Optical fiber preform manufacture using improved VAD
View Patent ↗The specification describes a VAD method for producing optical fiber preforms by depositing soot onto a solid core rod. The solid core rod preferably has a uniform composition, doped or undoped, suitable for the center core region of the preform. The primary cladding layer, and additional cladding layers if desired, are produced by depositing soot on the center core rod. The surface of the center core rod is treated with an etchant torch that traverses the center core rod in front of the soot deposition torch. This produces a clean interface between the core and primary cladding. This soot-on-center-core-rod method allows the production of sharp index profiles by reducing the diffusion of dopants into and out of the center core portion of the preform that occurs in soot-on-soot processes.
1. Process for the manufacture of an optical fiber preform comprising the steps of:
(a) preparing a core rod of solid glass,
(b) traversing the core rod sequentially with an etchant flame to etch the core rod followed immediately by a soot flame to deposit soot on the core rod so that the core rod is exposed to the etchant flame and the soot flame simultaneously.
2. The process of claim 1 wherein the etchant flame is produced by:
(i) flowing together:
a flow of etchant gas, and
a flow of fuel gas, to form an etchant gas mixture,
(ii) igniting the etchant gas mixture to form the etchant flame.
3. The process of claim 2 wherein the soot flame is produced by:
(i) flowing together:
a flow of one or more glass precursor gases, and
a flow of fuel gas, to form a soot gas mixture,
(ii) igniting the soot gas mixture to form the soot flame.
4. The process of claim 3 wherein the etchant gas comprises a fluoride gas.
5. The process of claim 4 wherein the etchant gas comprises CF 4 .
6. The process of claim 3 wherein the fuel gas comprises a mixture of hydrogen and oxygen.
7. The process of claim 3 wherein the glass precursor gases comprise SiCl 4 and GeCl 4 .
8. The process of claim 3 wherein the glass precursor gases comprise SiCl 4 .
9. The process of claim 3 including the step of heating the soot to consolidate it into solid glass.
10. The process of claim 1 wherein the core rod remains heated while traversed by the etchant flame and the soot flame.
11. Process for the manufacture of an optical fiber preform comprising the steps of:
(a) preparing a core rod of solid glass,
(b) traversing the core rod sequentially with an etchant flame to etch the core rod followed immediately by a first soot flame and a second soot flame to deposit soot on the core rod so that the core rod is exposed to the etchant flame and the soot flame simultaneously,
wherein the etchant flame is produced by:
(i) flowing together:
a flow of etchant gas, and
a flow of fuel gas, to form an etchant gas mixture,
(ii) igniting the etchant gas mixture to form the etchant flame and the first and second soot flames are each produced by
(i) flowing together:
a flow of one or more glass precursor gases, and
a flow of fuel gas, to form a soot gas mixture,
(ii) igniting the soot gas mixture to form the soot flame and further wherein the soot produced by the second flame has a composition different from the soot produced by the first flame.
12. The process of claim 11 wherein the core rod remains heated while traversed by the etchant flame and the soot flame.
13. Process for the manufacture of optical fibers comprising:
(a) preparing a preform, the preform having a core region and a cladding region comprising the steps of:
(i) preparing a core rod of solid glass;
(ii traversing the core rod sequentially with an etchant flame to etch the core rod followed immediately by a first soot flame and a second soot flame to deposit soot on the core rod so that the core rod is exposed to the etchant flame and the soot flame simultaneously, and
(iii) heating the soot to consolidate the soot into solid glass,
(b) mounting the preform in an optical fiber drawing apparatus,
(c) heating the preform to soften the glass, and
(d) drawing an optical fiber from the preform.
14. The process of claim 13 wherein the core rod remains heated while traversed by the etchant flame and the soot flame.