IP Library Granted Patent US 7,396,595
Granted Patent B2
US 7,396,595 · App. 10/489,757 · Granted Jul 8, 2008

Soft metal and method for preparation thereof, and exterior part of watch and method for preparation thereof

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Quick Facts
Patent No.
US 7,396,595
App. No.
10/489,757
Granted
Jul 8, 2008
Kind
B2
Abstract

A soft metal and a decorative article of wristwatch are produced by forming, on the surface of a soft metal article ( 2 ), a hard layer ( 3, 13 ) containing zirconium and molybdenum, or containing zirconium, molybdenum and further an additive element constituted of at least one or more elements selected from niobium, tantalum, and titanium. It is preferable that the content of molybdenum constituting the hard layer ( 3, 13 ) is about 30 to 75 wt %, or that the content of molybdenum is about 25 to 65 wt % and the total content of the additive elements is about 25 wt % or less.

Claims (34)

1. A soft metal article, comprising:

a substrate made of soft metal; and

a hard layer formed on a surface of said substrate, said hard layer containing

about 30 to 75 wt % of molybdenum, and

the balance essentially of zirconium,

wherein said hard layer is formed through an intermediate hard layer made of an alloy containing at least one selected from iron, cobalt, and nickel.

2. The soft metal article according to claim 1 , wherein a content of molybdenum constituting said hard layer is about 30 to 60 wt %.

3. A soft metal article, comprising:

a substrate made of soft metal; and

a hard layer formed on a surface of said substrate, said hard layer containing

about 25 to 65 wt % of molybdenum,

about 25 wt % or less of an additive element constituted of one or more selected from niobium, tantalum, and titanium, and

the balance essentially of zirconium,

wherein said hard layer is formed through an intermediate hard layer made of an alloy containing at least one selected from iron, cobalt, and nickel.

4. The soft metal article according to claim 3 , wherein a total content of molybdenum and additive elements constituting said hard layer is about 30 to 80 wt %.

5. The soft metal article according to claim 3 , wherein a total content of molybdenum and additive elements constituting said hard layer is about 30 to 55 wt %.

6. A decorative article, comprising:

a substrate made of soft metal; and

a hard layer formed on a surface of said substrate, said hard layer containing

about 30 to 75 wt % of molybdenum, and

the balance essentially of zirconium,

wherein said decorative article is a decorative article of wristwatch, and

wherein said hard layer is formed through an intermediate hard layer made of an alloy containing at least one selected from iron, cobalt, and nickel.

7. The decorative article of wristwatch according to claim 6 , wherein a content of molybdenum constituting said hard layer is about 30 to 60 wt %.

8. A decorative article, comprising:

a substrate made of soft metal; and

a hard layer formed on a surface of said substrate, said hard layer containing

about 25 to 65 wt % of molybdenum,

about 25 wt % or less of an additive element constituted of at least one or more selected from niobium, tantalum, and titanium, and

the balance essentially of zirconium,

wherein said decorative article is a decorative article of wristwatch, and

wherein said hard layer is formed through an intermediate hard layer made of an alloy containing at least one selected from iron, cobalt, and nickel.

9. The decorative article of wristwatch according to claim 8 , wherein a total content of molybdenum and additive elements constituting said hard layer is about 30 to 80 wt %.

10. The decorative article of wristwatch according to claim 8 , wherein a total content of molybdenum and additive elements constituting said hard layer is about 30 to 55 wt %.

Assignments (3)
CHANGE OF NAME Recorded Jan 25, 2017
From: CITIZEN HOLDINGS CO., LTD.
To: CITIZEN WATCH CO., LTD.
Reel/Frame 041479/0804 →
CHANGE OF NAME Recorded Jul 20, 2007
From: CITIZEN WATCH CO., LTD.
To: CITIZEN HOLDINGS CO., LTD.
Reel/Frame 019580/0654 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Mar 17, 2004
From: SHIBUYA, YOSHITSUGU; SATOH, JUNJI; ITO, SHIZUE
To: CITIZEN WATCH CO., LTD.
Reel/Frame 015639/0012 →