IP Library Granted Patent US 7,776,854
Granted Patent B2
US 7,776,854 · App. 10/496,785 · Granted Aug 17, 2010

Benzazole derivatives for the treatment of scleroderma

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Quick Facts
Patent No.
US 7,776,854
App. No.
10/496,785
Granted
Aug 17, 2010
Kind
B2
Abstract

The present invention is related to the use of benzazole derivatives of formula (I) for the treatment and/or prevention of scleroderma and its therapeutic implications selected in the group consisting of systemic sclerosis, scleroderma-like disorders, sine scleroderma, liver cirrhosis, interstitial pulmonary fibrosis, Dupuytren's contracture, keloid and other scarring/wound healing abnormalities, postoperative adhesions and reactive fibrosis, as well as chronic heart failure, in particular after myocardial infarction.

Claims (24)

1. A method for treating interstitial pulmonary fibrosis, comprising administering to a patient in need thereof that is suffering from interstitial pulmonary fibrosis an effective amount of a benzothiazole according to formula I

or its tautomers, its geometrical isomers, its optically active forms as enantiomers, diastereomers and its racemate forms, pharmaceutically acceptable salts thereof, and combinations thereof, wherein:

X is O, S or NR 0 , with R 0 being H or an C 1 -C 6 alkyl;

G is an pyrimidinyl group of the formula

wherein L is selected from the group consisting of hydrogen, C 1 -C 6 alkyl, C 1 -C 6 alkoxy, C 1 -C 6 thioalkoxy, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, primary, secondary or tertiary amino groups, aminoacyl, aminocarbonyl, amino-(C 1 -C 10 )alkyl, amino-(C 1 -C 10 )-alkyl-aryl, amino-(C 1 -C 10 )alkyl-heteroaryl, C 1 -C 6 alkoxycarbonyl, carboxyl, cyano, halogen, hydroxy, nitro, sulfoxy, sulfonyl, aryl, heteroaryl, 3-8 membered cycloalkyl, optionally containing at least one heteroatom selected from N, O, S, and hydrazido groups, wherein the arrow indicates the point of attachment;

R 1 is selected from the group consisting of hydrogen, C 1 -C 6 -alkoxy, C 1 -C 6 -thioalkoxy, C 1 -C 6 -alkyl, C 2 -C 6 -alkenyl, C 2 -C 6 -alkynyl, primary, secondary or tertiary amino groups, aminoacyl, aminocarbonyl, C 1 -C 6 alkoxycarbonyl, aryl, heteroaryl, carboxyl, cyano, halogen, hydroxy, nitro, sulfoxy, sulfonyl, sulfonamide or hydrazides;

R 2 is selected from the group consisting of hydrogen, C 1 -C 6 -alkyl, C 2 -C 6 -alkenyl, C 2 -C 6 -alkynyl, C 1 -C 6 -alkyl-aryl, aryl or heteroaryl, C 1 -C 6 -alkyl-heteroaryl, —C(O)—OR 3 , —C(O)—R 3 , —C(O)—NR 3 R 3′ , —(SO 2 )R 3 , with

R 3 and R 3′ being independently selected from the group consisting of hydrogen, C 1 -C 6 alkyl, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, aryl, heteroaryl, C 1 -C 6 -alkyl aryl, C 1 -C 6 -alkyl heteroaryl.

2. The method of claim 1 , wherein said benzothiazole is 1,3-benzothiazol-2-yl(2-{[4-(morpholin-4-ylmethyl)benzyl]oxy}pyrimidin-4-yl)-acetonitrile.

3. The method of claim 1 , wherein R 1 is selected from the group consisting of hydrogen, halogen, C 1 -C 6 alkyl or C 1 -C 6 alkoxy.

4. The method of claim 1 , wherein the benzothiazole is its tautomer according to formula II

or its geometrical isomers, its optically active forms as enantiomers, diastereomers and racemate forms, pharmaceutically acceptable salts thereof, and combinations thereof, wherein

G is a pyrimidinyl group of the formula

wherein L is selected from the group consisting of hydrogen, C 1 -C 6 alkyl, C 1 -C 6 alkoxy, C 1 -C 6 thioalkoxy, C 2 -C 6 alkenyl, C 2 -C 6 alkynyl, primary, secondary or tertiary amino groups, aminoacyl, aminocarbonyl, amino-(C 1 -C 10 )alkyl, amino-(C 1 -C 10 )-alkyl-aryl, amino-(C 1 -C 10 )alkyl-heteroaryl, C 1 -C 6 alkoxycarbonyl, carboxyl, cyano, halogen, hydroxy, nitro, sulfoxy, sulfonyl, aryl, heteroaryl, 3-8 membered cycloalkyl, optionally containing at least one heteroatom selected from N, O, S, and hydrazido groups wherein the arrow indicates the point of attachment; and

R 1 is selected from the group consisting of hydrogen, C 1 -C 6 -alkoxy, C 1 -C 6 -thioalkoxy, C 1 -C 6 -alkyl, C 2 -C 6 -alkenyl, C 2 -C 6 -alkynyl, primary, secondary or tertiary amino groups, aminoacyl, aminocarbonyl, C 1 -C 6 alkoxycarbonyl, aryl, heteroaryl, carboxyl, cyano, halogen, hydroxy, nitro, sulfoxy, sulfonyl, sulfonamide, hydrazides.

5. The method of claim 1 or 4 , wherein L is a group —N(R a , R b ) or —OR a , with R a and R b being each independently selected from the group consisting of H, (C 1 -C 10 )-alkyl, C 1 -C 6 alkyl-aryl, C 1 -C 6 -alkyl-heteroaryl, aryl or heteroaryl and 4-8 membered saturated or unsaturated cycloalkyl.

6. The method of claim 5 , wherein L is selected from the group consisting of:

wherein n is 1 to 10, and

R 5 and R 5′ are independently selected from each other from the group consisting of H, C 1 -C 10 alkyl, aryl or heteroaryl, C 1 -C 6 alkyl-aryl and C 1 -C 6 -alkyl-heteroaryl.

7. The method of claim 6 , wherein n is 1 to 6.

8. The method of claim 6 , wherein X is S, R 1 and R 2 are H or C 1 -C 6 alkyl, G is a pyrimidinyl group

with L being either

wherein n is 0, 1 or 2 and R 5 is an aryl or heteroaryl.

9. The method of claim 8 , wherein R 5 is phenyl, pyridyl or imidazolyl.

Assignments (4)
CHANGE OF NAME Recorded Nov 25, 2009
From: LABORATOIRES SERONO SA
To: MERCK SERONO SA
Reel/Frame 023569/0120 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Sep 11, 2007
From: APPLIED RESEARCH SYSTEMS ARS HOLDING N.V.
To: LABORATOIRES SERONO SA
Reel/Frame 019966/0026 →
CORRECTIVE ASSIGNMENT PREVIOUSLY RECORDED AT REEL 016225 FRAME 0189 TO CORRECT THE NAME OF THE 3RD CONVEYING PARTY. CONVEYING PARTIES HEREBY CONFIRM THE ASSIGNMENT OF THE ENTIRE INTEREST. Recorded Aug 3, 2005
From: GOTTELAND, JEAN-PIERRE; GAILLARD, PASCALE; CHVATCHKO, YOLENDE
To: APPLIED RESEARCH SYSTEMS ARS HOLDING N.V.
Reel/Frame 016917/0231 →
ASSIGNMENT OF ASSIGNOR'S INTEREST Recorded Jan 31, 2005
From: GOTTELAND, JEAN-PIERRE; GAILLARD, PASCALE; CHVATCHKO, YVONNE
To: APPLIED RESEARCH SYSTEMS ARS HOLDING N.V.
Reel/Frame 016225/0189 →