IP Library Granted Patent US 7,462,346
Granted Patent B2
US 7,462,346 · App. 10/487,329 · Granted Dec 9, 2008

Light-stabilized(in vivo) stain composition and method of manufacture

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Quick Facts
Patent No.
US 7,462,346
App. No.
10/487,329
Granted
Dec 9, 2008
Kind
B2
Abstract

Photochemical demethylation reactions in solutions of thiazine dyes, in which the dye molecules act as both sensitizer and substrate, are reduced by quenching triple-state dye molecules, returning them to the unreactive ground state.

Claims (6)

1. A method for at least partially reducing the oxidative demethylation of a thiazine dye, the method comprising the steps of:

(a) providing a thiazine dye in solution; and

(b) adding a metal ion to the thiazine dye solution;

wherein the thiazine dye comprises an inner thiazine ring and two outer rings, wherein at least one of the two outer rings has an -N-methylamino or an -N,N-dimethylamino substituent;

wherein the metal ion quenches the thiazine dye to at least partially reduce the oxidative demethylation of the thiazine dye; and

wherein the method further comprises the step of purifying the thiazine dye solution by high performance liquid chromatography before the step of adding the metal ion to the thiazine dye solution.

Assignments (2)
SECOND AMENDED AND RESTATED INTELLECTUAL PROPERTY SECURITY AGREEMENT Recorded Feb 26, 2014
From: DEN-MAT HOLDINGS, LLC; PERIOPTIX, INC.
To: MIDCAP FUNDING V, LLC, AS ADMINISTRATIVE AGENT
Reel/Frame 032382/0567 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Feb 20, 2014
From: ZILA, INC.
To: DEN-MAT HOLDINGS, LLC
Reel/Frame 032256/0187 →