IP Library Granted Patent US 7,081,183
Granted Patent B2
US 7,081,183 · App. 10/201,332 · Granted Jul 25, 2006

Method of deresinating pulp using alkyl alcohol alkoxylate surfactants

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Quick Facts
Patent No.
US 7,081,183
App. No.
10/201,332
Granted
Jul 25, 2006
Kind
B2
Abstract

This invention is a method of reducing the resin content of chemical pulps comprising heating wood chips in an aqueous alkaline medium in the presence of an effective deresinating amount of an alkyl alcohol alkoxylate of formula RO[(CH 2 CHCH 3 O) x (CH 2 CH 2 O) y ]M wherein R is C 4 to C 40 alkyl; x is 1–50; y is 0–100 and M is H or an alkali metal, a cooking liquor comprising sodium hydroxide and sodium sulfite and the alkyl alcohol alkoxylate and a deresinated pulp prepared according to the method.

Claims (16)

1. A method of reducing the resin content of chemical pulps comprising heating wood chips in an aqueous alkaline medium in the presence of an effective deresinating amount of one or more deresinating aids, wherein the deresinating aids are selected from the group consisting of alkyl alcohol alkoxylates of formula RO[(CH 2 CHCH 3 O) x (CH 2 CH 2 O) y ]M wherein R is C 8 –C 22 alkyl; x is 1–20; y is 20–80 and M is H or an alkali metal.

2. The method of claim 1 wherein M is H.

3. The method of claim 1 wherein M is K.

4. The method of claim 1 wherein R is C 16 alkyl.

5. The method of claim 1 wherein the alkyl alcohol alkoxylate is a block polymer.

6. The method of claim 1 wherein the heating is done at a temperature of about 150° C. to about 175° C.

7. The method of claim 1 wherein heating is done in the presence of about 0.5 to about 2 pounds per ton of alkyl alcohol alkoxylate on an oven dried chip basis.

8. A cooking liquor comprising sodium hydroxide and sodium sulfite and and one or more deresinating aids wherein the deresinating aids are selected from the group consisting of alkyl akohol alkoxylates according to claim 1 .

9. A method of reducing the resin content of chemical pulps comprising heating wood chips in an aqueous alkaline medium in the presence of an effective deresinating amount of one or more surfactants wherein the surfactants are selected from the group consisting of alkyl alcohol alkoxylates of formula RO[(CH 2 CHCH 3 O) x (CH 2 CH 2 O) y ]M wherein R is C 8 –C 22 alkyl; x is 1–20; y is 20–80 and M is H or an alkali metal.

10. The method of claim 9 wherein M is H.

11. The method of claim 9 wherein M is K.

12. The method of claim 9 wherein R is C 16 alkyl.

13. The method of claim 9 wherein the alkyl alcohol alkoxylate is a block polymer.

14. The method of claim 9 wherein the heating is done at a temperature of about 150° C. to about 175° C.

15. The method of claim 9 wherein heating is done in the presence of about 0.5 to about 2 pounds per ton of alkyl alcohol alkoxylate on an oven dried chip basis.

16. A cooking liquor comprising sodium hydroxide and sodium sulfite and one or more surfactants, wherein the surfactants are selected from the group consisting of the alkyl alcohol alkoxylates according to claim 9 .

Assignments (5)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 4, 2017
From: NALCO COMPANY
To: ECOLAB USA INC.
Reel/Frame 042147/0420 →
RELEASE OF SECURITY INTEREST Recorded Feb 28, 2017
From: CITICORP NORTH AMERICA, INC.
To: NALCO COMPANY
Reel/Frame 041832/0826 →
CHANGE OF NAME Recorded Feb 28, 2017
From: NALCO COMPANY
To: NALCO COMPANY LLC
Reel/Frame 041835/0903 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 28, 2017
From: NALCO COMPANY LLC; CALGON CORPORATION; CALGON LLC; ONDEO NALCO ENERGY SERVICES, L.P.
To: ECOLAB USA INC.
Reel/Frame 041836/0437 →
RELEASE OF SECURITY INTEREST Recorded Feb 24, 2017
From: BANK OF AMERICA, N.A.
To: NALCO COMPANY
Reel/Frame 041808/0713 →