IP Library Granted Patent US 7,078,374
Granted Patent B2
US 7,078,374 · App. 10/363,593 · Granted Jul 18, 2006

Method of preparing fabric conditioning compositions

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Quick Facts
Patent No.
US 7,078,374
App. No.
10/363,593
Granted
Jul 18, 2006
Kind
B2
Abstract

A method of preparing an aqueous dispersion of a fabric conditioning composition comprises mixing 7.5 to 60% by weight of a cationic fabric softening compound, the compound having one or more hydrocarbyl chains formed from parent fatty acyl compounds or fatty acids having an iodine value of from 0 to 20 with 0.01%–1.5% by weight of a nonionic surfactant viscosity modifier and up to 1.4% by weight of a fatty alcohol, the combination of (b) and (c) being no more than 1.5% by weight, based on the total weight of the composition, the aqueous dispersion being subjected to high-shear below the phase transition temperature of compound (a) for a time sufficient to provide a composition having a viscosity of from 10 to 250 mPa·s measured at 20 s−1 using a Haake NV1 Rotoviscometer at 20° C.

Claims (29)

1. A method for preparing a fabric conditioning composition comprising mixing with water:

(a) 7.5 to 60% by weight of a cationic fabric softening compound of formula (I), (II) or (III):

wherein each R is independently selected from a C 5-35 alkyl or alkenyl group, R 1 represents a C 1-4 alkyl, C 2-4 alkenyl or a C 1-4 hydroxyalkyl group,

n is O or a number selected from 1 to 4, m is 1, 2 or 3 and denotes the number of moieties to which it relates that pend directly from the N atom, and X − is an anionic group;

wherein each R 1 group is independently selected from C 1-4 alkyl, hydroxyalkyl or C 2-4 alkenyl groups; and wherein each R 2 group is independently selected from C 8-28 alkyl or alkenyl groups; n is 0 or an integer from 1 to 5 and T and X − are as defined above;

wherein each R 1 group is independently selected from C 1-4 alkyl, or C 2-4 alkenyl groups; and wherein each R 2 group is independently selected from C 8-28 alkyl or alkenyl groups; n is 0 or an integer from 1 to 5 and T and X − are as defined above;

the compound having one or more hydrocarbyl chains formed from parent fatty acyl compounds or fatty acids having an iodine value of from 0 to 20; and

(b) 0.01%–1.5% by weight of a nonionic surfactant viscosity modifier; and

(c) about 0.01% to about 1.4% by weight of a fatty alcohol; wherein said fatty alcohol is un-alkoxytated and contains about 15 to about 22 carbon atoms in a hydrocarbyl chain;

wherein the combination of (b) and (c) is no more than 1.5% by weight, based on the total weight of the composition;

and wherein components (a), (b) and (c) are mixed to form an aqueous dispersion, the aqueous dispersion being subjected to high-shear below the phase transition temperature of component (a) for a time sufficient to provide a composition having a viscosity of from 10 to 250 mPa·s measured at 20 s −1 using a Haake MV1 Rotoviscometer at 25° C.

2. A method according to claim 1 wherein components (a), (b), (c) are melted together to form a premix prior to mixing with water.

3. A fabric conditioning composition obtainable by the method of claim 1 .

4. A composition according to claim 3 comprising a cationic fabric softening compound of formula (I).

5. A composition according to claim 3 wherein the weight ratio of cationic softening material to the combined weight of the nonionic surfactant viscosity modifier and fatty alcohol is 5:1 to 50:1.

6. A composition according to claim 3 wherein the cationic softening material in present in an amount from 11 to 22% by weight, based on the total weight of the composition.

7. A composition as claimed in claim 3 wherein the nonionic surfactant viscosity modifier is a C 10-22 fatty alcohol having an alkoxylation number of 3 to 30.

8. A method for preparing a fabric conditioning composition comprising mixing with water:

(a) 7.5 to 60% by weight of a cationic fabric softening compound of formula (I), (II) or (III);

wherein each R is independently selected from a C 5-35 alkyl or alken group, R 1 represents a C 1-4 alkyl, C 2-4 alkenyl or a C 1-4 hydroxyalkyl group,

n is O or a number selected from 1 to 4, m is 1, 2 or 3 and denotes the number of moieties to which it relates that pend directly from the N atom, and X − is an anionic group:

wherein each R 1 group is independently selected from C 1-4 alkyl, hydroxyalkyl or C 2-4 alkenyl groups; and wherein each R 2 group is independently selected from C 8-28 alkyl or alkenyl groups; n is 0 or an integer from 1 to 5 and T and X − are as defined above;

wherein each R 1 group is independently selected from C 1-4 alkyl, or C 2-4 alkenyl groups: and wherein each R 2 group is independently selected from C 8-28 alkyl or alkenyl groups: n is 0 or an integer from 1 to 5 and T and X − are as defined above;

the compound having one or more hydrocarbyl chains formed from parent fatty acyl compounds or fatty acids having an iodine value of from 0 to 20; and

(b) 0.01%–1.5% by weight of a nonionic surfactant viscosity modifier; and

(c) up to 1.4% by weight of a fatty alcohol

wherein the combination of (b) and (c) is no more than 1.5% by weight, based on the total weight of the composition;

and wherein components (a), (b) and (c) are mixed to form an aqueous dispersion, the aqueous dispersion being subjected to high-shear below the phase transition temperature of component (a) for a time sufficient to provide a composition having a viscosity of from 10 to 250 mPa·s measured at 20 s −1 using a Haake MV1 Rotoviscometer at 25° C;

wherein the high shear is applied at an angular velocity of from 3,000 to 10,000 rpm where the number of batch volumes passing through a mill below the phase transition temperature is from 0.5 to 4 batch volumes.

Assignments (7)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 9, 2017
From: THE SUN PRODUCTS CORPORATION
To: HENKEL IP & HOLDING GMBH
Reel/Frame 041937/0131 →
RELEASE OF SECURITY INTEREST Recorded Sep 14, 2016
From: JPMORGAN CHASE BANK, N.A.
To: THE SUN PRODUCTS CORPORATION
Reel/Frame 040027/0272 →
SECURITY AGREEMENT Recorded Mar 27, 2013
From: THE SUN PRODUCTS CORPORATION
To: JPMORGAN CHASE BANK, N.A., AS ADMINISTRATIVE AGENT
Reel/Frame 030100/0687 →
RELEASE BY SECURITY PARTY AS PREVIOUSLY RECORDED ON REEL 029816 FRAME 0362 Recorded Mar 25, 2013
From: U.S. BANK NATIONAL ASSOCIATION
To: SPOTLESS HOLDING CORP.; SPOTLESS ACQUISITION CORP.; THE SUN PRODUCTS CORPORATION (F/K/A HUISH DETERGENTS, INC.)
Reel/Frame 030080/0550 →
SECOND LIEN GRANT OF SECURITY INTEREST IN PATENT RIGHTS Recorded Feb 14, 2013
From: SPOTLESS HOLDING CORP.; SPOTLESS ACQUISITION CORP.; THE SUN PRODUCTS CORPORATION (F/K/A HUISH DETERGENTS, INC.)
To: U.S. BANK NATIONAL ASSOCIATION
Reel/Frame 029816/0362 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 10, 2009
From: CONOPCO, INC.
To: THE SUN PRODUCTS CORPORATION
Reel/Frame 023065/0691 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 8, 2003
From: HOWARD, JANE; ORMANDY, KEVIN ANTHONY; PARSONS, JOHN STUART
To: UNILEVER HOME & PERSONAL CARE USA, DIVISION OF CONOPCO, INC.
Reel/Frame 013970/0202 →