IP Library Granted Patent US 6,928,839
Granted Patent B2
US 6,928,839 · App. 10/219,745 · Granted Aug 16, 2005

Method for production of silica optical fiber preforms

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Quick Facts
Patent No.
US 6,928,839
App. No.
10/219,745
Granted
Aug 16, 2005
Kind
B2
Abstract

A device and method is disclosed for manufacturing optical fiber preforms utilizing microwave plasma assisted chemical vapor deposition. Precursor gas is introduced to the face of a vertically mounted dielectric rod, and a plasma is struck by means of simultaneous excitation of an E 01 type wave and an H type wave with rotating linear polarization. The silica rod is positioned so that its face is at the bottom of the tube. Precursor gas is delivered from a position below the face of the silica rod, and microwave energy, which travels through the rod to the rod face, is delivered from a source positioned above the rod. With this configuration, a uniformly dense plasma localized on the face of the rod can simultaneously deposit both a pure or doped core and a doped cladding. It is also useful for creating waveguides, preform cores for use as substrates in creating optical fiber preforms, capillaries and ceramic rods.

Claims (15)

1. A method of manufacturing silica optical fiber preforms by plasma deposition comprising the following steps:

positioning a rotating cylindrical dielectric starter rod coaxially within a vertically positioned cylindrical tube, wherein a diameter of said starter rod is equal to an inside diameter of said tube;

introducing a precursor gas mixture into a cavity within said tube;

simultaneously applying microwaves from independent sources through a single waveguide, wherein a first source emits rotationally symmetric microwaves, and a second source emits rotationally non-symmetrical microwaves with rotating linear polarization.

depositing a fiber preform core and a fiber preform cladding on a face of said starter rod.

2. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said waveguide is positioned above said starter rod and said microwaves propagate through said starter rod to said face; wherein further said precursor gas mixture is introduced from a position below said face.

3. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said rotationally symmetric microwaves are in an E 01 mode.

4. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said rotationally non-symmetrical microwaves are in a H 11 mode.

5. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said rotating starter rod produces rotating linear polarization in said rotationally non-symmetrical microwaves.

6. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said first source emits pulsed microwaves, and wherein said second source emits continuous microwaves.

7. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said preform core and said fiber preform cladding are deposited simultaneously.

8. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said fiber preform cladding is selected from a group consisting of fluorine-doped SiO 2 and pure SiO 2 .

9. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said fiber preform core is selected from a group consisting of SiON, SiO 2 doped with Al, SiO 2 doped with Al and a rare earth element, SiO 2 doped with Ge, and SiO 2 doped with Ge and a rare earth element.

10. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein said precursor gas mixture includes doping elements for doping said core.

11. A method of manufacturing silica optical fiber preforms according to claim 1 , wherein a flat silica plate is mounted on said rod face prior to deposition for the formation of a planar lightguide.

Assignments (3)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Dec 23, 2016
From: BIOLITEC PHARMA MARKETING LTD.
To: BIOLITEC UNTERNEHMENSBETEILIGUNGS II AG
Reel/Frame 041182/0578 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 2, 2009
From: BIOLITEC, INC.
To: BIOLITEC PHARMA MARKETING LTD.
Reel/Frame 022482/0944 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 2, 2009
From: CERAMOPTEC INDUSTRIES, INC.
To: BIOLITEC, INC.
Reel/Frame 022482/0956 →