IP Library Granted Patent US 6,849,672
Granted Patent B2
US 6,849,672 · App. 10/050,375 · Granted Feb 1, 2005

Superabsorbent thermoplastic composition and article including same

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Quick Facts
Patent No.
US 6,849,672
App. No.
10/050,375
Granted
Feb 1, 2005
Kind
B2
Abstract

A thermoplastic composition that includes from about 1% by weight to 25% by weight block copolymer having the formula (A-B)x where the A block includes polyvinylarene, the B block includes poly(monoalkenyl) and x is an integer of at least one, spherical superabsorbent particles comprising polyacrylate, and plasticizing oil, the composition exhibiting water gel time of no greater than 2 minutes, a viscosity of no greater than 100,000 centipoise and a wet tensile strength of at least 15 g/in 2 .

Claims (96)

1. A thermoplastic composition comprising:

from about 1% by weight to 25% by weight block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

from about 45% by weight to about 75% by weight superabsorbent polymer particles comprising polyacrylate and having a median particle diameter of from 20 μm to 30 μm; and

from about 15% by weight to about 40% by weight plasticizing oil, and a viscosity of no greater than 100,000 centipoise at 300° F.

2. The thermoplastic composition of claim 1 , further comprising surfactant.

3. The thermoplastic composition of claim 1 , further comprising from about 1% by weight to about 5% by weight surfactant.

4. The thermoplastic composition of claim 1 , comprising from 60% by weight to about 75% by weight said superabsorbent polymer.

5. The thermoplastic composition of claim 1 , wherein the block copolymer is selected from the group consisting of styrene-isoprene-styrene, styrene-ethylene-butylene-styrene, styrene-ethylene-propylene-styrene, styrene-butadiene-styrene and combinations thereof.

6. The thermoplastic composition of claim 1 , wherein said composition exhibits a water gel time of no greater than 2 minutes.

7. The thermoplastic composition of claim 1 , wherein said composition exhibits a water gel time of no greater than 1.5 minutes.

8. The thermoplastic composition of claim 1 , wherein said composition exhibits a water gel time of no greater than 1 minute.

9. The thermoplastic composition of claim 1 , wherein said composition exhibits a 0.9% saline solution gel time of no greater than 4 hours.

10. The thermoplastic composition of claim 1 , wherein said composition exhibits a 0.9% saline solution gel time of no greater than 1 hour.

11. The thermoplastic composition of claim 1 , wherein said composition exhibits a 0.9% saline solution gel time of no greater than 25 minutes.

12. The thermoplastic composition of claim 1 , wherein said composition exhibits a 0.9% saline solution gel time of no greater than 10 minutes.

13. The thermoplastic composition of claim 1 , wherein said composition exhibits a 0.9% saline solution gel time of no greater than 5 minutes.

14. The thermoplastic composition of claim 1 , wherein said composition exhibits an absorbent capacity of at least 60 g water/g of composition.

15. The thermoplastic composition of claim 1 , wherein said composition exhibits an absorbent capacity of at least 70 g water/g of composition.

16. The thermoplastic composition of claim 1 , wherein said composition exhibits an absorbent capacity of at least 90 g water/g of composition.

17. The thermoplastic composition of claim 1 , wherein said composition exhibits an absorbent capacity of at least 100 g water/g of composition.

18. The thermoplastic composition of claim 1 , wherein said composition exhibits an absorbent capacity of at least 110 g water/g of composition.

19. The thermoplastic composition of claim 1 , wherein said composition exhibits an absorbent capacity of at least 25 g 0.9% saline solution/g of composition.

20. The thermoplastic composition of claim 1 , wherein said composition exhibits an absorbent capacity of at least 30 g 0.9% saline solution/g of composition.

21. The thermoplastic composition of claim 1 , wherein said composition exhibits an absorbent capacity of at least 35 g 0.9% saline solution/g of composition.

22. A thermoplastic composition comprising:

block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

spherical superabsorbent particles comprising polyacrylate and having a median particle diameter of from 20 μm to 30 μm; and

plasticizing oil,

said composition exhibiting water gel time of no greater than 2 minutes.

23. The thermoplastic composition of claim 22 , wherein said block copolymer is selected from the group consisting of styrene-isoprene-styrene, styrene-ethylene-butylene-styrene, styrene-ethylene-propylene-styrene, styrene-butadiene-styrene and combinations thereof.

24. A thermoplastic composition comprising:

block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

spherical superabsorbent particles comprising polyacrylate and having a median particle diameter of from 20 μm to 30 μm; and

plasticizing oil,

said composition exhibiting a 0.9% saline solution gel time of no greater than 1 hour.

25. A thermoplastic composition comprising:

block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

spherical superabsorbent particles comprising polyacrylate and having a median particle diameter of from 20 μm to 30 μm; and

plasticizing oil,

said composition exhibiting an absorbent capacity of at least 70 g water/g of composition.

26. A thermoplastic composition comprising:

block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

spherical superabsorbent particles comprising polyacrylate and having a median particle diameter of from 20 μm to 30 μm; and

plasticizing oil,

said composition exhibiting an absorbent capacity of at least 25 g 0.9% aqueous saline solution/g of composition.

27. A thermoplastic adhesive composition comprising:

from about 1% by weight to 25% by weight block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

from about 45% by weight to about 75% by weight superabsorbent polymer particles comprising polyacrylate and having a median particle diameter of from 20 μm to 30 μm;

tackifying agent; and

from about 15% by weight to about 40% by weight plasticizing oil, said compostition having a viscosity of no greater than 100,000 centipoise at 300° F.

28. An absorbent article comprising:

an absorbent core;

the thermoplastic composition of claim 1 incorporated in said absorbent core.

29. An absorbent article comprising:

an absorbent core; and

the thermoplastic composition of claim 1 disposed on said absorbent core.

30. An absorbent article comprising:

a liquid permeable sheet;

a liquid impermeable barrier sheet;

an absorbent element disposed between the liquid permeable sheet and the barrier sheet; and

the thermoplastic composition of claim 1 disposed on at least one of said liquid permeable sheet, said barrier sheet and said absorbent element.

31. An absorbent article comprising:

a liquid permeable sheet;

a liquid impermeable barrier sheet;

an absorbent element disposed between the liquid permeable sheet and the barrier sheet; and

the thermoplastic composition of claim 1 incorporated in said absorbent element.

32. A thermoplastic composition comprising:

block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

spherical superabsorbent particles comprising polyacrylate; and

plasticizing oil,

said composition exhibiting a water gel time of no greater than 2 minutes, a viscosity of no greater than 100,000 centipoise at 300° F. and a wet tensile strength of at least 15 g/in 2 .

33. The thermoplastic composition of claim 32 , wherein said composition exhibits a 0.9% saline solution gel time of no greater than 1 hour.

34. The thermoplastic composition of claim 32 , wherein said composition exhibits a 0.9% saline solution gel time of no greater than 10 minutes.

35. The thermoplastic composition of claim 32 , wherein said composition exhibits a water gel time of no greater than 1.5 minutes, a viscosity of no greater than 30,000 centipoise at 300° F. and a wet tensile strength of at least 40 g/in 2 .

36. The thermoplastic composition of claim 32 , wherein said composition exhibits an absorption capacity of at least 70 g water/g composition.

37. A thermoplastic composition comprising:

block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

from about 45% by weight to about 75% by weight superabsorbent polymer particles that include polyacrylate; and

from about 15% by weight to about 40% by weight plasticizing oil,

said composition exhibiting a water gel time of no greater than 2 minutes, and an absorption capacity of at least 70 g water/g composition and at least 10 g 0.9% saline solution/g composition.

said compostion having a viscosity of no greater than 100,000 centipoise at 300° F.

38. A thermosplastic composition comprising:

block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

from about 45% by weight to about 75% by weight superabsorbent polymer particles comprising polyacrylate; and

from about 15% by weight to about 40% by weight plasticizer,

said composition exhibiting a viscosity of no greater than about 65,000 centipoise at 300° F.

39. A thermoplastic composition comprising:

thermoplastic polymer selected from the group consisting of amorphous polyolefins, crystalline polyolefins, polylactides, polyvinyl alcohols, copolyesters, polyesters, poly(ehtylene oxide) polyether amides, polyester ether block copolymers, polyamides, and combinations thereof;

from about 45% by weight to about 75% by weight superabsorbant polymer particles comprising polyacrylate; and

from about 15% by weight to about 40% by weight plasticizer,

said composition exhibiting a viscosity of no greater than about 65,000 centipoise at 300° F.

40. A thermoplastic composition comprising:

from about 1% by weight to 25% by weight block copolymer having the formula (A-B)x or A-B-A where the A block comprises polyvinylarene, the B block comprises poly(monoalkenyl), and x is an integer of at least one;

from 60% by weight to 75% by weight superabsorbent polymer particles comprising polyacrylate and having a median particle diameter of from 20μm to 30μm; and

from about 15% by weight to about 40% by weight plasticizing oil.

41. An absorbent article according to claim 31 selected from the group consisting of disposable diapers, sanitary napkins, wound care products, wipes, towels and tissues.

Assignments (4)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS (TERM LOAN) Recorded Feb 15, 2023
From: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
To: H.B. FULLER COMPANY; H.B. FULLER CONSTRUCTION PRODUCTS INC.; ROYAL ADHESIVES AND SEALANTS, LLC; ADCO PRODUCTS, LLC
Reel/Frame 062761/0884 →
TERM LOAN SECURITY AGREEMENT Recorded Oct 25, 2017
From: H.B. FULLER COMPANY; H.B. FULLER CONSTRUCTION PRODUCTS INC.; ROYAL ADHESIVES AND SEALANTS, LLC; ADCO PRODUCTS, LLC
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 044616/0671 →
RCF SECURITY AGREEMENT Recorded Oct 25, 2017
From: H.B. FULLER COMPANY; H.B. FULLER CONSTRUCTION PRODUCTS INC.; ROYAL ADHESIVES AND SEALANTS, LLC; ADCO PRODUCTS, LLC
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 044616/0700 →
CHANGE OF NAME Recorded Nov 30, 2009
From: H.B. FULLER LICENSING & FINANCING, INC.
To: H.B. FULLER COMPANY
Reel/Frame 023574/0530 →