IP Library Granted Patent US 8,545,828
Granted Patent B1
US 8,545,828 · App. 10/371,459 · Granted Oct 1, 2013

High viscosity heat-treated xanthan gum

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Quick Facts
Patent No.
US 8,545,828
App. No.
10/371,459
Granted
Oct 1, 2013
Kind
B1
Abstract

The present invention is directed to heat treated xanthan gums, which have improved solution viscosity over other xanthan gums heat-treated under the same processing conditions while maintaining the improved ease of use and the short, non-stringy gel texture of heat treated xanthan gums. Such high solution viscosity xanthan gums are suitable in a variety of applications, including cosmetic and personal care compositions.

Claims (17)

1. A method of producing heat-treated xanthan gum comprising:

heat treating native xanthan gum having a solution viscosity of about 3000 cps or greater prior to heat treating and an ash content of about 8.5% or less,

wherein the resultant heat treated xanthan gum has a solution viscosity of about 15,000 cps or greater, in a 1% aqueous solution,

wherein the increase in solution viscosity of the heat treated xanthan gum is about 10,000 cps or greater over the viscosity of the xanthan gum prior to heat treatment,

wherein the native xanthan gum is heat treated to a moisture content of about 1% or less,

wherein a time to fully disperse the heat treated xanthan gum is reduced by at least 25% and no more than 70% compared to the xanthan gum prior to heat treatment, and

wherein the heat treated xanthan gum has clear to translucent clarity.

2. The method of claim 1 , wherein the heat treatment is at a temperature of about 60° C. or more for about 30 minutes or more.

3. The method of claim 1 , wherein the heat treatment is at a temperature between 100° C. and about 120° C.

4. The method of claim 1 , wherein the heat treatment is for about one hour or more.

5. The method of claim 1 , wherein the heat treatment is from about 2 to about 4 hours.

6. The method of claim 1 further comprising modifying the xanthan gum wherein the modification is chosen from oxidation, enzyme conversion, acid hydrolysis, heat and/or acid dextrinization, shear, chemical modification, enzymatical modification, and physical modification.

7. The method of claim 1 further comprising purifying the heat treated xanthan gum.

8. The method of claim 1 wherein the xanthan gum is heat treated using oven, fluidized bed, infrared or microwave heat treatment.

9. The method of claim 8 wherein the xanthan gum is heat treated using a vented oven.

10. The method of claim 1 wherein the xanthan gum is heat treated at atmospheric pressure.

11. The method of claim 8 , wherein the xanthan gum is heat treated using a fluidized bed.

Assignments (5)
CHANGE OF NAME Recorded Sep 18, 2019
From: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: NOURYON CHEMICALS INTERNATIONAL B.V.
Reel/Frame 050426/0671 →
SECURITY INTEREST Recorded Oct 1, 2018
From: STARFRUIT US MERGER SUB 1 LLC; STARFRUIT US MERGER SUB 2 LLC; AKZO NOBEL SURFACE CHEMISTRY LLC; AKZO NOBEL CHEMICALS B.V.; AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
To: WILMINGTON TRUST (LONDON) LIMITED, AS COLLATERAL AGENT
Reel/Frame 047231/0001 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Nov 13, 2017
From: AKZO NOBEL N.V.
To: AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
Reel/Frame 044427/0759 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 19, 2009
From: NATIONAL STARCH AND CHEMICAL INVESTMENT HOLDING CORPORATION
To: AKZO NOBEL N.V.
Reel/Frame 022117/0694 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Apr 29, 2003
From: CAO, HONGJIE; MARTINO, GARY T.
To: NATIONAL STARCH AND CHEMICAL INVESTMENT HOLDING CORPORATION
Reel/Frame 013996/0193 →