IP Library Granted Patent US 7,169,827
Granted Patent B2
US 7,169,827 · App. 10/332,160 · Granted Jan 30, 2007

Production of polypropylene having improved properties

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Quick Facts
Patent No.
US 7,169,827
App. No.
10/332,160
Granted
Jan 30, 2007
Kind
B2
Abstract

A process for producing polypropylene having increased melt strength, the process comprising irradiating polypropylene which has been polymerised using a Ziegler-Natta catalyst with an electron beam having an energy of at least 5 MeV and a radiation dose of at least 10 kGray and mechanically processing the irradiated polypropylene to form long chain branches on the polypropylene molecules, whereby the polypropylene has a melt flow index (MFI) of at least 25 dg/min.

Claims (9)

1. A process for producing a propylene polymer having increased melt strength, the process comprising irradiating a propylene polymer which has been polymerized using a Ziegler-Natta catalyst with an electron beam having an energy of at least 5 MeV and a radiation dose of at least 10 kGray and mechanically processing a melt of the irradiated propylene polymer to form long chain branches on the propylene polymer molecules, whereby the irradiated propylene polymer has a melt flow index (MFI) of at least 25 dg/min.

2. A process according to claim 1 wherein the electron beam has an energy of at least 10 MeV.

3. A process according to claim 1 wherein the electron beam has an energy within the range of 10–25 MeV.

4. A process according to claim 1 wherein the power of the electron beam is from 50 to 500 kW.

5. A process according to claim 1 wherein the power of the electron beam is from 120–250 kW.

6. A process according to claim 1 wherein the radiation dose is within the range of 10–60 kGray.

7. A process according to claim 1 wherein said propylene polymer is a polypropylene homopolymer.

8. A method of claim 1 wherein said pro;ylene polymer is a copolymer of propylene and at least one alpha olefin selected from a group consisting of ethylene and C 4 –C 10 1-olefins.

9. A process accorded to claim 1 wherein said propylene polymer is isotactic polypropylene.

Assignments (2)
CHANGE OF NAME Recorded Aug 30, 2005
From: ATOFINA RESEARCH
To: TOTAL PETROCHEMICALS RESEARCH FELUY
Reel/Frame 016470/0203 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 7, 2003
From: DEBRAS, GUY; DUPIRE, MARC; MICHAEL, JACQUES
To: ATOFINA RESEARCH, S.A.
Reel/Frame 014671/0405 →