IP Library Granted Patent US 7,704,424
Granted Patent B2
US 7,704,424 · App. 10/498,692 · Granted Apr 27, 2010

Method of making models

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Quick Facts
Patent No.
US 7,704,424
App. No.
10/498,692
Granted
Apr 27, 2010
Kind
B2
Abstract

A method of a seamless model free of bond lines. The method includes the sequential steps of providing a substructure having an exposed outer surface, applying a modelling paste to a structure support in the form of a continuous layer, curing the applied modelling paste, and machining the cured layer of modelling paste to the desired contour. The modelling paste a low density curable composition prepared from thixotropic epoxy or polyurethane containing microballoons.

Claims (18)

1. A method of making a seamless model comprising the steps of:

a) providing at least one tank filled with a resin component and tank filled with a hardener component;

b) delivering the resin component and hardener component from the tanks to a mix block and mixing the resin component and hardener component to produce a modeling paste wherein the modeling paste is a low density thixotropic curable paste comprising a resin composition and microballoons;

c) dispensing the modeling paste onto an outer surface of a support in a continuous layer;

d) curing the paste at room temperature; and

e) machining the cured paste to a desired or pre-determined contour to form the seamless model

wherein the microballoons are present in an amount of greater than about 50% and less than about 80% of the uncured paste by volume and wherein the density of the uncured paste is in the range of about 0.4 to about 0.9 g/cm 3 and

wherein the resin composition comprises:

(i) an epoxy resin;

(ii) a thixotropic agent; and

(iii) a hardener comprising at least one polyethyleneimine and at least one other amine having at least two hydrogen groups.

2. The method of claim 1 wherein the thixotropic agent is selected from the group consisting of: a hydrogen-bonding type of thixotropic agent present in an amount of about 0.2 to about 4% by weight of the paste; and a chemical thixotropic agent present in an amount of about 0.05 to about 1.5% by weight of the paste.

3. The method of claim 1 wherein the paste includes a filler in an amount of about 1% to about 30% by weight based on the weight of the paste.

4. The method of claim 1 wherein the thixotropic agent comprises a hydrophilic fumed silica and is present in an amount of about 1% to about 20% by weight based on the weight of the epoxy resin.

5. The method of claim 1 wherein the polyethyleneimine has a molecular weight of about 700 to about 1,000,000 and is present in an amount of about 0.2-2 parts by weight per 100 parts by weight of the epoxy resin.

6. The method of claim 5 wherein the other amine is an aliphatic amine comprising an N-hydroxyalkyl derivative of a polyalkylene polyamine and a polyaminoamide reaction product of a polyalkylenepolyamine and a polymerized vegetable oil acid.

7. The method of claim 1 wherein the resin composition further comprises ethylenically unsaturated component.

8. The method of claim 1 wherein the paste further comprises at least one molecular sieve, surfactant, antifoaming agent and calcium stearate.

Assignments (2)
TERMINATION AND RELEASE OF SECURITY INTEREST IN UNITED STATES TRADEMARKS AND PATENTS Recorded Jun 13, 2018
From: JPMORGAN CHASE BANK, N.A.
To: HUNTSMAN ADVANCED MATERIALS AMERICAS INC. (N/K/A HUNTSMAN ADVANCED MATERIALS AMERICAS LLC)
Reel/Frame 046352/0893 →
CORRECTIVE ASSIGNMENT TO CORRECT THE NATURE OF CONVEYANCE FROM ASSIGNMENT TO SECURITY AGREEMENT PREVIOUSLY RECORDED ON REEL 025855 FRAME 0192. ASSIGNOR(S) HEREBY CONFIRMS THE ASSIGNMENT. Recorded Jun 28, 2011
From: DEUTSCHE BANK TRUST AG NEW YORK BRANCH, AS RESIGNING ADMINISTRATIVE AGENT AND COLLATERAL AGENT
To: JPMORGAN CHASE BANK, N.A., AS COLLATERAL AGENT
Reel/Frame 026515/0735 →