Process for improving the internal stability of sodium percarbonate
View Patent ↗The invention relates to uncoated and/or coated sodium percarbonate with improved internal stability and storage stability; and, a process that provides uncoated and/or coated sodium percarbonate with improved internal stability and storage stability.
1. A process, consisting essentially of:
thermally treating coated or uncoated dry sodium percarbonate with continuously replacing ambient air for a time of at least 2 minutes at a temperature from 70° C. to 120° C.;
wherein the thermally treating does not result in a substantial reduction of the oxygen and moisture content of the dry sodium percarbonate.
2. The process according to claim 1 , wherein the temperature is from 85° C. to 95° C.
3. The process according to claim 1 , wherein the time is from 5 to 60 minutes.
4. The process according to claim 1 , wherein the time is from 10 to 60 minutes.
5. The process according to claim 1 , wherein the sodium percarbonate is in a fluidized layer,
atmospheric air is heated to a treatment temperature from 70° C. to 120° C.; and the atmospheric air is passed through the fluidized layer.
6. The process according to claim 5 , wherein the atmospheric air is heated by flue gases.
7. The process according to claim 5 , wherein the thermal treatment is performed in a fluidized bed.
8. The process according to claim 5 , wherein the atmospheric air is heated to a treatment temperature from 80° C. to 95° C.
9. The process according to claim 1 ,
wherein the sodium percarbonate is uncoated.
10. The process according to claim 1 , wherein the sodium percarbonate is coated and the coated sodium percarbonate is thermally treated immediately following a drying step subsequent to a coating process of sodium percarbonate.
11. The process according to claim 10 , wherein the temperature is from 85° C. to 95° C.
12. The process according to claim 10 , wherein said thermally treating of the sodium percarbonate occurs from 10 to 60 minutes.
13. The process according to claim 11 , wherein said thermally treating of the sodium percarbonate occurs from 10 to 60 minutes.