IP Library Granted Patent US 7,037,474
Granted Patent B2
US 7,037,474 · App. 10/324,833 · Granted May 2, 2006

Use of sulfide-containing liquors for removing mercury from flue gases

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Quick Facts
Patent No.
US 7,037,474
App. No.
10/324,833
Granted
May 2, 2006
Kind
B2
Abstract

A method and apparatus for reducing and removing mercury in industrial gases, such as a flue gas, produced by the combustion of fossil fuels, such as coal, adds sulfide ions to the flue gas as it passes through a scrubber. Ideally, the source of these sulfide ions may include at least one of: sulfidic waste water, kraft caustic liquor, kraft carbonate liquor, potassium sulfide, sodium sulfide, and thioacetamide. The sulfide ion source is introduced into the scrubbing liquor as an aqueous sulfide species. The scrubber may be either a wet or dry scrubber for flue gas desulfurization systems.

Claims (14)

1. In a method using a scrubber, having a scrubber liquor containing an aqueous alkali reagent, for receiving and scrubbing an industrial gas with the scrubbing liquor, the improvement comprising:

providing an industrial gas containing oxidized mercury to a scrubber;

providing an aqueous sulfide species selected from the group consisting of: sodium sulfide, potassium sulfide, sodium hydrosulfide, potassium hydrosulfide, sulfidic waste water, kraft caustic liquor and kraft carbonate liquor to the scrubber;

creating a gas-liquid interface within the scrubber and mixing the industrial gas with the aqueous sulfide species in order to rapidly precipitate the oxidized mercury at the gas-liquid interface, thereby producing a mercury-free industrial gas within the scrubber wherein the precipitated mercury remains in the scrubbing liquor; and

subsequently removing the mercury-free industrial gas from the scrubber.

2. The method according to claim 1 , wherein the scrubber is a wet scrubber and further comprising the step of: conveying the industrial gas through a dust collector to remove particulates from the industrial gas prior to the creating a gas-liquid interface in the wet scrubber.

3. The method according to claim 2 , wherein the dust collector is a fabric filter or an electrostatic precipitator.

4. The method according to claim 1 , wherein the scrubber is a dry scrubber and further comprising the step of: providing the mercury-free industrial gas to a dust collector in order to remove other non-mercuric particulates from the mercury-free industrial gas.

5. The method according to claim 4 , wherein the dust collector is a fabric filter or an electrostatic precipitator.

6. The method according to claim 1 , wherein the sulfide species is provided directly to the scrubbing liquor.

7. The method according to claim 6 , wherein the scrubber is a wet scrubber and further comprising the steps of: conveying the industrial gas through a dust collector to remove particulates from the industrial gas prior to the creating a gas-liquid interface in the wet scrubber.

8. The method according to claim 7 , wherein the dust collector is a fabric filter or an electrostatic precipitator.

9. The method according to claim 6 , wherein the scrubber is a dry scrubber and further comprising the step of providing the mercury-free industrial gas to a dust collector in order to remove other non-mercuric particulates from the mercury-free industrial gas.

10. The method according to claim 9 , wherein the dust collector is a fabric filter or an electrostatic precipitator.

Assignments (10)
RELEASE OF SECURITY INTEREST Recorded Jul 1, 2021
From: BANK OF AMERICA, N.A.
To: DIAMOND POWER INTERNATIONAL, LLC (F/K/A DIAMOND POWER INTERNATIONAL, INC.); MEGTEC TURBOSONIC TECHNOLOGIES, INC.; THE BABCOCK & WILCOX COMPANY (F/K/A BABCOCK & WILCOX POWER GENERATION GROUP, INC.); BABCOCK & WILCOX SPIG, INC.; BABCOCK & WILCOX TECHNOLOGY, LLC (F/K/A MCDERMOTT TECHNOLOGY, INC.); SOFCO-EFS HOLDINGS LLC; BABCOCK & WILCOX MEGTEC, LLC
Reel/Frame 057337/0823 →
CHANGE OF NAME Recorded Sep 24, 2015
From: BABCOCK & WILCOX POWER GENERATION GROUP, INC.
To: THE BABCOCK & WILCOX COMPANY
Reel/Frame 036675/0434 →
SECURITY INTEREST Recorded Jul 28, 2015
From: BABCOCK & WILCOX POWER GENERATION GROUP, INC. (TO BE RENAMED THE BABCOCK AND WILCOX COMPANY)
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 036201/0598 →
CORRECTIVE ASSIGNMENT TO CORRECT THE ASSIGNEE NAME PREVIOUSLY RECORDED AT REEL: 021998 FRAME: 0870. ASSIGNOR(S) HEREBY CONFIRMS THE CHANGE OF NAME. Recorded Jun 9, 2015
From: THE BABCOCK & WILCOX COMPANY
To: BABCOCK & WILCOX POWER GENERATION GROUP, INC.
Reel/Frame 035871/0019 →
SECURITY INTEREST Recorded Jul 22, 2014
From: BABCOCK & WILCOX POWER GENERATION GROUP, INC.
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 033380/0744 →
NOTICE OF GRANT OF SECURITY INTEREST IN PATENTS Recorded Sep 30, 2010
From: BABCOCK & WILCOX POWER GENERATION GROUP, INC. (F.K.A. THE BABCOCK & WILCOX COMPANY)
To: BANK OF AMERICA, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 025066/0080 →
RELEASE OF SECURITY INTEREST Recorded Aug 3, 2010
From: CREDIT SUISSE AG, CAYMAN ISLANDS BRANCH
To: THE BABCOCK & WILCOX COMPANY; AMERICON EQUIPMENT SERVICES, INC.; AMERICON, INC.; APPLIED SYNERGISTICS, INC.; B & W SERVICE COMPANY; BABCOCK & WILCOX CHINA HOLDINGS, INC.; BABCOCK & WILCOX CONSTRUCTION CO., INC.; BABCOCK & WILCOX DENMARK HOLDINGS, INC.; BABCOCK & WILCOX EBENSBURG POWER, INC.; BABCOCK & WILCOX EQUITY INVESTMENTS, INC.; BABCOCK & WILCOX INTERNATIONAL SALES AND SERVICE CORPORATION; BABCOCK & WILCOX INTERNATIONAL, INC.; DIAMOND OPERATING CO., INC.; DIAMOND POWER AUSTRALIA HOLDINGS, INC.; DIAMOND POWER CHINA HOLDINGS, INC.; DIAMOND POWER EQUITY INVESTMENTS, INC.; DIAMOND POWER INTERNATIONAL, INC.; PALM BEACH RESOURCE RECOVERY CORPORATION; POWER SYSTEMS OPERATIONS, INC.; REVLOC RECLAMATION SERVICE, INC.; NATIONAL ECOLOGY COMPANY; NORTH COUNTY RECYCLING, INC.
Reel/Frame 024776/0693 →
CHANGE OF NAME Recorded Dec 19, 2008
From: THE BABCOCK & WILCOX COMPANY
To: THE BABCOCK & WILCOX POWER GENERATION GROUP, INC.
Reel/Frame 021998/0870 →
SECURITY AGREEMENT Recorded Mar 22, 2006
From: THE BABCOCK & WILCOX COMPANY
To: CREDIT SUISSE, CAYMAN ISLANDS BRANCH, AS COLLATERAL AGENT
Reel/Frame 017344/0565 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 21, 2006
From: MCDERMOTT TECHNOLOGY, INC.
To: THE BABCOCK & WILCOX COMPANY
Reel/Frame 017186/0749 →