IP Library Granted Patent US 7,018,971
Granted Patent B2
US 7,018,971 · App. 10/278,409 · Granted Mar 28, 2006

Process for the production of detergent granules

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Quick Facts
Patent No.
US 7,018,971
App. No.
10/278,409
Granted
Mar 28, 2006
Kind
B2
Abstract

A process for the preparation of detergent granules, the process comprising: (i) a first step of admixing in a mechanical granulator, an aluminosilicate and a first liquid binder comprising at least one surfactant, to produce a powder; and (ii) a second step of admixing in a low shear granulator, the powder produced in step (i), a water soluble salt and a second liquid binder, to produce the said detergent granules; wherein in step (ii), no more than 2%, preferably 0% by weight of the aluminosilicate based on the weight of the detergent granules is introduced into the low shear granulator of step (ii).

Claims (13)

1. A process for the preparation of detergent granules, the process comprising:

(i) a first step of admixing in a mechanical granulator, an aluminosilicate and a first liquid binder comprising at least one surfactant, to produce a powder; and

(ii) a second step of admixing in a low shear gas fluidization granulator, the powder produced in step (i), a water soluble salt and a second liquid binder, to produce the said detergent granules;

wherein in step (ii), no more than 2%, preferably 0% by weight of the aluminosilicate based on the weight of the detergent granules is introduced into the low shear granulator of step (ii); and wherein no more than 9% by weight of the water soluble salt, based on the weight of the detergent granules, is introduced into the mechanical granulator of step (i).

2. A process according to claim 1 , wherein the first liquid binder and second liquid binder have substantially the same composition.

3. A process according to claim 1 , wherein the first and second liquid binders comprise anionic surfactant, nonionic surfactant, and preferably also, soap.

4. A process according to claim 1 , wherein the first liquid binder is from 30% to 90%, preferably from 60% to 80% by weight of the total weight of first liquid binder plus second liquid binder.

5. A process according to claim 1 , wherein no more than 7%, by weight of the water soluble salt, based on the weight of the detergent granules is introduced into the mechanical granulator of step (i).

6. A process according to claim 1 , wherein the inorganic salt comprises sodium carbonate.

7. A process according to claim 1 , wherein the amount of aluminosilicate in the detergent granules is from 10% to 60%, preferably from 15% to 50% by weight of those granules.

8. A process according to claim 1 , wherein up to 90%, preferably up to 70% by weight of the aluminosilicate in the detergent granules is replaced by an insoluble absorbent powder substance.

9. A process according to claim 8 , wherein the insoluble absorbent powder substance is selected from clays, silica and insoluble silicate salts.

10. A process according to claim 1 , wherein no more than 0%, by weight of the water soluble salt, based on the weight of the detergent granules is introduced into the mechanical granulator of step (i).

Assignments (6)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2017
From: THE SUN PRODUCTS CORPORATION
To: HENKEL IP & HOLDING GMBH
Reel/Frame 041937/0131 →
RELEASE OF SECURITY INTEREST Recorded Sep 14, 2016
From: JPMORGAN CHASE BANK, N.A.
To: THE SUN PRODUCTS CORPORATION
Reel/Frame 040027/0272 →
SECURITY AGREEMENT Recorded Mar 27, 2013
From: THE SUN PRODUCTS CORPORATION
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 030100/0687 →
RELEASE BY SECURITY PARTY AS PREVIOUSLY RECORDED ON REEL 029816 FRAME 0362 Recorded Mar 25, 2013
From: U.S. BANK NATIONAL ASSOCIATION
To: SPOTLESS HOLDING CORP.; SPOTLESS ACQUISITION CORP.; THE SUN PRODUCTS CORPORATION (F/K/A HUISH DETERGENTS, INC.)
Reel/Frame 030080/0550 →
SECOND LIEN GRANT OF SECURITY INTEREST IN PATENT RIGHTS Recorded Feb 14, 2013
From: SPOTLESS HOLDING CORP.; SPOTLESS ACQUISITION CORP.; THE SUN PRODUCTS CORPORATION (F/K/A HUISH DETERGENTS, INC.)
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 029816/0362 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 10, 2009
From: CONOPCO, INC.
To: THE SUN PRODUCTS CORPORATION
Reel/Frame 023065/0691 →