Titanium dioxide scouring media and method of production
View Patent ↗The present invention relates to a round and spherical titanium dioxide scouring media and a method for producing the media. The scouring media is effective in removing titanium dioxide buildup on the walls of a titanium dioxide reaction vessel. The method consists of forming green titanium dioxide pellets in a high intensity mixer by mixing commercially available titanium dioxide dust and water. The high intensity mixer produces substantially round and spherical green pellets which are subsequently sized and sintered in a kiln to form round and spherical titanium dioxide sintered pellets that are suitable as a scouring media. The high intensity mixer allows the operator to closely control the size and shape of the pellets during the forming process to produce substantially round and spherical green pellets. Because the sintered titanium dioxide pellets are substantially round and spherical in shape, they are much less abrasive to the walls of the reaction vessel. Furthermore, as the pellets themselves abrade away, they do not contaminate the titanium dioxide product, and they can even be reprocessed into round and spherical scouring media.
1. A method for producing sintered titanium dioxide pellets comprising:
(a) mixing water and titanium dioxide dust in a high intensity mixer to form the titanium dioxide dust directly into substantially round and spherical green pellets;
(b) drying the titanium dioxide green pellets; and
(c) sintering the dried titanium dioxide pellets at 850° C. to about 1050° C.;
wherein the sintered titanium dioxide pellets have a substantially round and spherical shape that measures at least about 0.8 on the Krumbein/Sloss Roundness and Sphericity Chart.
2. The method according to claim 1 further comprising mixing a binder with the water and titanium dioxide dust.
3. The method according to claim 1 further comprising screening the substantially round and spherical green pellets prior to sintering.
4. The method according to claim 1 further comprising screening the sintered pellets.
5. The method of claim 1 wherein the titanium dioxide dust comprises at least about 90% titanium dioxide.
6. The method of claim 2 wherein the binder is selected from polyvinyl alcohol and starch.
7. The method of claim 1 wherein the sintered pellets have a bulk density from between about 1.38 g/cc to about 2.46 g/cc.
8. The method of claim 1 wherein the sintered pellets have a bulk density from between about 1.63 g/cc to about 2.46 g/cc.