IP Library Granted Patent US 7,442,727
Granted Patent B2
US 7,442,727 · App. 10/455,504 · Granted Oct 28, 2008

Pyrogenically prepared, surface modified aluminum oxide

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Quick Facts
Patent No.
US 7,442,727
App. No.
10/455,504
Granted
Oct 28, 2008
Kind
B2
Abstract

Pyrogenically prepared, surface modified aluminum oxide, having the following physical chemical properties: Surface area [m 2 /g]  50 to 150 Tamped density [g/L]  25 to 130 Drying loss [%] less than 5 Loss on ignition [%] 0.1 to 15  C content [%] 0.1 to 15  pH value 3 to 9 is prepared by treating pyrogenically prepared aluminum oxide with a surface modifying agent.

Claims (18)

1. A product consisting of a pyrogenically prepared, surface modified aluminum oxide modified by a surface modifying agent selected from the group consisting of octyltrimethoxysilane and octyltriethoxysilane, and having the following physical chemical properties:

Surface area [m 2 /g]

  50 to 150

Tamped density [g/L]

  25 to 130

Drying loss [%]

less than 5

Loss on ignition [%]

0.1 to 15

C content [%]

0.1 to 15

pH value

 3 to 9.

2. A corona resistant polymer composition comprising a filled thermosetting or thermoplastic polymer having dispersed within said polymer as a filler an additive consisting of the product according to claim 1 .

3. The corona resistant polymer composition according to claim 2 wherein the polymer is a polyimide.

4. A shaped article made from the polymer composition according to claim 2 .

5. A process for the preparation of the product in accordance with claim 1 , comprising spraying the pyrogenically prepared aluminum oxide with the surface modifying agent at room temperature to form a mixture and subsequently thermally treating the mixture at a temperature of 50 to 400° C. over a period of 1 to 6 h.

6. A process for the preparation of the product in accordance with claim 1 , comprising spraying the pyrogenically prepared aluminum oxide with the surface modifying agent in vapor form and to form a mixture subsequently thermally treating the mixture at a temperature of 50 to 800° C. over a period of 0.5 to 6 h.

Assignments (5)
CHANGE OF NAME Recorded Mar 29, 2020
From: EVONIK DEGUSSA GMBH
To: EVONIK OPERATIONS GMBH
Reel/Frame 052254/0052 →
CHANGE OF NAME Recorded Feb 23, 2010
From: DEGUSSA GMBH
To: EVONIK DEGUSSA GMBH
Reel/Frame 024006/0127 →
CHANGE ADDRESS Recorded Feb 22, 2010
From: EVONIK DEGUSSA GMBH
To: EVONIK DEGUSSA GMBH
Reel/Frame 023985/0296 →
CHANGE OF ENTITY Recorded Feb 22, 2010
From: DEGUSSA AG
To: DEGUSSA GMBH
Reel/Frame 023998/0937 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Aug 27, 2003
From: MEYER, JUERGEN; ETTLINGER, MANFRED
To: DEGUSSA AG
Reel/Frame 014424/0698 →