IP Library Granted Patent US 7,291,694
Granted Patent B1
US 7,291,694 · App. 10/049,549 · Granted Nov 6, 2007

Method and device for producing crystallizable plastic material

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Quick Facts
Patent No.
US 7,291,694
App. No.
10/049,549
Granted
Nov 6, 2007
Kind
B1
Abstract

A method for manufacturing a crystallizable plastic material is disclosed. The process includes the step of melting an amorphous plastic material, pelletizing the material, crystallizing it and then post condensing the plastic material with the proviso that the plastic material is not subjected to heating after the melting step but prior to the crystallization step and then subjecting the plastic material to sieving after the crystallization step.

Claims (24)

1. A process for manufacturing crystallizable polyester comprising:

(a) providing amorphous polyester from a melt reactor;

(b) pelletizing the polyester;

(c) crystallizing the polyester at a temperature of 140° C. to 180° C.; and

(d) post-condensing the polyester;

wherein the polyester is not subjected to heating after step (a) and prior to the crystallization step and the polyester is subjected to sieving after the crystallization step.

2. The process according to claim 1 wherein the polyester is polyethylene terephthalate.

3. A device for manufacturing crystallizable polyester for executing a process according to claim 1 , the device comprising a pelletizer, a fluidized bed ( 4 ) and a shaft reactor ( 7 ), wherein a sieve ( 5 ) is placed downstream from the fluidized bed ( 4 ).

4. The device according to claim 3 , wherein the polyester is polyethylene terephthalate.

5. A process for manufacturing crystallizable polyester comprising:

(a) providing amorphous polyester from a melt reactor;

(b) crystallizing the polyester at 140° C. to 180° C.;

(c) pelletizing the polyester; and

(d) post-condensing the polyester;

wherein the polyester is not warmed again after step (a) and prior to the crystallization step and the is subjected to sieving after the pelletization step at roughly the same temperature as during the crystallization step and the pelletization step.

6. The process according to claim 5 , wherein the temperature during the pelletization step and the sieving step is between 100° C. and 200° C.

7. The process according to claim 5 , wherein the temperature during the pelletization step and the sieving step is between 120° C. and 160° C.

8. The process according to claim 5 , wherein retention time during the crystallization step is approximately 1 to 40 seconds.

9. The process according to claim 5 , wherein retention time during the crystallization step is approximately 2 to 20 seconds.

10. The process according to claim 5 , wherein the sieving step is followed by a second crystallization step.

11. The process according to claim 5 , wherein the polyester is polyethylene terephthalate.

12. A device for manufacturing crystallizable polyester, for executing a process according to claim 5 , comprising a first crystallizer and a downstream cutter ( 2 ), wherein a sieve ( 5 ) is placed downstream from the cutter ( 2 ).

13. The device according to claim 12 , wherein a second crystallizer is placed downstream from the sieve ( 5 ).

14. The device according to claim 12 , wherein the polyester is polyethylene terephthalate.

Assignments (2)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 22, 2013
From: BÜHLER AG
To: BÜHLER THERMAL PROCESSES AG
Reel/Frame 031660/0660 →
CORRECTIVE DOCUMENT REEL/013681 FRAME 0492 DOCUMENT ID NO. 102345834A Recorded Jun 16, 2003
From: BORER, CAMILLE; MUELLER, MARTIN; GLOECKNER, FRANK
To: BUEHLER AG
Reel/Frame 014167/0610 →