 · Granted Aug 2, 2005

Apparatus for forming a resin impregnated flexible graphite sheet

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Quick Facts
Patent No.
US 6,923,631
App. No.
09/906,281
Granted
Aug 2, 2005
Kind
B2
Abstract

A flexible graphite sheet exhibiting enhanced isotropy is provided. In addition, an apparatus, system and method for continuously producing a resin-impregnated flexible graphite sheet is also provided.

Claims (17)

1. A system for the continuous production of surface patterned, resin-impregnated flexible graphite sheet which comprises:

(i) a reactor vessel for containing as reactants raw natural graphite particles in mixture with sulfuric and nitric acids;

(ii) an acid containing vessel communicating with said reactor vessel for the introduction of a mixture of sulfuric and nitric acid into said reactor vessel;

(iii) a graphite particle containing vessel for the introduction of graphite particles into the reactor vessel;

(iv) a first additive containing vessel communicating with said reactor vessel for the introduction of intercalation enhancing materials, acids or organic chemicals;

(v) a wash vessel containing water communicating with the reactor vessel to receive reaction product in the form of acid intercalated graphite particles and remove acid from the surface of the acid intercalated graphite particles and a portion of the mineral impurities contained in the natural graphite particles introduced into the reactor vessel;

(vi) a drying chamber for drying washed acid intercalated graphite particles;

(vii) conduit means extending from said wash vessel to said drying chamber for passing washed acid intercalated graphite particles from the wash vessel to the drying chamber;

(viii) an expansion chamber enclosing an open flame at a temperature of at least about 700° C.;

(ix) conduit means extending from said collecting vessel to said expansion chamber for passing dried acid intercalated graphite particles to said expansion chamber;

(x) gas inlet means communicating with the conduit means of (viii) for entraining the acid intercalated graphite particles in a stream of non-reactive gas and passing the entrained acid intercalated graphite particles into the open flame enclosed in said expansion chamber to cause expansion of the acid intercalated graphite particles to form vermiform elongated graphite particles;

(xi) a collecting hopper for receiving said vermiform elongated graphite particles;

(xii) a compression chamber positioned to receive vermiform graphite particles for compressing said vermiform particles into a coherent self-supporting mat of flexible graphite;

(xiii) an impregnation chamber for contacting the flexible graphite mat of (xviii) with resin and impregnating said flexible graphite with resin;

(xiv) a calender mill disposed to receive the flexible graphite mat for increasing the density of said flexible graphite mat to form a continuous flexible graphite sheet;

(xv) a device for mechanically deforming a surface of the continuous flexible graphite sheet of (xiv) to provide a series of repeating patterns on said surface flexible graphite sheet or the removal of material from said flexible graphite sheet in a series of repeating patterns; and

(xvi) an oven for receiving the mat from the dryer of (xv) to cure the resin.

Assignments (7)
RELEASE OF SECURITY INTEREST Recorded Feb 1, 2023
From: WELLS FARGO BANK, NATIONAL ASSOCIATION
To: NEOGRAF SOLUTIONS, LLC
Reel/Frame 062972/0634 →
SECURITY AGREEMENT Recorded Sep 13, 2017
From: NEOGRAF SOLUTIONS, LLC
To: WELLS FARGO BANK, NATIONAL ASSOCIATION
Reel/Frame 043843/0582 →
CHANGE OF NAME Recorded Jul 26, 2017
From: ADVANCED ENERGY TECHNOLOGIES LLC
To: NEOGRAF SOLUTIONS, LLC
Reel/Frame 043336/0472 →
RELEASE OF SECURITY INTERESTS RECORDED AT REEL/FRAMES 013463/0360, 024678/0830, 014357/0075, AND 035839/0754 Recorded Jul 6, 2017
From: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT FKA MORGAN GUARANTY TRUST COMPANY OF NEW YORK
To: ADVANCED ENERGY TECHNOLOGIES LLC AS ASSIGNEE OF GRAFTECH INTERNATIONAL HOLDINGS INC. FKA ADVANCED ENERGY TECHNOLOGY INC. FKA GRAFTECH INC.
Reel/Frame 043099/0502 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 6, 2017
From: GRAFTECH INTERNATIONAL HOLDINGS INC.
To: ADVANCED ENERGY TECHNOLOGIES LLC
Reel/Frame 042922/0807 →
SECURITY AGREEMENT Recorded Jul 14, 2010
From: GRAFTECH INTERNATIONAL HOLDINGS INC.
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 024678/0830 →
CHANGE OF NAME Recorded Apr 18, 2002
From: UCAR GRAPH-TECH INC.
To: GRAFTECH INC.
Reel/Frame 012839/0331 →