IP Library Granted Patent US 7,318,998
Granted Patent B2
US 7,318,998 · App. 10/394,576 · Granted Jan 15, 2008

Tissue decellularization

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Quick Facts
Patent No.
US 7,318,998
App. No.
10/394,576
Granted
Jan 15, 2008
Kind
B2
Abstract

The present invention relates, in general, to tissue decellularization and, in particular to a method of treating tissues, for example, heart valves, tendons and ligaments, so as to render them acellular and thereby limit mineralization and/or immunoreactivity upon implementation in vivo.

Claims (16)

1. A method of producing a bioprosthetic tissue consisting essentially of the of the steps of:

i) washing a starting tissue selected from the group consisting of a heart valve, tendon, ligament, artery, vein, diaphragm, pericardium, fascia, dura mater and tympanic membrane with a bioburden reducing agent so that said starting tissue is disinfected,

ii) subsequent to step (i), contacting said disinfected tissue with a hypotonic solution so that lysis of cells of said disinfected tissue is effected,

iii) incubating the hypotonic solution-treated tissue resulting from step (ii) with at least one enzyme, wherein said at least one enzyme consists of at least one nuclease, so that nucleic acid associated with said cells lysed as a result of step (ii) is degraded, and

iv) sterilizing the nuclease-treated tissue resulting from step (iii).

2. The method according to claim 1 wherein said method of production further consists essentially of, after step (iii), the step of contacting the tissue resulting from step (iii) with a physiologically isotonic solution.

3. The method according to claim 1 wherein said starting tissue is a human tissue.

4. The method according to claim 3 wherein said starting tissue is obtained from a human heart valve.

5. The method according to claim 1 wherein said tissue resulting from step (iii) is at least 70% decellularized.

6. The method according to claim 1 wherein said at least one enzyme consists of DNAase or RNAase.

7. The method according to claim 1 wherein said at least one enzyme consists of DNAase and RNAase.

8. The method according to claim 1 wherein said starting tissue is non-human tissue.

9. The method according to claim 1 wherein said bioburden reducing agent is an antibiotic or mixture of antibiotics.

10. The method according to claim 1 wherein said step (ii) is carried out at a temperature of between 30° to 40° C.

11. The method according to claim 1 wherein said method of production further consists essentially of, after step (i), the steps of cryopreserving said disinfected tissue and then thawing said cryopreserved, disinfected tissue.

12. The method according to claim 1 wherein, in step (ii), said hypotonic solution is water.

Assignments (8)
TERMINATION AND RELEASE OF SECURITY INTEREST IN PATENTS Recorded Jan 22, 2024
From: DEUTSCHE BANK AG NEW YORK BRANCH
To: CRYOLIFE, INC.; ON-X LIFE TECHNOLOGIES, INC.
Reel/Frame 066360/0562 →
PATENT SECURITY AGREEMENT Recorded Dec 1, 2017
From: CRYOLIFE, INC.; ON-X LIFE TECHNOLOGIES, INC. (F/K/A MCRI, INC.)
To: DEUTSCHE BANK AG NEW YORK BRANCH, AS COLLATERAL AGENT
Reel/Frame 044616/0940 →
RELEASE OF SECURITY INTEREST IN PATENTS Recorded Dec 1, 2017
From: HEALTHCARE FINANCIAL SOLUTIONS, LLC, AS ADMINISTRATIVE AGENT
To: CRYOLIFE, INC.; CRYOLIFE ACQUISITION CORPORATION; CARDIOGENESIS CORPORATION (N/K/A CRYOLIFE, INC.); HEMOSPHERE, INC.; ON-X LIFE TECHNOLOGIES, INC. (F/K/A MCRI, INC.); VALVE SPECIAL PURPOSE CO., LLC
Reel/Frame 044621/0240 →
SECURITY INTEREST Recorded Jan 21, 2016
From: CRYOLIFE, INC., AS GRANTOR; VALVE SPECIAL PURPOSE CO., LLC, AS GRANTOR; ON-X LIFE TECHNOLOGIES, INC., AS GRANTOR
To: HEALTHCARE FINANCIAL SOLUTIONS, LLC, AS AGENT
Reel/Frame 037569/0212 →
ASSIGNMENT OF INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Nov 19, 2015
From: GENERAL ELECTRIC CAPITAL CORPORATION, AS RETIRING AGENT
To: HEALTHCARE FINANCIAL SOLUTIONS, LLC, AS SUCCESSOR AGENT
Reel/Frame 037146/0466 →
PATENT SECURITY AGREEMENT Recorded Mar 31, 2008
From: CRYOLIFE, INC.; CRYOLIFE ACQUISITION CORPORATION
To: GENERAL ELECTRIC CAPITAL CORPORATION, AS AGENT
Reel/Frame 020723/0392 →
RELEASE OF SECURITY INTEREST Recorded Feb 29, 2008
From: WELLS FARGO FOOTHILL, INC.
To: CRYOLIFE, INC.
Reel/Frame 020580/0036 →
SECURITY AGREEMENT Recorded Feb 10, 2005
From: CRYOLIFE, INC.; CRYOLIFE TECHNOLOGY, INC.
To: WELLS FARGO FOOTHILL, INC.
Reel/Frame 016256/0042 →