IP Library Granted Patent US 7,618,579
Granted Patent B2
US 7,618,579 · App. 10/477,882 · Granted Nov 17, 2009

Manufacturing device and the method of preparing for the nanofibers via electro-blown spinning process

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Quick Facts
Patent No.
US 7,618,579
App. No.
10/477,882
Granted
Nov 17, 2009
Kind
B2
Abstract

The invention relates to a nanofiber web preparing apparatus and method via electro-blown spinning. The nanofiber web preparing method includes feeding a polymer solution, which is a polymer dissolved into a given solvent, toward a spinning nozzle, discharging the polymer solution via the spinning nozzle, which is charged with a high voltage, while injecting compressed air via the lower end of the spinning nozzle, and collecting fiber spun in the form of a web on a grounded suction collector under the spinning nozzle, in which both of thermoplastic and thermosetting resins are applicable, the solution does not need to be heated and electrical insulation is readily realized.

Claims (17)

1. A method for preparing nanofiber webs comprising:

feeding a polymer solution comprising between 15 to 25 wt % polymer to a spinning nozzle;

compressively discharging the polymer solution through the spinning nozzle at a discharge rate between about 0.1 to 5 cc/min·hole, which is charged with a high voltage, while injecting compressed air through an air nozzle positioned adjacent the lower end of the spinning nozzle to form nanofibers; and collecting the nanofibers on a grounded collector under the spinning nozzle in the form of a nanofiber web.

2. The method of claim 1 , wherein the spinning nozzle is charged between about 1 to 300 kV.

3. The method of claim 1 , wherein the polymer solution is compressively discharged through the spinning nozzle under a discharge pressure in the range of 0.1 to 200 kg/cm 2 .

4. The method of claim 1 , wherein the compressed air has a flow rate of about 10 to 10,000 m/min and a temperature from about room temperature to 300° C.

5. The method of claim 4 , wherein the compressed air has a temperature ranging from room temperature to about 100° C.

6. The method of claim 1 , wherein said nanofiber web is spun directly onto the collector.

7. The method of claim 1 , wherein the nanofiber web is spun onto a substrate disposed on said collector.

8. The method of claim 1 , wherein the polymer is one of polyimide, nylon, polyaramide, polybenzimidazole, polyetherimide, polyacrylonitrile, PET (polyethylene terephthalate), polypropylene, polyaniline, polyethylene oxide, PEN (polyethylene naphthalate), PBT (polybutylene terephthalate), SBR (styrene butadiene rubber), polystyrene, PVC (polyvinyl chloride), polyvinyl alcohol, PVDF (polyvinylidene fluoride), polyvinyl butylene and copolymers or derivative compounds thereof.

9. The method of claim 1 , wherein the spun nanofibers are collected under vacuum onto the grounded collector.

10. A method for preparing nanofiber webs comprising:

feeding a polymer solution comprising between 15 to 25 wt % polymer to a spinning nozzle;

compressively discharging the polymer solution through the spinning nozzle at a discharge rate between about 0.1 to 5 cc/min·hole, which is charged with a high voltage, while injecting compressed air through an air nozzle positioned adjacent the discharge end of the spinning nozzle to form nanofibers; and collecting the nanofibers on a grounded collector in the form of a nanofiber web.

11. A method for preparing nanofiber webs comprising:

feeding a polymer solution comprising between 15 to 25 wt % polymer to a spinning nozzle; discharging the polymer solution through the spinning nozzle at a discharge rate between about 0.1 to 5 cc/min·hole and at a discharge pressure of between 0.1 to about 20 kg/cm 2 , which spinning nozzle is charged with a high voltage, while injecting compressed air through an air nozzle positioned adjacent the discharge end of the spinning nozzle to form nanofibers; and collecting the nanofibers on a grounded collector in the form of a nanofiber web.

12. The method of claim 11 , wherein said discharge pressure is between about 3 and 20 kg/cm 2 .

Assignments (1)
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jun 25, 2019
From: E. I. DU PONT DE NEMOURS AND COMPANY
To: DUPONT SAFETY & CONSTRUCTION, INC.
Reel/Frame 049586/0001 →