Preparation of styryl dyes
View Patent ↗Process for preparing compounds of the formula (I) where R 1 , R 2 and R 3 are independently hydrogen, alkyl or cycloalkyl, characterized in that an aldehyde of the formula (II) is reacted with CH 2 (CN) 2 in the presence of butanol.
1. Process for preparing compounds of the formula (I)
where
R 1 , R 2 and R 3 are independently hydrogen, alkyl or cycloalkyl, comprising
reacting an aldehyde of the formula (II)
with CH 2 (CN) 2 in the presence of butanol.
2. Process according to claim 1 , wherein
R 1 is cycloalkyl,
R 2 is hydrogen, and
R 3 is C 1 -C 6 -alkyl.
3. Process according to claim 2 wherein R 1 is C 5 -C 7 cycloalkyl.
4. Process according to claim 3 wherein R 1 is cyclohexyl.
5. Process according to claim 2 wherein R 3 is ethyl.