IP Library Granted Patent US 6,916,750
Granted Patent B2
US 6,916,750 · App. 10/395,820 · Granted Jul 12, 2005

High performance elastic laminates made from high molecular weight styrenic tetrablock copolymer

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Quick Facts
Patent No.
US 6,916,750
App. No.
10/395,820
Granted
Jul 12, 2005
Kind
B2
Abstract

An elastic laminate is provided which has an elastic layer and one or two outer facing layers. The elastic layer is formed from an improved styrene-(ethylene-butylene)-styrene-(ethylene-butylene) tetrablock copolymer, or a blend of the copolymer. The copolymer has a number average molecular weight of at least about 70,000. The two ethylene-butylene blocks have number average molecular weights which together constitute more than 75% of the number average molecular weight of the copolymer.

Claims (88)

1. An elastic laminate, comprising:

an elastic layer including about 25-100% by weight of a SEBSEB copolymer; and

at least one facing layer comprising a fibrous thermoplastic nonwoven web, bonded to the elastic layer;

the SEBSEB copolymer having a number average molecular weight of at least about 70,000 and including a styrene end block, an ethylene-butylene midblock, a styrene midblock, and an ethylene-butylene end block;

the ethylene-butylene blocks having number average molecular weights which together constitute more than 75% of the number average molecular weight for the SEBSEB copolymer;

the styrene midblock having a number average molecular weight about 5-50% higher than a number average molecular weight of the styrene end block.

2. The elastic laminate of claim 1 , comprising a stretch-bonded laminate.

3. The elastic laminate of claim 2 , comprising a vertical filament laminate.

4. The elastic laminate of claim 1 , comprising a neck-bonded laminate.

5. The elastic laminate of claim 4 , comprising a neck-stretch bonded laminate.

6. The elastic laminate of claim 1 , comprising two of the facing layers bonded on both sides of the elastic layer.

7. The elastic laminate of claim 1 , wherein the elastic layer comprises an array of substantially parallel, nonintersecting filaments.

8. The elastic laminate of claim 1 , wherein the elastic layer comprises a film.

9. The elastic laminate of claim 1 , wherein the elastic layer comprises a foam.

10. The elastic laminate of claim 1 , wherein the elastic layer comprises a fibrous nonwoven web.

11. The elastic laminate of claim 1 , wherein the elastic layer comprises a net.

12. The elastic laminate of claim 1 , wherein the SEBSEB copolymer has a number average molecular weight of about 73,000 to about 100,000.

13. The elastic laminate of claim 1 , wherein the elastic layer further comprises a poly(monoalkenyl arene).

14. The elastic laminate of claim 13 , wherein the elastic layer further comprises a polyolefin.

15. The elastic laminate of claim 14 , wherein the elastic layer further comprises a tackifying resin.

16. An elastic laminate, comprising:

an elastic layer including about 50-80% by weight of a SEBSEB copolymer, about 4-15% by weight of a poly(monoalkenyl arene), about 5-20% by weight of a polyolefin, and zero to about 25% by weight of a tackifying resin; and

at least one fibrous thermoplastic nonwoven facing layer bonded to the elastic layers;

the SEBSEB copolymer having a number average molecular weight of at least about 70,000 and including a styrene end block, an ethylene-butylene midblock, a styrene midblock, and an ethylene-butylene end block;

the styrene midblock having a number average molecular weight about 5-50% higher than a number average molecular weight of the styrene end block.

17. The elastic laminate of claim 16 , comprising two of the facing layers bonded on both sides of the elastic layer.

18. The elastic laminate of claim 16 , wherein the elastic layer includes about 65-75% by weight of the SEBSEB copolymer, about 5-10% by weight of the poly(monoalkenyl arene), about 5-15% by weight of the polyolefin, and about 10-25% by weight of the tackifying resin.

19. The elastic laminate of claim 16 , wherein the SEBSEB copolymer has a number average molecular weight of about 70,000 to about 120,000.

20. The elastic laminate of claim 16 , wherein the poly(monoalkenyl arene) comprises polystyrene.

21. The elastic laminate of claim 16 , wherein the polyolefin comprises a polyethylene wax.

22. The elastic laminate of claim 16 , wherein the tackifying resin comprises a hydrocarbon resin selected from low molecular weight hydrogenated polystyrene, low molecular weight hydrogenated poly-alphamethyl styrene, and combinations thereof.

23. The elastic laminate of claim 16 , wherein the facing layer comprises a fibrous nonwoven web.

24. The elastic laminate of claim 16 , wherein the elastic layer comprises an array of substantially parallel, nonintersecting filaments.

25. The elastic laminate of claim 16 , wherein the elastic layer comprises a film.

26. The elastic laminate of claim 16 , wherein the elastic layer comprises a foam.

27. The elastic laminate of claim 16 , wherein the elastic layer comprises a net.

28. The elastic laminate of claim 16 , wherein the elastic layer comprises a fibrous nonwoven web.

29. A disposable garment comprising the elastic laminate of claim 16 .

30. A disposable infection control product comprising the elastic laminate of claim 16 .

31. A disposable personal care product comprising the elastic laminate of claim 16 .

32. An elastic laminate, comprising:

an elastic layer including about 25-100% by weight of a SEBSEB copolymer, zero to about 25% by weight of a poly(monoalkenyl arene), zero to about 25% by weight of a polyolefin, and zero to about 25% by weight of a tackifying resin; and

two nonwoven facing layers bonded to the elastic layer;

the SEBSEB copolymer having a number average molecular weight of at least about 70,000 and including a styrene end block, an ethylene-butylene midblock, a styrene midblock, and an ethylene-butylene end block, each of the blocks having a number average molecular weight;

the number average molecular weight of the styrene midblock being at least about 5% higher than the number average molecular weight of the styrene end block.

33. The elastic laminate of claim 32 , wherein the number average molecular weight of the styrene midblock is about 10-50% higher than the number average molecular weight of the styrene end block.

34. The elastic laminate of claim 32 , wherein the number average molecular weight of the styrene midblock is about 15-35% higher than the number average molecular weight of the styrene end block.

35. The elastic laminate of claim 32 , wherein:

the styrene end block has a number average molecular weight of about 6,000 to about 8,000;

the styrene midblock has a number average molecular weight of about 7,500 to about 9,000;

the ethylene-butylene midblock has a number average molecular weight of about 55,000 to about 70,000; and

the ethylene-butylene end block has a number average molecular weight of about 5,000 to about 12,000.

36. The elastic laminate of claim 32 , wherein the elastic layer includes about 50-80% by weight of the SEBSEB copolymer.

37. The elastic laminate of claim 32 , wherein the elastic layer includes about 4-15% by weight of the poly(monoalkenyl arene).

38. The elastic laminate of claim 32 , wherein the elastic layer includes about 5-20% by weight of the polyolefin.

39. The elastic laminate of claim 32 , wherein the elastic layer includes about 10-25% by weight of the tackifying resin.

40. A disposable garment comprising the elastic laminate of claim 32 .

41. A disposable infection control product comprising the elastic laminate of claim 32 .

42. A disposable personal care product comprising the elastic laminate of claim 32 .

43. The elastic laminate of claim 32 , wherein the nonwoven facing layers comprise spunbond webs.

44. The elastic laminate of claim 32 , wherein the elastic layer comprises an array of substantially continuous, nonintersecting filaments.

45. The elastic laminate of claim 44 , comprising a stretch-bonded laminate.

46. The elastic laminate of claim 32 , wherein the elastic layer comprises a material selected from a film, foam, fibrous nonwoven web, and combinations thereof.

47. The elastic laminate of claim 46 , comprising a neck-bonded laminate.

48. The elastic laminate of claim 46 , comprising a stretch-bonded laminate.

49. The elastic laminate of claim 46 , comprising a neck-stretch bonded laminate.

50. An elastic laminate, comprising:

an elastic layer including about 25-100% by weight of a SEBSEB tetrablock copolymer; and

at least one fibrous thermoplastic nonwoven facing layer bonded to the elastic layer;

wherein the elastic layer is formed of an elastic polymer composition having an elastic modulus at least 10% higher than for a control polymer composition including 80% by weight styrene-(ethylene-propylene)-styrene-(ethylene-propylene) tetrablock copolymer, 7% by weight polyethylene wax, and 13% by weight tackifying resin;

the SEBSEB copolymer having a number average molecular weight of at least about 70,000 and including a styrene end block, an ethylene-butylene midblock, a styrene midblock, and an ethylene-butylene end block;

the styrene midblock having a number average molecular weight about 5-50% higher than a number average molecular weight of the styrene end block.

51. The elastic laminate of claim 50 , wherein the elastic modulus for the elastic polymer composition is at least 25% higher than for the control polymer composition.

52. An elastic laminate, comprising:

an elastic layer including about 25-100% by weight of a SEBSEB tetrablock copolymer; and

at least one fibrous thermoplastic nonwoven facing layer bonded to the elastic layer;

wherein the elastic layer is formed of an elastic polymer composition having a stress at 50% elongation at least 5% higher than for a control polymer composition including 80% by weight styrene-(ethylene-propylene)-styrene-(ethylene-propylene) tetrablock copolymer, 7% by weight polyethylene wax, and 13% by weight tackifying resin;

the SEBSEB copolymer having a number average molecular weight of at least about 70,000 and including a styrene end block, an ethylene-butylene midblock, a styrene midblock, and an ethylene-butylene end block;

the styrene midblock having a number average molecular weight about 5-50% higher than a number average molecular weight of the styrene end block.

53. The elastic laminate of claim 52 , wherein the stress at 50% elongation for the elastic polymer composition is at least 15% higher than for the control polymer composition.

54. An elastic laminate, comprising:

an elastic layer including about 25-100% by weight of a SEBSEB tetrablock copolymer; and

at least one fibrous thermoplastic nonwoven facing layer bonded to the elastic layer;

wherein the elastic layer is formed of an elastic polymer composition having an elongation at break at least 10% higher than for a control polymer composition including 80% by weight styrene-(ethylene-propylene)-styrene-(ethylene-propylene) tetrablock copolymer, 7% by weight polyethylene wax, and 13% by weight tackifying resin;

the SEBSEB copolymer having a number average molecular weight of at least about 70,000 and including a styrene end block, an ethylene-butylene midblock, a styrene midblock, and an ethylene-butylene end block;

the styrene midblock having a number average molecular weight about 5-50% higher than a number average molecular weight of the styrene end block.

55. The elastic laminate of claim 54 , wherein the elastic polymer composition has a stress at break at least 40% higher than for the control polymer composition.

56. The elastic laminate of claim 55 , wherein the stress at break for the elastic polymer composition is at least 100% higher than for the control polymer composition.

Assignments (2)
NAME CHANGE Recorded Feb 3, 2015
From: KIMBERLY-CLARK WORLDWIDE, INC.
To: KIMBERLY-CLARK WORLDWIDE, INC.
Reel/Frame 034880/0742 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jul 31, 2003
From: THOMAS, OOMMAN PAINUMOOTTIL; MILDENHALL, GLEN THOMAS; NEEB, ALEXANDER; PAUL, SUSAN CAROL; MACE, TAMARA LEE; GARAVAGLIA, ARTHUR EDWARD
To: KIMBERLY-CLARK WORLDWIDE, INC.
Reel/Frame 014328/0808 →