Method of manufacturing polymer particles
View Patent ↗A method of manufacturing polymer particles capable of increasing the easiness of handling of powder when the powder is collected and preventing the powder from adhering to the wall surface of a dryer and the outlet of the dryer from being clogged with the powder by suppressing the occurrence of ruptured particles to reduce the produced amount of the fine powder when polymer particles are produced by spraying and drying polymer latex, characterized in that, when the polymer latex having a minimum film forming temperature of 50° C. or higher is sprayed and dried with heating gas for drying in the dryer, the temperature of the heating gas for drying at the dryer outlet is less than the temperature obtained by adding 15° C. to the minimum film forming temperature of the polymer latex, the wet-bulb temperature thereof at the dryer outlet is higher than the temperature obtained by deducing 30° C. from the minimum film forming temperature of the polymer latex, and the heating gas for drying contains a vapor of 5 to 60 volume %.
1. A method of manufacturing polymer particles, comprising spray-drying at least one polymer latex having a minimum film forming temperature (T/° C.) of 50° C. or higher with heated gas in a spray-dryer that has a gas inlet and a gas outlet, wherein:
the temperature of the heated gas for drying the polymer latex at said outlet of the dryer (T 0 /° C.) is within the limits of the formula:
T 0 <T+ 15;
the wet-bulb temperature (T w /° C.) of the heated gas for drying the polymer latex at said outlet of the dryer is within the limits of the formula:
T w >T− 30; and
the content of steam in the heated gas ranges from 5 to 60% by volume.
2. The method according to claim 1 , wherein said polymer latex comprises a polymer having 35% by weight or more of one or more of methyl methacrylate monomer units or butyl methacrylate monomer units.
3. The method according to claim 2 , wherein said polymer latex comprises a polymer having 35% by weight or more of one or more of methyl methacrylate monomer units.
4. The method according to claim 1 wherein the moisture containing gas is air, nitrogen or carbon dioxide.